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ericlee99

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[交流] 【求助】求高人指点迷津

我是个菜鸟,投了ACTA E,编辑给回复了,理解的不太好。那位好人给解释些我需要做点什么
Please find attached the final *.res file I obtained.

I have added the manner in which to get the hydrogen bonds and which are then automatically added to the CIF.

I also refined the C-C distances in the isopropyl groups with distance restraints.

As the absolute configuration is unknown then you can merge the Friedel pairs using the MERG 4 instructruction.


The final C Alerts I got with checkcif are reasonable.

It would suggest you make
Fig. 1 as the view of the molecular structure of the first molecule with the labels.

Provide a Fig. 2 with all four molecules but just label the O atoms in all foru molecules
and a
Fig. 3 showing the crystal packing with the O-H...O hydroge bonds.
Omit all the C-bound H-atoms to do this.

If you have the program PLATON you will find it is easy to do this.
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yunruirui

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nash603(金币+1):谢谢回贴交流! 2011-01-04 10:11:00
ericlee99(金币+20):谢谢 2011-01-06 15:54:24
你需要做的就是上传有第一个分子的图要求标注原子,提供四个分子图只标注氧原子,画出氢键堆积图,使用platon软件很好做到,
2楼2011-01-03 20:01:30
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lilywang501

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帝夫(金币+1):感谢回帖交流! 2011-01-05 09:48:10
ericlee99(金币+20):谢谢 2011-01-06 15:55:16
编辑已经帮你处理好了氢键,以及限制了C-C键长,为了获得绝对构型,你需要在ins文件中加入 merg 4 命令拼合衍射点,其它的就是提供三个图啦
3楼2011-01-05 09:47:38
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