24小时热门版块排行榜    

查看: 320  |  回复: 2

ericlee99

金虫 (正式写手)


[交流] 【求助】求高人指点迷津

我是个菜鸟,投了ACTA E,编辑给回复了,理解的不太好。那位好人给解释些我需要做点什么
Please find attached the final *.res file I obtained.

I have added the manner in which to get the hydrogen bonds and which are then automatically added to the CIF.

I also refined the C-C distances in the isopropyl groups with distance restraints.

As the absolute configuration is unknown then you can merge the Friedel pairs using the MERG 4 instructruction.


The final C Alerts I got with checkcif are reasonable.

It would suggest you make
Fig. 1 as the view of the molecular structure of the first molecule with the labels.

Provide a Fig. 2 with all four molecules but just label the O atoms in all foru molecules
and a
Fig. 3 showing the crystal packing with the O-H...O hydroge bonds.
Omit all the C-bound H-atoms to do this.

If you have the program PLATON you will find it is easy to do this.
回复此楼

» 猜你喜欢

» 抢金币啦!回帖就可以得到:

查看全部散金贴

已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

yunruirui

荣誉版主 (著名写手)



nash603(金币+1):谢谢回贴交流! 2011-01-04 10:11:00
ericlee99(金币+20):谢谢 2011-01-06 15:54:24
你需要做的就是上传有第一个分子的图要求标注原子,提供四个分子图只标注氧原子,画出氢键堆积图,使用platon软件很好做到,
2楼2011-01-03 20:01:30
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

lilywang501

金虫 (小有名气)



帝夫(金币+1):感谢回帖交流! 2011-01-05 09:48:10
ericlee99(金币+20):谢谢 2011-01-06 15:55:16
编辑已经帮你处理好了氢键,以及限制了C-C键长,为了获得绝对构型,你需要在ins文件中加入 merg 4 命令拼合衍射点,其它的就是提供三个图啦
3楼2011-01-05 09:47:38
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
相关版块跳转 我要订阅楼主 ericlee99 的主题更新
普通表情 高级回复 (可上传附件)
信息提示
请填处理意见