24小时热门版块排行榜    

查看: 1975  |  回复: 11
当前只显示满足指定条件的回帖,点击这里查看本话题的所有回帖

wanss

铁虫 (正式写手)


[交流] 【求助】支架材料的制备方法

看到一篇文献,制备支架材料,叙述如下:
Scaffold preparation by solid–liquid phase separation: a known amount of polylactide was dissolved in dioxane to form solutions with desired concentrations. Four different concentrations of PLLA solution (0.5, 1.0, 3.0 and 5.0% w/v) were frozen and maintained over 2 hr to induce solid–liquid phase separation completely. The clear 5% PLLA solutions were poured into aluminum foil molds (4x4 cm2) which were fast-frozen in liquid
nitrogen, ice-water bath or freezer, respectively, and then were maintained at those
temperatures for over 2 hr to induce solid–liquid phase separation completely. Solvent was removed by freeze-drying for 3 days and the dried scaffolds were then kept in a desiccator until characterization or usage.
此方法是固液相分离法。把PLA溶在dioxane中,通过冷冻就可以固液相分离吗,什么原理啊?
冷冻后为什么会出现固液分离(solid-liquid phase separation)啊?

[ Last edited by wanss on 2010-11-29 at 19:15 ]
回复此楼
已阅   关注TA 给TA发消息 送TA红花 TA的回帖

placopolymer

金虫 (职业作家)



shileinjut:谢谢参与! 2010-11-28 00:03:39
americanyk(金币+1):Thank you 2010-11-28 17:43:18
americanyk:编辑内容 2010-11-28 10:43
冷冻,溶剂升华形成多孔,我们使用溶盐制孔发制备多孔支架.

[ Last edited by americanyk on 2010-11-28 at 10:43 ]
5楼2010-11-27 19:11:01
已阅   关注TA 给TA发消息 送TA红花 TA的回帖
查看全部 12 个回答

毁人不倦

银虫 (正式写手)


★ ★
americanyk(金币+2):tks 新虫 2010-11-27 16:15:31
wanss(金币+2): 2010-11-28 04:36:45
本人个人理解,首先溶剂带着溶质进入模具,然后降温冷却模具中的溶液,溶剂变为固体,形成模具设计的形状,然后抽真空除去溶剂,剩余溶质。不知道对不对?
2楼2010-11-27 15:39:40
已阅   关注TA 给TA发消息 送TA红花 TA的回帖

axiu3961

捐助贵宾 (职业作家)



wanss(金币+3): 2010-11-27 17:19:02
americanyk(金币+1):Thank you 2010-11-27 18:03:48
溶液配制后,先0°C下降温保持2个小时,去上层清夜再在低温冷冻,然后冻干去掉溶液。这样可能可以制作出多空支架。
3楼2010-11-27 16:59:51
已阅   关注TA 给TA发消息 送TA红花 TA的回帖

placopolymer

金虫 (职业作家)



shileinjut(金币+1):谢谢参与! 2010-11-28 00:03:29
冷冻,溶剂升华形成多孔
4楼2010-11-27 19:10:16
已阅   关注TA 给TA发消息 送TA红花 TA的回帖
最具人气热帖推荐 [查看全部] 作者 回/看 最后发表
[基金申请] 为什么资助数各大高校都创新高,自己申请怎么就这么难 +9 Kittylucky 2026-08-27 9/450 2026-08-28 01:08 by jurkat.1640
[教师之家] 售SCI文章,我:8O5.5.1.O.54,科目齐全,可+急 +3 XLGfUIdOmEAO 2026-08-27 4/200 2026-08-27 22:26 by 3RAFyYXYSwGS
[教师之家] 导师吐槽:我怎么摊上了这么个极品研究生! +7 苏东坡二世 2026-08-23 7/350 2026-08-27 18:14 by 瞬息宇宙
[基金申请] 基金不中,共勉 +10 eulota 2026-08-26 10/500 2026-08-27 17:23 by lqllinqiaoli
[文学芳草园] 梦想 +3 myrtle 2026-08-26 3/150 2026-08-27 10:01 by angelyueyi
[教师之家] 售SCI一区文章,我:8.O.551.O.5.4,科目全,可伽急 +3 LIbGuocjEEYw 2026-08-26 4/200 2026-08-27 04:33 by Ie9AyIAvGbvs
[硕博家园] 售SCI一区T0P文章,我:8.O.55.1.O.54,科目齐全,可+急 +3 LIbGuocjEEYw 2026-08-26 4/200 2026-08-27 02:01 by Ie9AyIAvGbvs
[基金申请] 系统查不到 +10 董八千 2026-08-26 10/500 2026-08-26 16:30 by Equinoxhua
[基金申请] 怎么查啊 +5 huang1991js 2026-08-26 5/250 2026-08-26 16:09 by Equinoxhua
[基金申请] 范进中举一文的中心思想 +9 炎黄贵胄 2026-08-22 10/500 2026-08-26 15:40 by semaglutide
[基金申请] 能否退出参与的面上项目解除限项 +23 koalala 2026-08-24 26/1300 2026-08-26 14:29 by 宝贝虫子
[基金申请] 为什么国自然不能直接公布 +4 bjdxyxy 2026-08-26 4/200 2026-08-26 13:12 by qingmu1201
[基金申请] 国际合作可查了,中了面上 (EPI+1)(金币+50) +18 Ldrop2023 2026-08-26 18/900 2026-08-26 11:15 by cmrandy
[基金申请] 今天务委会开完了,明天出结果吗 +19 angus9576 2026-08-25 23/1150 2026-08-26 10:03 by zp519
[基金申请] 在坚冰还盖着北海的时候,我看到了怒放的梅花。 (金币+10) +6 ziyangfang 2026-08-25 9/450 2026-08-25 20:26 by huagongfeihu
[基金申请] 明天应该可查了!? +6 chengyan1220 2026-08-23 6/300 2026-08-25 19:45 by zfd97
[基金申请] 某些机构,以效率低为荣,以效率低作为存在感 +9 yuleib84 2026-08-25 10/500 2026-08-25 17:14 by alexon
[基金申请] 人气不行了 +11 fansofjerry 2026-08-21 11/550 2026-08-25 11:04 by 孤独的英雄6
[基金申请] 建议基金发布提前给出明确的时间点 +13 kulium 2026-08-21 16/800 2026-08-24 16:27 by superceng
[基金申请] 看来今天不会放榜了? +8 chengyan1220 2026-08-21 11/550 2026-08-21 17:52 by dcqxinyang
信息提示
请填处理意见