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2楼2010-11-03 11:22:07
daxu
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3楼2010-11-03 12:41:05
4楼2010-11-03 14:23:35
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小木虫(金币+0.5):给个红包，谢谢回帖交流
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Name and formula Reference code: 00-012-0219 Mineral name: Montmorillonite-18A PDF index name: Sodium Magnesium Aluminum Silicate Hydroxide Hydrate Empirical formula: Al2H14Mg2Na0.3O17Si4 Chemical formula: Na0.3 ( AlMg )2Si4O10OH2 ?6H2O Crystallographic parameters Crystal system: Hexagonal Space group: P a (?): 5.1950 b (?): 5.1950 c (?): 17.9300 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 120.0000 Volume of cell (10^6 pm^3): 419.07 Z: 1.00 RIR: - Subfiles and Quality Subfiles: Inorganic Mineral Corrosion Educational pattern Forensic Pigment/Dye Quality: Indexed (I) Comments Color: White, yellow, green Sample source: Specimen from Chambers, Arizona, USA. Sample preparation: Glycol sodium saturated. Optical data: A=1.48-1.61, B=1.50-1.64, Q=1.50-1.64, Sign=-, 2V=15(15)? Additional pattern: To replace 00-012-0204. References Primary reference: Earley et al., Am. Mineral., 38, 707, (1953) Optical data: Deer, W., Howie, R., Zussman, J., Rock Forming Minerals, 3, 226, (1962) Unit cell: Bayliss, P., Powder Diffraction, 4, 19, (1989) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 17.60000 5.017 100.0 2 0 0 2 9.00000 9.820 50.0 3 0 0 3 5.99000 14.777 10.0 4 0 0 4 4.49000 19.757 80.0 5 0 0 5 3.58000 24.851 40.0 6 0 0 6 2.99000 29.858 30.0 7 1 1 1 2.57000 34.882 40.0 8 0 0 8 2.24200 40.190 10.0 9 0 0 9 1.98900 45.571 5.0 10 2 1 0 1.69900 53.922 20.0 11 3 0 0 1.50400 61.617 60.0 12 3 0 7 1.29400 73.066 10.0 13 3 1 0 1.25000 76.084 10.0 |
5楼2010-11-04 08:52:06
daxu
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Name and formula Reference code: 00-013-0135 Mineral name: Montmorillonite-15A PDF index name: Calcium Magnesium Aluminum Silicate Hydroxide Hydrate Empirical formula: Al2Ca0.2H10O16Si4 Chemical formula: Ca0.2 ( Al , Mg )2Si4O10 ( OH )2 ?4H2O Crystallographic parameters Crystal system: Hexagonal Space group: P a (?): 5.1690 b (?): 5.1690 c (?): 15.0200 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 120.0000 Measured density (g/cm^3): 2.30 Volume of cell (10^6 pm^3): 347.55 Z: 1.00 RIR: - Subfiles and Quality Subfiles: Inorganic Mineral Corrosion Common Phase Educational pattern Forensic Quality: Blank (B) Comments Color: White, yellow, green Sample source: Specimen from Skyrvedalen, Hemsedal, Norway. Analysis: Analysis (wt.%): SiO2 59.58, Al2O3 22.96, Fe2O3 0.47, MgO 3.67, CaO 3.38, Na2O 0.06, loss 110-950? 9.61. Optical data: A=1.545(6), B=1.57(7), Q=1.57(7), Sign=-, 2V=0(15)? References Primary reference: Rosenquist., Nor. Geol. Tidsskr., 39, 350, (1959) Unit cell: Bayliss, P., Powder Diffraction, 4, 19, (1989) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 15.00000 5.887 100.0 2 0 0 3 5.01000 17.689 60.0 3 1 0 0 4.50000 19.713 80.0 4 0 0 4 3.77000 23.580 20.0 5 3.50000 25.428 10.0 6 1 0 3 3.30000 26.998 10.0 7 0 0 5 3.02000 29.555 60.0 8 1 1 0 2.58000 34.743 40.0 9 0 0 6 2.50000 35.892 40.0 10 2 0 0 2.26000 39.856 10.0 11 0 0 7 2.15000 41.989 10.0 12 0 0 8 1.88000 48.376 10.0 13 2 1 0 1.70000 53.888 30.0 14 0 0 10 1.50000 61.799 50.0 15 3 0 0 1.49300 62.121 50.0 16 2 2 1 1.28500 73.662 20.0 17 3 1 0 1.24300 76.590 20.0 Stick Pattern |
6楼2010-11-04 08:52:22
daxu
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Name and formula Reference code: 00-013-0259 Mineral name: Montmorillonite-14A PDF index name: Sodium Magnesium Aluminum Silicate Hydroxide Hydrate Chemical formula: Na0.3 ( Al , Mg )2Si4O10 ( OH )2 ?xH2O Crystallographic parameters Crystal system: Unknown Measured density (g/cm^3): 2.50 RIR: - Subfiles and Quality Subfiles: Inorganic Mineral Corrosion Common Phase Educational pattern Forensic Quality: Doubtful (O) Comments Color: White, yellow, green Sample source: Specimen from Polkville mine, Polkville, Mississippi, USA. Analysis: Chemical analysis (wt.%): SiO2 50.95, Al2O3 16.54, Fe2O3 1.36, FeO 0.26, MgO 4.65, CaO 2.26, Na2O 0.17, K2O 0.47, H2O 23.29. Optical data: A=1.545(6), B=1.57(7), Q=1.57(7), Sign=-, 2V=15(15)? Reason "O" quality: O assigned because unindexed. References Primary reference: Molloy, Kerr., Am. Mineral., 46, 583, (1961) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 13.60000 6.494 100.0 2 4.47000 19.846 18.0 3 3.34000 26.668 10.0 4 3.23000 27.594 10.0 5 2.92000 30.591 8.0 6 2.59000 34.605 5.0 7 2.49000 36.041 5.0 Stick Pattern |
7楼2010-11-04 08:52:39
daxu
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Name and formula Reference code: 00-029-1498 Mineral name: Montmorillonite-15A PDF index name: Sodium Magnesium Aluminum Silicate Hydroxide Hydrate Empirical formula: Al2H10Na0.3O16Si4 Chemical formula: Na0.3 ( Al , Mg )2Si4O10 ( OH )2 ?4H2O Crystallographic parameters Crystal system: Hexagonal Space group: P a (?): 5.1650 b (?): 5.1650 c (?): 15.5400 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 120.0000 Volume of cell (10^6 pm^3): 359.02 Z: 1.00 RIR: - Subfiles and Quality Subfiles: Inorganic Mineral Corrosion Common Phase Educational pattern Forensic Quality: Doubtful (O) Comments General comments: Reflection at 3.13 (I=80) was deleted, because it was probably cristobalite. Sample source: Specimen from Wyoming, USA. Sample preparation: 50% relative humidity. Additional pattern: To replace 00-002-0037, 00-003-0009 and 00-003-0016. References Primary reference: Brindley, G., Penn State Univ., University Park, PA, USA., ICDD Grant-in-Aid, (1977) Unit cell: Bayliss, P., Powder Diffraction, 4, 19, (1989) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 13.60000 6.494 100.0 2 0 0 3 5.16000 17.171 12.0 3 1 0 0 4.46000 19.891 65.0 4 1 0 5 2.56000 35.023 18.0 5 2 1 0 1.69000 54.233 8.0 6 3 0 0 1.49500 62.028 12.0 Stick Pattern |
8楼2010-11-04 08:52:52
daxu
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Name and formula Reference code: 00-029-1499 Mineral name: Montmorillonite-22A PDF index name: Sodium Magnesium Aluminum Silicate Hydroxide Hydrate Empirical formula: Al2H18Na0.3O20Si4 Chemical formula: Na0.3 ( Al , Mg )2Si4O10 ( OH )2 ?8H2O Crystallographic parameters Crystal system: Hexagonal Space group: P a (?): 5.2100 b (?): 5.2100 c (?): 22.0000 Alpha (°): 90.0000 Beta (°): 90.0000 Gamma (°): 120.0000 Volume of cell (10^6 pm^3): 517.16 Z: 1.00 RIR: - Subfiles and Quality Subfiles: Inorganic Mineral Corrosion Common Phase Educational pattern Quality: Star (S) Comments General comments: Reflection at 3.15 (I=40) was deleted, because it was probably cristobalite. Sample source: Specimen from Wyoming, USA. Sample preparation: Stored over water, four days, 100% relative humidity. References Primary reference: Brindley, G., Penn State Univ., University Park, PA, USA., ICDD Grant-in-Aid, (1977) Unit cell: Bayliss, P., Powder Diffraction, 4, 19, (1989) Peak list No. h k l d [A] 2Theta[deg] I [%] 1 0 0 1 21.50000 4.106 100.0 2 0 0 2 10.60000 8.335 18.0 3 1 0 1 4.45000 19.936 55.0 4 1 0 7 2.56000 35.023 35.0 5 0 0 13 1.69000 54.233 8.0 6 2 0 11 1.49500 62.028 25.0 7 3 0 8 1.32500 71.092 8.0 Stick Pattern |
9楼2010-11-04 08:53:06
10楼2010-11-04 10:47:01
5