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ting110新虫 (初入文坛)
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[交流]
【求助】铟单质、氧化铟、氮化铟 具体的晶格结构？不同晶格结构对晶体形貌的影响已有3人参与
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最好是用CCDC帮我查一个铟单质、氧化铟、氮化铟 具体的晶格结构，我自己实在是不会弄。 还有一个重要问题是：我是做掺杂实验，请问用不同的晶格结构的源，对合成物的形貌是怎样影响的呢？（其他条件不变）最好以铟单质、氧化铟、氮化铟 为例。 拜托各位了！！！！  |
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zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
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Al
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*data for ICSD #240129 Coll Code 240129 Rec Date 2004/10/01 Mod Date 2006/04/01 Chem Name Aluminium Structured Al Sum Al1 ANX N D(calc) 2.68 Title Stoichiometry of U Al4 Author(s) Tougait, O.;Noel, H. Reference Intermetallics (2004), 12, 219-223 Unit Cell 4.056(1) 4.056(1) 4.056(1) 90 90 90 Vol 66.73 Z 4 Space Group F m -3 m SG Number 225 Cryst Sys cubic Pearson cF4 Wyckoff a Red Cell F 2.868 2.868 2.868 60 60 60 16.681 Trans Red 0.500 0.500 0.000 / 0.000 0.500 0.500 / 0.500 0.000 0.500 Comments Annealed at 600C for 2 weeks, slow cooling M.p. 933.5 K The structure has been assigned a PDF number (calculated powder diffraction data): 01-072-3440 The structure has been assigned a PDF number (experimental powder diffraction data): 4-787 Rietveld profile refinement applied Structure type : Cu X-ray diffraction (powder) No R value given in the paper. At least one temperature factor missing in the paper. Atom # OX SITE x y z SOF H Al 1 +0 4 a 0 0 0 1. 0 *end for ICSD #240129 |
12楼2010-11-02 09:16:18
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
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In
★ ★ ★ ★ ★
nash603(金币+5):谢谢猫哥帮忙！辛苦了！ 2010-10-27 19:30:24
ting110(金币+5):谢谢您的帮助！我是做晶体合成的，对晶体结构空间群不大了解，所以弱弱的问一句：这个有中文版本的吗？好多专业的词我不大懂。太不好意思啦！希望你能帮助我啊！ 2010-10-28 10:03:48
ting110(金币+1): 2010-10-28 10:05:32
nash603(金币+5):谢谢猫哥帮忙！辛苦了！ 2010-10-27 19:30:24
ting110(金币+5):谢谢您的帮助！我是做晶体合成的，对晶体结构空间群不大了解，所以弱弱的问一句：这个有中文版本的吗？好多专业的词我不大懂。太不好意思啦！希望你能帮助我啊！ 2010-10-28 10:03:48
ting110(金币+1): 2010-10-28 10:05:32
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*data for ICSD #171679 Coll Code 171679 Rec Date 2006/10/01 Chem Name Indium Structured In Sum In1 ANX N D(calc) 7.29 Title Structure of Ce2 Rh In8: an example of complementary use of high- resolution neutron powder diffraction and reciprocal-space mapping to study complex materials Author(s) Moshopoulou, E.G.;Ibberson, R.M.;Sarrao, J.L.;Thompson, J.D.;Fisk, Z. Reference Acta Crystallographica B (39,1983-) (2006), 62(2), 173-189 Unit Cell 3.25094(17) 3.25094(17) 4.9474(5) 90.0 90.0 90.0 Vol 52.28 Z 2 Space Group I 4/m m m SG Number 139 Cryst Sys tetragonal Pearson tI2 Wyckoff a Red Cell I 3.250 3.250 3.376 118.773 118.773 89.999 26.143 Trans Red 1.000 0.000 0.000 / 0.000 -1.000 0.000 / -0.500 0.500 -0.500 Comments Neutron diffraction (single crystal) Rietveld profile refinement applied Structure type : In Atom # OX SITE x y z SOF H In 1 +0 2 a 0.0 0.0 0.0 1.0 0 *end for ICSD #171679 |
2楼2010-10-27 12:43:02
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
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- 虫号: 664055
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- 专业: 敏感电子学与传感器
In2O3－I
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*data for ICSD #14388 Coll Code 14388 Rec Date 1980/01/01 Mod Date 2007/04/01 Chem Name Indium Oxide Structured In2 O3 Sum In2 O3 ANX A2X3 D(calc) 7.12 Title Refinement of the crystal structure of In2 O3 at two wavelengths Author(s) Marezio, M. Reference Acta Crystallographica (1,1948-23,1967) (1966), 20, 723-728 Unit Cell 10.117(1) 10.117(1) 10.117(1) 90. 90. 90. Vol 1035.51 Z 16 Space Group I a -3 SG Number 206 Cryst Sys cubic Pearson cI80 Wyckoff e d b R Value .033 Red Cell I 8.761 8.761 8.761 109.471 109.471 109.471 517.756 Trans Red 0.500 0.500 -0.500 / -0.500 0.500 0.500 / 0.500 -0.500 0.500 Comments Mo K-alpha-refinement The structure has been assigned a PDF number (calculated powder diffraction data): 01-071-2195 Structure type : Mn2O3 X-ray diffraction from single crystal Atom # OX SITE x y z SOF H ITF(B) In 1 +3 8 b 0.25 0.25 0.25 1. 0 0.46 In 2 +3 24 d 0.4663(1) 0 0.25 1. 0 0.41 O 1 -2 48 e 0.3912(12) 0.1558(11) 0.3796(13) 1. 0 0.45 *end for ICSD #14388 |
3楼2010-10-27 12:43:41
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
- 应助: 820 (博后)
- 贵宾: 0.902
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- 散金: 6682
- 红花: 141
- 沙发: 435
- 帖子: 126445
- 在线: 7408.7小时
- 虫号: 664055
- 注册: 2008-11-29
- 专业: 敏感电子学与传感器
In2O3－II
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*data for ICSD #16086 Coll Code 16086 Rec Date 1986/09/23 Mod Date 2000/07/15 Chem Name Indium Oxide - Ii Structured In2 O3 Sum In2 O3 ANX A2X3 D(calc) 7.31 Title The C rare earth oxide-corundum transition and crystal chemistry of oxides having the corundum structure Author(s) Prewitt, C.T.;Shannon, R.D.;Rogers, D.B.;Sleight, W.W. Reference Inorganic Chemistry (1969), 8, 1985-1993 Unit Cell 5.4870(3) 5.4870(3) 14.510(1) 90. 90. 120. Vol 378.33 Z 6 Space Group R -3 c H SG Number 167 Cryst Sys trigonal/rhombohedral Pearson hR10 Wyckoff e c R Value .022 Red Cell RH 5.487 5.487 5.781 61.672 61.672 60 126.109 Trans Red 1.000 0.000 0.000 / 1.000 1.000 0.000 / 0.667 0.333 0.333 Comments Cell of Ga2O3: 4.9791, 13.437; Fe2O3: 5.0351, 13.750 Cell of Ti2O3: 5.1572, 13.600; Tl2O3: 5.7468, 14.851 The structure has been assigned a PDF number (calculated powder diffraction data): 01-072-0683 The structure has been assigned a PDF number (experimental powder diffraction data): 22-336 Structure type : Al2O3 X-ray diffraction (powder) Unusual difference between calculated and measured density Atom # OX SITE x y z SOF H In 1 +3 12 c 0 0 0.35731(2) 1. 0 O 1 -2 18 e 0.2980(5) 0 0.25 1. 0 Lbl Type Beta11 Beta22 Beta33 Beta12 Beta13 Beta23 In1 In3+ 0.36(3) 0.36(3) 0.41(3) 0.18 0 0 O1 O2- 0.05(8) 0.09(9) 0.51(8) 0.05 0.11(6) 0.22 *end for ICSD #16086 [ Last edited by zbdfwq5777 on 2010-10-27 at 12:46 ] |
4楼2010-10-27 12:44:07