| 查看: 387 | 回复: 2 | |||
[交流]
【求助】晶体学报编辑提出的问题，该如何解决
|
|
1. As you can see from checkCIF your refinement has not properly converged: SHFSU01_ALERT_2_C The absolute value of parameter shift to su ratio > 0.05 Absolute value of the parameter shift to su ratio given 0.095 Additional refinement cycles may be required. Please carry out further refinement cycles. 2. Your refinement section MUST contain details of how ALL hydrogen atoms were refined. This includes a discussion of any bond distance restraints used. 3. The refinement section must also contain a discussion of the large residual peak. It must be discussed, e.g. stating its size and location of nearest non-H atom. It is probably not solvent! If it was, why didn't you include an extra water molecule in your model? 4. Your revised manuscript does not have a related literature section, it must do so. 5. The resolution of the new Figures which you sent to me seems quite poor. You can submit the PostScript output from XP without needing to convert to a TIF file. Actually, I think PostScript files are preferred. 6. The Abstract should also contain details of the hydrogen bonding. |
回复此楼» 猜你喜欢
在MOF中，有没有羧基参加配位的情况
已经有2人回复
-
招2026年入学上海交通大学博士生，急！！！
已经有1人回复
-
无机化学论文润色/翻译怎么收费?
已经有269人回复
-
理论计算合作
已经有0人回复
-
求高校合作
已经有1人回复
-
27级无机化学申博自荐
已经有2人回复
-
Chemdraw免费软件
已经有0人回复
-
单晶结构解析，各类疑难晶体数据处理和答疑
已经有38人回复
-
这个水相反应有没有催化剂促进发生
已经有4人回复
-
Mn Me3TACN
已经有5人回复
hjh509
铁杆木虫 (职业作家)
- CMEI: 1
- 应助: 46 (小学生)
- 金币: 7743.1
- 散金: 35
- 红花: 23
- 沙发: 120
- 帖子: 3915
- 在线: 327.5小时
- 虫号: 797728
- 注册: 2009-06-23
- 专业: 有机金属化学
2楼2010-10-21 19:06:19
3楼2010-10-23 21:09:20
