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【求助】投了篇晶体学报，审稿给提了几个问题，不知道怎么回答，在此请教一下高手
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1. This compound crystallizes in a chiral space group but no Flack parameter has been reported 2. In the cif file: _diffrn_measured_fraction_theta_max 0.964 _diffrn_reflns_theta_full 25.00 Some explanation should be made as to why the measured coverage is less that 0.97. 3. The fcf report indicates that 83 reflections were omitted between theta(min) to theta(max). Some explanation should be provided as to why there reflections were omitted. 5. For 5-coordinate complexes the tau-parameter has been used to indicate where the coordination geometry lies on the continuum between square pyramidal (C4v) and trigonal bipyramidal (D3h). The reference is: Addison, A. W., Rao, T. N., Reedijk, J., van Rijn, J. & Verschoor, G. C. (1984). J. Chem. Soc. Dalton Trans. pp. 1349-1356. The calculated values should included in the Abstract as well. |
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2楼2010-10-16 09:06:04
