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pangshaofeng06金虫 (小有名气)
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[交流]
麻烦能人帮我翻译一句话，谢谢。
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| Recrystallization of the resulting residue from pentane at -35 °C afforded analytically and spectroscopically pure 1-(N2)2. |
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yihua8808
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5楼2010-10-07 15:51:35
xiaomuyu2010
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2楼2010-10-07 14:44:18
pangshaofeng06
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我给你这一段文字，你从上下文，分析一下，因为你的翻译我还是不太理解。谢谢 Preparation of 1-(N2)2: Method 2. A 50 mL round-bottomed flask was charged with 0.102 g (0.15 mmol) of 1-Br2 and approximately 30 mL of diethyl ether. The resulting blue suspension was cooled to -35 °C in the drybox freezer. Via microsyringe, 0.293 mL (0.293 mmol) of a 1.0 M solution of NaBEt3H in toluene was added to the reaction flask. After being stirred under a N2 atmosphere at ambient temperature for 3 h, the green-purple solution was filtered through Celite, and the volatiles were removed from the filtrate in vacuo. Recrystallization of the resulting residue from pentane at -35 °C afforded analytically and spectroscopically pure 1-(N2)2. |
3楼2010-10-07 14:50:10
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4楼2010-10-07 15:30:12