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[交流] 【求助】求助羟基磷灰石晶体的XRD谱的标准卡（谢金币8个）已有1人参与

求助羟基磷灰石晶体的XRD谱的标准卡,包括Theta角度和d值，急啊，先谢谢了哦

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1楼 2010-09-29 16:11:09

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小木虫(金币+0.5):给个红包，谢谢回帖交流
americanyk(金币+2):Thank you 2010-09-29 09:43:54

PDF#09-0432: QM=Indexed; d=Guinier; I=Other/Unknown
Hydroxylapatite, syn
Ca5 ( P O4 )3 ( O H ) (pinkish red, pinkish-red, blue)
Radiation=CuKa1 Lambda=1.54056 Filter=
Calibration= d-Cutoff= I/Ic(RIR)=
Ref= de Wolff, P., Technisch Physische Dienst, Delft, The Netherlands.
ICDD Grant-in-Aid
Hexagonal - Powder Diffraction,  P63/m (176) Z=2 mp=
Cell=9.418x6.884 Pearson=hP44 (?)
Density(c)=3.160 Density(m)=3.080 Mwt=502.32 Vol=528.80 F(30)=54.6(.0157,35)
Ref= Ibid.

Strong Line: 2.81/X 2.78/6 2.72/6 3.44/4 1.84/4 1.94/3 2.63/3 2.26/2 1.81/2 1.72/2
NOTE:  See ICSD 22059 (PDF 01-073-0293; ICSD 22060 (PDF 01-073-0294); ICSD 24240 (PDF 01-073-1731); ICSD 26204 (PDF  01-074-0565); ICSD 26205 (PDF 01-074-566); ICSD 34457 (PDF 01-076-0694) and ICSD 203027 (PDF 01-084-1998).
I/I1 are peak values from a pattern which shows slight broadening of prism reflections.
Sample obtained following the procedure indicated by Hodge et al., Ind.
Eng.
Chem.
Anal.
Ed., 10 156 (1938).
Validated by calculated data 00-024-0033.
To replace 34-10.
d(A)    I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
8.1700 12.0 4.0 1 0 0      10.820 5.410 0.0612 0.7691
5.2600 6.0 3.0 1 0 1      16.841 8.421 0.0951 1.1945
4.7200 4.0 2.0 1 1 0      18.785 9.392 0.1059 1.3312
4.0700 10.0 7.0 2 0 0      21.819 10.909 0.1229 1.5438
3.8800 10.0 7.0 1 1 1      22.902 11.451 0.1289 1.6194
3.5100 2.0 2.0 2 0 1      25.354 12.677 0.1425 1.7901
3.4400 40.0 33.0 0 0 2      25.879 12.939 0.1453 1.8265
3.1700 12.0 11.0 1 0 2      28.126 14.063 0.1577 1.9821
3.0800 18.0 16.0 2 1 0      28.966 14.483 0.1623 2.0400
2.8140 100.0 100.0 2 1 1      31.773 15.886 0.1777 2.2328
2.7780 60.0 61.0 1 1 2      32.196 16.098 0.1800 2.2618
2.7200 60.0 62.0 3 0 0      32.902 16.451 0.1838 2.3100
2.6310 25.0 27.0 2 0 2      34.048 17.024 0.1900 2.3881
2.5280 6.0 7.0 3 0 1      35.480 17.740 0.1978 2.4854
2.2960 8.0 10.0 2 1 2      39.204 19.602 0.2178 2.7366
2.2620 20.0 25.0 3 1 0      39.818 19.909 0.2210 2.7777
2.2280 2.0 3.0 2 2 1      40.452 20.226 0.2244 2.8201
2.1480 10.0 13.0 3 1 1      42.029 21.014 0.2328 2.9251
2.1340 4.0 5.0 3 0 2      42.318 21.159 0.2343 2.9443
2.0650 8.0 11.0 1 1 3      43.804 21.902 0.2421 3.0427
2.0400 2.0 3.0 4 0 0      44.369 22.184 0.2451 3.0800
2.0000 6.0 8.0 2 0 3      45.305 22.652 0.2500 3.1416
1.9430 30.0 43.0 2 2 2      46.711 23.356 0.2573 3.2338
1.8900 16.0 24.0 3 1 2      48.103 24.051 0.2646 3.3244
1.8710 6.0 9.0 3 2 0      48.623 24.311 0.2672 3.3582
1.8410 40.0 61.0 2 1 3      49.468 24.734 0.2716 3.4129
1.8060 20.0 31.0 3 2 1      50.493 25.246 0.2769 3.4791
1.7800 12.0 19.0 4 1 0      51.283 25.642 0.2809 3.5299
1.7540 16.0 26.0 4 0 2      52.100 26.050 0.2851 3.5822
1.7220 20.0 33.0 0 0 4      53.143 26.572 0.2904 3.6488
1.6840 4.0 7.0 1 0 4      54.440 27.220 0.2969 3.7311
1.6440 10.0 17.0 3 2 2      55.879 27.940 0.3041 3.8219
1.6110 8.0 14.0 3 1 3      57.128 28.564 0.3104 3.9002
1.5870 4.0 7.0 5 0 1      58.073 29.037 0.3151 3.9592
1.5420 6.0 11.0 4 2 0      59.938 29.969 0.3243 4.0747
1.5300 6.0 11.0 3 3 1      60.457 30.229 0.3268 4.1067
1.5030 10.0 19.0 2 1 4      61.660 30.830 0.3327 4.1804
1.4740 12.0 23.0 5 0 2      63.011 31.505 0.3392 4.2627
1.4650 4.0 8.0 5 1 0      63.443 31.721 0.3413 4.2889
1.4520 13.0 25.0 3 2 3      64.078 32.039 0.3444 4.3273
1.4520 13.0 25.0 3 0 4      64.078 32.039 0.3444 4.3273
1.4330 9.0 18.0 5 1 1      65.031 32.516 0.3489 4.3846
1.4070 4.0 8.0 4 2 2      66.386 33.193 0.3554 4.4657
1.4070 4.0 8.0 4 1 3      66.386 33.193 0.3554 4.4657
1.3480 3.0 6.0 5 1 2      69.699 34.850 0.3709 4.6611
1.3160 5.0 11.0 4 0 4      71.651 35.826 0.3799 4.7745
1.3160 5.0 11.0 4 3 1      71.651 35.826 0.3799 4.7745
1.3060 4.0 9.0 2 0 5      72.286 36.143 0.3828 4.8110
1.3060 4.0 9.0 5 2 0      72.286 36.143 0.3828 4.8110
1.2800 7.0 15.0 4 2 3      73.995 36.998 0.3906 4.9087
1.2650 3.0 7.0 3 2 4      75.022 37.511 0.3953 4.9669
1.2650 3.0 7.0 6 0 2      75.022 37.511 0.3953 4.9669
1.2570 9.0 20.0 2 1 5      75.583 37.792 0.3978 4.9986
1.2490 1.0 2.0 4 3 2      76.154 38.077 0.4003 5.0306
1.2350 11.0 25.0 5 1 3      77.175 38.587 0.4049 5.0876
1.2210 9.0 21.0 5 2 2      78.227 39.114 0.4095 5.1459
这里有全部的2004的PDF卡http://d.namipan.com/d/3c3b31a62 ... 2fbb125e0ac93a7dc0a

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