| 查看: 697 | 回复: 2 | |||
| 本帖产生 1 个 翻译EPI ，点击这里进行查看 | |||
jiaxiaopen木虫 (小有名气)
|
[交流]
酬金求助摘要翻译
|
||
|
摘 要 以2-芳基吗啉为先导化合物，利用外消旋化合物2-氨基丙醇与α-溴-芳基烷基酮反应，合成了吗啉环上3,5位含二甲基的新型2-芳基吗啉类化合物3,5-二甲基-2-芳基吗啉，经干燥氯化氢酸化后得到其盐酸盐，总收率为63.7%，这在国内外从未见有过报道,本合成路线反应条件不苛刻，副反应少，反应溶剂可回收利用等特点，目标化合物结构也已经质谱和核磁测试技术确证。 麻烦虫友兄弟们帮忙翻译一下，在此谢过，祝各位虫友家庭幸福，工作顺利。。 |
回复此楼» 猜你喜欢
求个博导看看
已经有16人回复
-
上海工程技术大学张培磊教授团队招收博士生
已经有4人回复
-
上海工程技术大学【激光智能制造】课题组招收硕士
已经有5人回复
-
求助院士们，这个如何合成呀
已经有4人回复
-
临港实验室与上科大联培博士招生1名
已经有9人回复
-
需要合成515-64-0，50g，能接单的留言
已经有4人回复
-
自荐读博
已经有4人回复
-
写了一篇“相变储能技术在冷库中应用”的论文，论文内容以实验为主，投什么期刊合适？
已经有6人回复
-
带资进组求博导收留
已经有10人回复
-
最近几年招的学生写论文不引自己组发的文章
已经有11人回复
★ ★ ★ ★ ★
jiaxiaopen(金币+15, 翻译EPI+1):谢谢你的翻译。。。祝你工作顺利，万事如意 2010-07-12 16:16:13
cfk580713(金币+5):谢谢参与。 2010-11-30 17:23:11
jiaxiaopen(金币+15, 翻译EPI+1):谢谢你的翻译。。。祝你工作顺利，万事如意 2010-07-12 16:16:13
cfk580713(金币+5):谢谢参与。 2010-11-30 17:23:11
|
Abstract 3,5 - dimethyl -2 - aryl morpholine,as the new kind of 2-Arylmorpholine compounds containing 3,5-dimethyl in Morpholine ring ,was synthesized by racemic compound 2-amino-propanol ,α-bromo - aryl alkyl ketones and 2 - Arylmorpholine as Lead compound.Then its hydrochloride salt was obtained by acidification by dry hydrogen chloride ,the overall yield was 63.7%.This has never been reported at home and abroad , the synthetic reaction condition is not harsh with few side effects, recyclable solvent characteristics such as .The structure of the target compound has been confirmed by MS and NMR . |
2楼2010-07-12 11:28:09
|
Abstract 3,5 - dimethyl -2 - aryl morpholine,as the new kind of 2-Arylmorpholine compounds containing 3,5-dimethyl in Morpholine ring ,was synthesized by racemic compound 2-amino-propanol ,α-bromo - aryl alkyl ketones and 2 - Arylmorpholine as Lead compound.Then its hydrochloride salt was obtained by acidification by dry hydrogen chloride ,the overall yield was 63.7%.This has never been reported at home and abroad , the synthetic reaction condition is not harsh with few side effects, besides the solvent is recyclable.The structure of the target compound has been confirmed by MS and NMR . |
3楼2010-07-12 11:32:18