[交流] 【求助】求助PDF卡片已有3人参与

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1楼2010-05-26 10:41:50

碧水云天

至尊木虫 (著名写手)

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yehuimei(金币+1): 2010-05-30 10:06:56
wsht212:谢谢交流，希望常来！ 2010-05-30 11:10:30

X1、X2代表啥意思？？ PDF ：21-1458、21-1461

2楼2010-05-26 10:50:22

zbdfwq5777

木虫之王 (文学泰斗)

至尊山羊

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★ ★
yehuimei(金币+1): 2010-05-30 10:07:14
wsht212(金币+2):谢谢交流，希望常来！ 2010-05-30 11:10:41

Card Information
Names: Yttrium Silicate
Formula: Y2 Si O5
PDF Number: 36-1476
Quality: star
Subfiles: inorganic NBS CP

Cell and Symmetry Information
System: monoclinic Space Group: I*/a    (no.  15)
a: 12.5013 b: 6.7282 c: 10.4217
b: 102.682
Z: 8

Instrument Information
Radiation: CuKa1 Wavelength: 1.5405981 Filter: Graph
Instrument(d): diffractometer Cut Off: 17.7 Standard: Ag  FP
Instrument(I): diffractometer I type: peak heights

Comments and Additional Information
Preparation: The sample was made by heating a 1:1 molar mixture of Y2 O3 and Si O2 to 1500 C for 48 hours.
Structure: The structure of Y2 Si O5 has been determined by Harris, L., Finch, C.,  Am. Mineral., 50  1493 (1965).
Colour: Colorless
Temperature: The mean temperature of data collection was 25.1 C.

Literature References
General: McMurdie, H., Morris, M., Evans, E.,Paretzkin, B., Wong-Ng, W., Hubbard, C. Powder Diffraction 1 99 (1986)

PeakList
   h    k    l    d    I
   2    0    0 6.1030    19
   1    1    0 5.8972    24
   0    0    2 5.0896    1
-2    0    2 4.4081    2
-1    1    2 4.0701    11
   2    1    1 3.9004    73
   1    1    2 3.6620    13
   2    0    2 3.5414    70
   3    1    0 3.4809    1
   0    2    0 3.3652    10
-1    2    1 3.1444    75
   0    1    3 3.0278    81
   2    2    0 2.9463    55
-4    0    2 2.9120    100
   0    2    2 2.8060    9
-2    2    2 2.6755    20
   3    1    2 2.6499    9
-3    2    1 2.6001    17
   4    1    1 2.5529    51
   2    1    3 2.5205    3
   3    2    1 2.4307    26
-1    2    3 2.4150    13
-5    1    2 2.2738    28
   4    2    0 2.2600    11
   1    1    4 2.2491    11
-4    2    2 2.2015    42
   0    3    1 2.1904    46
   2    0    4 2.1830    48
-6    0    2 2.0483    9
   6    0    0 2.0318    17
-5    2    1 2.0065    4
-6    1    1 1.9905    15
   3    3    0 1.9637    11
   0    1    5 1.9465    11
   3    2    3 1.9320    4
-5    1    4 1.9097    4
   3    1    4 1.8903    10
-5    2    3 1.8556    24
-4    2    4 1.8438    9
   2    2    4 1.8307    17
-4    1    5 1.8234    27
-4    3    1 1.8196    23
   3    3    2 1.7699    8
   6    0    2 1.7589    18
-6    2    2 1.7503    25
   2    3    3 1.7301    39
-3    2    5 1.7204    9
-1    3    4 1.7000    6
   7    1    0 1.6872    15
   1    2    5 1.6790    13
-3    1    6 1.6504    6
-4    0    6 1.6425    7
   2    4    0 1.6213    10
   0    4    2 1.5968    12
   1    1    6 1.5841    12
-6    2    4 1.5810    18
-7    2    1 1.5758    20
-2    4    2 1.5715    16
-7    1    4 1.5671    14
-5    2    5 1.5627    12
   6    1    3 1.5523    11

3楼2010-05-26 11:03:20

yehuimei

木虫 (小有名气)

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Y2SiO5有X1和X2两种晶型，具体求助PDF 41-4和21-1456

赞一下

4楼2010-05-26 11:03:23

zbdfwq5777

木虫之王 (文学泰斗)

至尊山羊

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41-4

★
yehuimei(金币+2): 2010-05-30 10:07:26
wsht212(金币+1):谢谢交流，希望常来！ 2010-05-30 11:10:58

Card Information
Names: Yttrium Silicate
Formula: Y2 Si O5
PDF Number: 41-4
Quality: unknown
Subfiles: inorganic

Cell and Symmetry Information
System: monoclinic Space Group: P21/c (no.  14)
a: 9.012 b: 6.979 c: 6.630
b: 106.7

Instrument Information
Radiation: CuKa Wavelength: 1.5418    Filter: Ni
Instrument(d): unknown
Instrument(I): diffractometer I type: unknown

Comments and Additional Information
Colour: Colorless
General: 1050 C in air, X#1 phase.
Pattern: To replace 21-1456.

Literature References
General: Ito, Johnson. Private Communication          ( )
Powder: Ito, Johnson. Am. Mineral. 53  1940 (1968)
Unit Cell: Liddell, K., Thompson, D. Trans. J. Br. Ceram. Soc. 85 17 (1986)

PeakList
   h    k    l    d    I
   1    1    0 5.4000    20
   0    1    1 4.6800    6
   2    0    0 4.3300    10
   1    1    1 3.8000    8
   2    1    0 3.6600    6
   2    1 -1 3.5800    10
   1    0 -2 3.3200    8
   0    2    1 3.0500    80
   1    2 -1 3.0200    100
   0    1    2 2.8840    60
   3    0    0 2.8840    60
   2    1 -2 2.7530    80
   1    0    2 2.7530    80
   3    1    0 2.6650    50
   3    0 -2 2.5060    6
   -    -    - 2.3080    6
-2    2    2 2.2910    6
   3    2 -1 2.2540    6
   4    0    0 2.1590    8
   4    0 -2 2.0880    16
   2    1 -3 2.0700    20
   3    2    1 1.9630    25
   1    2 -3 1.8650    50
   3    3 -1 1.8240    10
   3    1    2 1.8140    10
   3    2 -3 1.7350    10
   5    1 -2 1.6940    10

[ Last edited by zbdfwq5777 on 2010-5-26 at 11:05 ]

5楼2010-05-26 11:04:40

zbdfwq5777

木虫之王 (文学泰斗)

至尊山羊

CMEI: 3
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21-1456

★
yehuimei(金币+2): 2010-05-30 10:07:34
wsht212(金币+1):谢谢交流，希望常来！ 2010-05-30 11:11:06

Card Information
Names: Yttrium Silicate
Formula: Y2 Si O5
PDF Number: 21-1456
Quality: unknown
Subfiles: inorganic

Cell and Symmetry Information
System: unknown

Instrument Information
Radiation: CuKa Wavelength: 1.5418    Filter: Ni
Instrument(d): unknown
Instrument(I): diffractometer I type: unknown

Comments and Additional Information
Colour: Colorless
General: 1050 C in air, X#1 phase.
Deleted by: Deleted by 41-4.

Literature References
General: Ito, Johnson. Private Communication          ( )
Powder: Ito, Johnson. Am. Mineral. 53  1940 (1968)

PeakList
   h    k    l    d    I
   -    -    - 5.4000    20
   -    -    - 4.6800    6
   -    -    - 4.3300    10
   -    -    - 3.8000    8
   -    -    - 3.6600    6
   -    -    - 3.5800    10
   -    -    - 3.3200    8
   -    -    - 3.0500    80
   -    -    - 3.0200    100
   -    -    - 2.8840    60
   -    -    - 2.7530    80
   -    -    - 2.6650    50
   -    -    - 2.5060    6
   -    -    - 2.3080    6
   -    -    - 2.2910    6
   -    -    - 2.2540    6
   -    -    - 2.1590    8
   -    -    - 2.0880    16
   -    -    - 2.0700    20
   -    -    - 1.9630    25
   -    -    - 1.8650    50
   -    -    - 1.8240    10
   -    -    - 1.8140    10
   -    -    - 1.7350    10
   -    -    - 1.6940    10
   -    -    - 1.6550    10
   -    -    - 1.5940    20

6楼2010-05-26 11:05:37