| 查看: 888 | 回复: 4 | |||
| 当前主题已经存档。 | |||
| 【有奖交流】积极回复本帖子，参与交流，就有机会分得作者 navypang 的 15 个金币 | |||
[交流]
【交流】请高手帮我看看审稿意见中的一句话 已有2人参与
|
|||
|
请高手帮我看看审稿意见中的一句话（如下），这句话是什么意思？我该如何解决？不胜感激！ The bond distances and errors presented are in some cases not chemically reasonable/excessively large. 附该晶体的checkcif报告 Alert level B PLAT241_ALERT_2_B Check High Ueq as Compared to Neighbors for C7 PLAT241_ALERT_2_B Check High Ueq as Compared to Neighbors for O9 PLAT241_ALERT_2_B Check High Ueq as Compared to Neighbors for O20 PLAT241_ALERT_2_B Check High Ueq as Compared to Neighbors for O21 PLAT242_ALERT_2_B Check Low Ueq as Compared to Neighbors for N1 PLAT342_ALERT_3_B Low Bond Precision on C-C Bonds (x 1000) Ang .. 38 PLAT410_ALERT_2_B Short Intra H...H Contact H14A .. H16A .. 1.86 Ang. PLAT234_ALERT_4_B Large Hirshfeld Difference C4 -- C7 .. 0.26 Ang. Alert level C PLAT026_ALERT_3_C Ratio Observed / Unique Reflections too Low .... 45 Perc. PLAT094_ALERT_2_C Ratio of Maximum / Minimum Residual Density .... 3.57 PLAT220_ALERT_2_C Large Non-Solvent O Ueq(max)/Ueq(min) ... 3.13 Ratio PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C10 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C11 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for C13 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O8 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O14 PLAT241_ALERT_2_C Check High Ueq as Compared to Neighbors for O16 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for N2 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for C4 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for W2 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for W3 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for W4 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for W5 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for W6 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for O6 PLAT242_ALERT_2_C Check Low Ueq as Compared to Neighbors for O13 PLAT362_ALERT_2_C Short C(sp3)-C(sp2) Bond C4 - C7 ... 1.37 Ang. PLAT362_ALERT_2_C Short C(sp3)-C(sp2) Bond C9 - C18 ... 1.35 Ang. PLAT410_ALERT_2_C Short Intra H...H Contact H9B .. H13A .. 1.93 Ang. PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ ? PLAT043_ALERT_1_C Check Reported Molecular Weight ................ 7362.04 PLAT068_ALERT_1_C Reported F000 Differs from Calcd (or Missing)... ? PLAT120_ALERT_1_C Reported SPGR ? Inconsistent with Explicit Pnnn PLAT147_ALERT_1_C su on Symmetry Constrained Cell Angle(s) ....... ? PLAT153_ALERT_1_C The su's on the Cell Axes are Equal (x 100000) 500 Ang. PLAT194_ALERT_1_C Missing _cell_measurement_reflns_used datum .... ? PLAT195_ALERT_1_C Missing _cell_measurement_theta_max datum .... ? PLAT196_ALERT_1_C Missing _cell_measurement_theta_min datum .... ? PLAT731_ALERT_1_C Bond Calc 1.82(2), Rep 1.82(5) ...... 2.50 su-Ra CU2 -N2 1.555 5.756 PLAT751_ALERT_4_C Bond Calc 1.34821, Rep 1.348(15) ...... Senseless su N1 -C10 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.34785, Rep 1.348(15) ...... Senseless su N1 -C12 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.34792, Rep 1.347(15) ...... Senseless su C10 -C11 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.34271, Rep 1.348(15) ...... Senseless su C11 -N2 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.35352, Rep 1.347(15) ...... Senseless su N2 -C12 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.41120, Rep 1.412(12) ...... Senseless su C15 -C15 1.555 3.556 PLAT751_ALERT_4_C Bond Calc 1.36911, Rep 1.369(17) ...... Senseless su N3 -C19 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.36953, Rep 1.369(17) ...... Senseless su N3 -C21 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.36935, Rep 1.369(17) ...... Senseless su C19 -N4 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.36842, Rep 1.368(17) ...... Senseless su N4 -C20 1.555 1.555 PLAT751_ALERT_4_C Bond Calc 1.36073, Rep 1.369(17) ...... Senseless su |
回复此楼» 猜你喜欢
MIL-101有单晶样品吗
已经有1人回复
-
已删除
已经有3人回复
-
无机化学论文润色/翻译怎么收费?
已经有222人回复
-
收调剂研究生
已经有2人回复
-
【2026 考研调剂】哈尔滨工程大学核科学与技术学院核化工系 招收调剂生
已经有3人回复
-
【2026 考研调剂】哈尔滨工程大学核科学与技术学院核化工系 招收调剂生
已经有1人回复
-
广州大学环境大分子材料研究所2026年研究生招生简章
已经有0人回复
-
武汉纺织大学技术研究院招收化学、生物、材料、纺织、机械等专业调剂生
已经有0人回复
-
台州学院有序多孔材料团队化学、材料与化工硕士招生，请速联系！
已经有0人回复
-
首都师范大学化学系田洋课题组专硕招调剂生
已经有4人回复
fmopily
铁杆木虫 (正式写手)
- 应助: 65 (初中生)
- 金币: 8223.1
- 散金: 34
- 红花: 11
- 帖子: 941
- 在线: 327.1小时
- 虫号: 484100
- 注册: 2007-12-26
- 专业: 配位化学
2楼2010-04-13 20:00:33
fmopily
铁杆木虫 (正式写手)
- 应助: 65 (初中生)
- 金币: 8223.1
- 散金: 34
- 红花: 11
- 帖子: 941
- 在线: 327.1小时
- 虫号: 484100
- 注册: 2007-12-26
- 专业: 配位化学
3楼2010-04-13 20:13:06
yeqs1
铁杆木虫 (职业作家)
- 应助: 3 (幼儿园)
- 贵宾: 0.21
- 金币: 9461.3
- 散金: 250
- 红花: 2
- 帖子: 4642
- 在线: 646.1小时
- 虫号: 304423
- 注册: 2006-12-09
- 专业: 配位化学
4楼2010-04-14 14:46:50
fmopily
铁杆木虫 (正式写手)
- 应助: 65 (初中生)
- 金币: 8223.1
- 散金: 34
- 红花: 11
- 帖子: 941
- 在线: 327.1小时
- 虫号: 484100
- 注册: 2007-12-26
- 专业: 配位化学
5楼2010-04-14 20:27:47
10