| 查看: 1118 | 回复: 8 | ||
| 当前主题已经存档。 | ||
materyang至尊木虫 (文坛精英)
|
[交流]
【求助】求助Mg和MgZn2的pdf卡片
|
|
|
哪位高手能给出Mg和MgZn2的pdf卡片,就是能够有晶体结构进行衍射标定的 愿意用20金币作为酬谢 再加上Mg2Zn11,MgO,Al2Mg,再加上45个金币 [ Last edited by materyang on 2010-3-18 at 16:04 ] |
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
- 应助: 820 (博后)
- 贵宾: 0.902
- 金币: 166542
- 散金: 6682
- 红花: 141
- 沙发: 435
- 帖子: 126445
- 在线: 7408.7小时
- 虫号: 664055
- 注册: 2008-11-29
- 专业: 敏感电子学与传感器
materyang(金币+10):3Q 2010-03-18 12:43
|
Mg: Card Information Names: Magnesium Formula: Mg PDF Number: 35-821 Quality: star Subfiles: inorganic alloy NBS CP FOR EDU EXP Cell and Symmetry Information System: hexagonal Space Group: P63/mmc (no. 194) a: 3.20936 c: 5.2112 Z: 2 Instrument Information Radiation: CuKa1 Wavelength: 1.5405981 Filter: Graph Instrument(d): diffractometer Cut Off: 17.7 Standard: W Instrument(I): diffractometer I type: peak heights Comments and Additional Information Source: The sample was obtained from Fisher Scientific Company, Fair Lawn, NJ, USA. It contained a small amount of Mg ( O H )2. Colour: Dark gray Temperature: The temperature of data collection was approximately 25.0 C. Pattern: To replace 4-770. General: Pyrotechnic. Literature References General: Natl. Bur. Stand. (U.S.) Monogr. 25 21 82 (1984) Structure: Jevins, A. et al. Z. Phys. Chem. (B) 40 347 (1938) PeakList h k l d I 1 0 0 2.7782 25 0 0 2 2.6050 36 1 0 1 2.4520 100 1 0 2 1.9002 15 1 1 0 1.6047 12 1 0 3 1.4730 16 2 0 0 1.3899 2 1 1 2 1.3664 13 2 0 1 1.3430 8 0 0 4 1.3028 2 2 0 2 1.2264 2 1 0 4 1.1797 2 2 0 3 1.0854 3 2 1 0 1.0506 1 2 1 1 1.0299 4 1 1 4 1.0116 3 1 0 5 0.9760 2 2 1 2 0.9742 2 2 0 4 0.9505 1 3 0 0 0.9266 1 2 1 3 0.8988 2 3 0 2 0.8729 1 2 0 5 0.8338 1 1 0 6 0.8289 1 2 1 4 0.8178 1 3 0 3 0.8174 1 2 2 0 0.8023 1 |
2楼2010-03-18 12:31:09
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
- 应助: 820 (博后)
- 贵宾: 0.902
- 金币: 166542
- 散金: 6682
- 红花: 141
- 沙发: 435
- 帖子: 126445
- 在线: 7408.7小时
- 虫号: 664055
- 注册: 2008-11-29
- 专业: 敏感电子学与传感器
materyang(金币+10): 2010-03-18 12:44
|
MgZn2: Card Information Names: Magnesium Zinc Formula: Mg Zn2 PDF Number: 77-1177 Quality: calculated Subfiles: inorganic alloy MAP COR Cell and Symmetry Information System: hexagonal Space Group: P63/mmc (no. 194) a: 5.23300 c: 8.56600 Density (Dm): 5.090 Density (Dx): 5.069 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.54060 Instrument(d): calculated Cut Off: 17.7 Instrument(I): calculated I type: peak heights I/Icor: 3.43 Comments and Additional Information ICSD Number: 046006 Temperature factor: ATF Literature References General: Calculated from ICSD using POWD-12++ (1997) Structure: Ohba, T., Kitano, Y., Komura, Y. Acta Crystallogr., Sec. C, 40 1 (1984) PeakList h k l d I 1 0 0 4.5319 591 0 0 2 4.2830 323 1 0 1 4.0058 315 1 0 2 3.1128 32 1 1 0 2.6165 63 1 0 3 2.4158 397 2 0 0 2.2660 60 1 1 2 2.2328 863 2 0 1 2.1906 999 0 0 4 2.1415 300 2 0 2 2.0029 434 1 0 4 1.9362 164 2 0 3 1.7750 213 2 1 0 1.7129 142 2 1 1 1.6796 24 1 0 5 1.6025 2 2 1 2 1.5904 1 2 0 4 1.5564 7 3 0 0 1.5106 9 3 0 1 1.4877 1 2 1 3 1.4689 99 0 0 6 1.4277 30 3 0 2 1.4246 141 2 0 5 1.3666 180 2 1 4 1.3376 84 3 0 3 1.3353 44 2 2 0 1.3082 161 3 1 0 1.2569 26 1 1 6 1.2532 35 2 2 2 1.2512 30 3 1 1 1.2436 11 2 0 6 1.2079 76 1 0 7 1.1814 11 3 1 3 1.1504 39 3 0 5 1.1330 4 4 0 0 1.1330 4 4 0 1 1.1232 57 2 2 4 1.1164 105 2 1 6 1.0967 9 4 0 2 1.0953 30 |
3楼2010-03-18 12:32:20
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
- 应助: 820 (博后)
- 贵宾: 0.902
- 金币: 166542
- 散金: 6682
- 红花: 141
- 沙发: 435
- 帖子: 126445
- 在线: 7408.7小时
- 虫号: 664055
- 注册: 2008-11-29
- 专业: 敏感电子学与传感器
4楼2010-03-18 12:36:34
materyang
至尊木虫 (文坛精英)
- 应助: 7 (幼儿园)
- 金币: 44565.9
- 红花: 3
- 帖子: 23438
- 在线: 763小时
- 虫号: 776702
- 注册: 2009-05-22
- 专业: 元素化学
5楼2010-03-18 20:11:44
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
- 应助: 820 (博后)
- 贵宾: 0.902
- 金币: 166542
- 散金: 6682
- 红花: 141
- 沙发: 435
- 帖子: 126445
- 在线: 7408.7小时
- 虫号: 664055
- 注册: 2008-11-29
- 专业: 敏感电子学与传感器
★
小木虫(金币+0.5):给个红包,谢谢回帖交流
materyang(金币+15):3Q 2010-03-19 11:55
小木虫(金币+0.5):给个红包,谢谢回帖交流
materyang(金币+15):3Q 2010-03-19 11:55
|
Mg2Zn11 Card Information Names: Magnesium Zinc Formula: Mg2 Zn11 PDF Number: 6-664 Quality: unknown Subfiles: inorganic alloy Cell and Symmetry Information System: cubic Space Group: Pm3 (no. 200) a: 8.552 Density (Dm): 6.160 Density (Dx): 6.110 Z: 3 Instrument Information Radiation: CuKa Wavelength: 1.542 Instrument(d): unknown Instrument(I): visual estimate I type: unknown Comments and Additional Information Preparation: Sample prepared by melting Mg and Zn in an evacuated system at 700 C, then annealing at 350 C for 3 weeks. Literature References General: Samson. Acta Chem. Scand. 3 835 (1949) PeakList h k l d I 1 1 0 6.0300 65 1 1 1 4.9500 45 2 0 0 4.2600 40 2 1 0 3.8400 60 2 1 1 3.5000 40 3 0 0 2.8500 45 3 1 0 2.7000 40 3 1 1 2.5800 40 2 2 2 2.4700 75 3 2 0 2.3700 75 3 2 1 2.2900 85 4 0 0 2.1400 80 4 1 0 2.0700 100 3 3 0 2.0100 60 4 2 0 1.9120 65 4 2 1 1.8650 60 4 3 0 1.7100 45 5 1 0 1.6750 20 5 2 0 1.5860 20 5 2 1 1.5690 15 4 4 0 1.5120 45 4 4 1 1.4900 20 5 3 0 1.4650 10 6 0 0 1.4240 55 6 1 0 1.4090 10 6 1 1 1.3860 65 6 2 0 1.3520 20 5 4 0 1.3350 55 5 4 1 1.3190 45 6 2 2 1.2890 35 |
6楼2010-03-19 09:28:52
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
- 应助: 820 (博后)
- 贵宾: 0.902
- 金币: 166542
- 散金: 6682
- 红花: 141
- 沙发: 435
- 帖子: 126445
- 在线: 7408.7小时
- 虫号: 664055
- 注册: 2008-11-29
- 专业: 敏感电子学与传感器
materyang(金币+15):3q 2010-03-19 11:55
|
Al2Mg Card Information Names: Aluminum Magnesium Formula: Al2 Mg PDF Number: 34-1035 Quality: unknown Subfiles: inorganic alloy Cell and Symmetry Information System: tetragonal Space Group: I41/amd (no. 141) a: 4.132 c: 26.602 Density (Dx): 2.290 Z: 8 Instrument Information Radiation: CuKa Wavelength: 1.54178 Filter: Ni Instrument(d): Debye-Scherrer Standard: Si Instrument(I): visual estimate I type: unknown Comments and Additional Information Preparation: Prepared from 99.99% pure metals by melting together, casting, hot working and homogenization for 20 hours at 350 C, followed by liquisol quenching. Literature References General: Suryanarayana, C. et al. Z. Metallkd. 69 155 (1978) PeakList h k l d I 1 0 5 3.2500 60 1 1 6 2.4400 80 - - - 2.1400 20 0 2 0 2.0660 100 0 2 4 1.9610 20 1 1 10 1.9610 20 2 2 0 1.4610 90 1 1 18 1.3220 60 1 2 15 1.2780 20 2 3 15 0.9630 10 3 3 6 0.9490 10 1 4 9 0.9490 10 4 0 18 0.8460 40 1 5 6 0.7970 20 |
7楼2010-03-19 09:30:52
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
- 应助: 820 (博后)
- 贵宾: 0.902
- 金币: 166542
- 散金: 6682
- 红花: 141
- 沙发: 435
- 帖子: 126445
- 在线: 7408.7小时
- 虫号: 664055
- 注册: 2008-11-29
- 专业: 敏感电子学与传感器
materyang(金币+15):非常感谢您的帮助 2010-03-19 11:55
|
MgO Card Information Names: Magnesium Oxide Periclase, syn Formula: Mg O PDF Number: 45-946 Quality: star Subfiles: inorganic mineral alloy COR EDU CP FOR CEM Cell and Symmetry Information System: cubic Space Group: Fm3m (no. 225) a: 4.2112 Density (Dm): 3.560 Z: 4 Instrument Information Radiation: CuKa1 Wavelength: 1.5405981 Filter: Ge Instrument(d): diffractometer Standard: Si Instrument(I): diffractometer I type: integrated intensities I/Icor: 1.0 Comments and Additional Information Preparation: MgO (Heraeus, 99.99 %) annealed in open Au crucible at 800 C for 1 week. Colour: Colorless Pattern: To replace 4-829. General: Validated by calculated pattern 43-1022. Literature References General: Kern, A., Doetzer, R., Eysel, W.,Mineralogisch-Petrographisches Inst.,Univ. Heidelberg, Germany. ICDD Grant-in-Aid (1993) Optical: Winchell, Winchell. Elements of Optical Mineralogy 57 (1964) Structure: Moscow University Geology Bulletin 47 80 (1992) PeakList h k l d I 1 1 1 2.4316 4 2 0 0 2.1056 100 2 2 0 1.4891 39 3 1 1 1.2698 5 2 2 2 1.2158 10 4 0 0 1.0528 8 3 3 1 0.9662 2 4 2 0 0.9417 19 4 2 2 0.8597 14 5 1 1 0.8105 4 |
8楼2010-03-19 09:32:29
zbdfwq5777
木虫之王 (文学泰斗)
至尊山羊
- CMEI: 3
- 应助: 820 (博后)
- 贵宾: 0.902
- 金币: 166542
- 散金: 6682
- 红花: 141
- 沙发: 435
- 帖子: 126445
- 在线: 7408.7小时
- 虫号: 664055
- 注册: 2008-11-29
- 专业: 敏感电子学与传感器
★
小木虫(金币+0.5):给个红包,谢谢回帖交流
小木虫(金币+0.5):给个红包,谢谢回帖交流
9楼2010-03-19 09:34:27













回复此楼