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chukaiyan(金币+5,VIP+0): 12-4 19:02
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PDF#12-0017: QM=Star/Calculated; d=Other/Unknown; I=(Unknown) Magnesium Sulfate MgSO4 Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= d-Cutoff= I/Ic(RIR)= Ref= Level-1 PDF Orthorhombic, Cmcm(63) Z=4 mp= Cell=5.181x7.885x6.501<90x90x90> Pearson= Density(c)=2.93 Density(m)= Mwt= Vol= Ref= Ibid. Strong Line: 3.61/X 2.60/8 3.38/6 1.41/3 2.35/3 1.63/2 1.80/2 2.03/2 d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 3.6070 100.0 90.0 1 1 1 24.661 12.331 0.1386 1.7419 3.3780 55.0 53.0 0 2 1 26.362 13.181 0.1480 1.8600 3.2540 2.0 2.0 0 0 2 27.386 13.693 0.1537 1.9309 2.5990 80.0 100.0 1 1 2 34.480 17.240 0.1924 2.4175 2.5100 6.0 8.0 0 2 2 35.743 17.872 0.1992 2.5033 2.3460 30.0 42.0 1 3 0 38.336 19.168 0.2131 2.6783 2.1660 15.0 22.0 2 2 0 41.663 20.832 0.2308 2.9008 2.0550 4.0 6.0 2 2 1 44.028 22.014 0.2433 3.0575 2.0260 15.0 24.0 2 0 2 44.692 22.346 0.2468 3.1013 1.9710 8.0 13.0 0 4 0 46.009 23.005 0.2537 3.1878 1.9000 10.0 17.0 0 2 3 47.834 23.917 0.2632 3.3069 1.8020 15.0 27.0 2 2 2 50.613 25.306 0.2775 3.4868 1.6850 13.0 25.0 0 4 2 54.405 27.203 0.2967 3.7289 1.6300 20.0 40.0 3 1 1 56.402 28.201 0.3067 3.8547 1.5920 10.0 20.0 1 3 3 57.874 28.937 0.3141 3.9467 1.5300 10.0 21.0 2 2 3 60.457 30.229 0.3268 4.1067 1.4970 12.0 26.0 3 1 2 61.935 30.967 0.3340 4.1972 1.4690 2.0 4.0 1 5 1 63.250 31.625 0.3404 4.2772 1.4430 8.0 18.0 3 3 0 64.526 32.263 0.3465 4.3543 1.4130 30.0 69.0 2 4 2 66.068 33.034 0.3539 4.4467 1.3690 2.0 5.0 1 5 2 68.480 34.240 0.3652 4.5896 1.3320 10.0 24.0 3 1 3 70.660 35.330 0.3754 4.7171 1.2950 8.0 20.0 4 0 0 72.998 36.499 0.3861 4.8519 1.2710 2.0 5.0 2 4 3 74.608 37.304 0.3934 4.9435 1.2450 6.0 16.0 1 1 5 76.442 38.221 0.4016 5.0467 1.2380 8.0 21.0 1 5 3 76.954 38.477 0.4039 5.0753 1.2090 4.0 11.0 4 2 1 79.155 39.578 0.4136 5.1970 1.1530 6.0 17.0 2 6 1 83.836 41.918 0.4337 5.4494 1.1460 2.0 6.0 3 5 1 84.466 42.233 0.4363 5.4827 1.0790 6.0 18.0 3 3 4 91.103 45.552 0.4634 5.8232 1.0700 4.0 12.0 4 2 3 92.090 46.045 0.4673 5.8721 1.0510 4.0 12.0 1 1 6 94.260 47.130 0.4757 5.9783 1.0420 4.0 12.0 1 7 2 95.332 47.666 0.4798 6.0299 1.0260 10.0 32.0 3 5 3 97.313 48.656 0.4873 6.1240 1.0100 4.0 13.0 4 0 4 99.397 49.699 0.4950 6.2210 PDF#21-0546: QM=Intermediate; d=Other/Unknown; I=(Unknown) Magnesium Sulfate MgSO4 Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= d-Cutoff= I/Ic(RIR)= Ref= Level-1 PDF Orthorhombic, Pbnm(62) Z=4 mp= Cell=4.75x8.59x6.71<90x90x90> Pearson= Density(c)=2.93 Density(m)= Mwt= Vol= Ref= Ibid. Strong Line: 3.53/X 3.61/7 4.15/3 2.64/3 3.35/2 2.45/2 3.18/2 2.61/2 d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 4.1500 30.0 26.0 1 1 0 21.393 10.697 0.1205 1.5140 3.8700 10.0 9.0 1 0 1 22.962 11.481 0.1292 1.6236 3.6100 70.0 68.0 0 2 1 24.640 12.320 0.1385 1.7405 3.5300 100.0 100.0 1 1 1 25.208 12.604 0.1416 1.7799 3.3500 18.0 19.0 0 0 2 26.586 13.293 0.1493 1.8756 3.1800 16.0 18.0 1 2 0 28.036 14.018 0.1572 1.9758 2.8730 4.0 5.0 1 2 1 31.104 15.552 0.1740 2.1870 2.6390 25.0 33.0 0 2 2 33.941 16.971 0.1895 2.3809 2.6050 16.0 22.0 1 1 2 34.398 17.199 0.1919 2.4120 2.4480 18.0 26.0 1 3 0 36.680 18.340 0.2042 2.5667 2.3710 10.0 15.0 2 0 0 37.916 18.958 0.2109 2.6500 2.3050 16.0 25.0 1 3 1 39.045 19.523 0.2169 2.7259 2.2860 12.0 19.0 2 1 0 39.383 19.691 0.2187 2.7486 2.1630 6.0 10.0 2 1 1 41.724 20.862 0.2312 2.9048 2.1440 4.0 7.0 0 4 0 42.111 21.056 0.2332 2.9306 2.0420 8.0 14.0 0 4 1 44.323 22.161 0.2449 3.0770 2.0180 6.0 10.0 1 0 3 44.879 22.439 0.2478 3.1136 1.9810 4.0 7.0 0 2 3 45.764 22.882 0.2524 3.1717 1.9760 4.0 7.0 1 3 2 45.886 22.943 0.2530 3.1797 1.9650 8.0 14.0 1 1 3 46.158 23.079 0.2545 3.1976 1.9340 4.0 7.0 2 0 2 46.942 23.471 0.2585 3.2488 1.8250 4.0 8.0 2 3 0 49.931 24.965 0.2740 3.4428 1.8050 8.0 16.0 0 4 2 50.523 25.261 0.2770 3.4810 1.7630 16.0 32.0 2 3 1 51.814 25.907 0.2836 3.5639 1.6730 10.0 21.0 0 0 4 54.828 27.414 0.2989 3.7556 1.6490 4.0 9.0 1 3 3 55.695 27.847 0.3032 3.8103 1.6020 4.0 9.0 2 1 3 57.478 28.739 0.3121 3.9221 PDF#17-0935: QM=Doubtful(?); d=Other/Unknown; I=(Unknown) Tin Sulfate SnSO4 Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= d-Cutoff= I/Ic(RIR)= Ref= Level-1 PDF Orthorhombic, Pnma(62) Z=4 mp= Cell=8.799x5.319x7.115<90x90x90> Pearson= Density(c)=4.185 Density(m)= Mwt= Vol= Ref= Ibid. Strong Line: 3.06/X 3.55/5 2.10/5 2.09/5 3.39/4 4.25/3 2.17/3 4.39/3 d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 5.5100 4.0 2.0 1 0 1 16.072 8.036 0.0907 1.1403 4.3900 25.0 17.0 2 0 0 20.211 10.106 0.1139 1.4312 4.2500 30.0 22.0 0 1 1 20.884 10.442 0.1176 1.4784 3.8300 1.0 1.0 1 1 1 23.205 11.602 0.1305 1.6405 3.5500 50.0 43.0 0 0 2 25.063 12.532 0.1408 1.7699 3.3900 35.0 32.0 2 1 0 26.267 13.134 0.1475 1.8534 3.2900 8.0 7.0 1 0 2 27.080 13.540 0.1520 1.9098 3.0600 100.0 100.0 2 1 1 29.159 14.580 0.1634 2.0533 2.8030 12.0 13.0 1 1 2 31.901 15.950 0.1784 2.2416 2.7650 10.0 11.0 2 0 2 32.351 16.176 0.1808 2.2724 2.6600 25.0 29.0 0 2 0 33.665 16.833 0.1880 2.3621 2.4540 18.0 22.0 2 1 2 36.587 18.294 0.2037 2.5604 2.3980 4.0 5.0 1 2 1 37.473 18.737 0.2085 2.6202 2.2890 2.0 3.0 1 0 3 39.329 19.665 0.2184 2.7449 2.2760 18.0 24.0 2 2 0 39.563 19.782 0.2197 2.7606 2.2620 2.0 3.0 3 0 2 39.818 19.909 0.2210 2.7777 2.1990 1.0 1.0 4 0 0 41.010 20.505 0.2274 2.8573 2.1680 25.0 35.0 2 2 1 41.623 20.812 0.2306 2.8981 2.1300 12.0 17.0 0 2 2 42.401 21.201 0.2347 2.9499 2.1010 50.0 73.0 4 0 1 43.015 21.508 0.2380 2.9906 2.0870 50.0 73.0 2 0 3 43.318 21.659 0.2396 3.0106 PDF#16-0846: QM=Star/Calculated; d=Other/Unknown; I=(Unknown) Tin Oxide Sulfate Sn2OSO4 Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= d-Cutoff= I/Ic(RIR)= Ref= Level-1 PDF Tetragonal, P-421c(114) Z=8 mp= Cell=10.93x10.93x8.931<90x90x90> Pearson= Density(c)=4.351 Density(m)= Mwt= Vol= Ref= Ibid. Strong Line: 3.22/X 6.91/8 1.76/8 2.14/8 4.66/8 2.36/8 2.61/8 1.83/8 d(A) I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d 7.7300 80.0 23.0 1 1 0 11.438 5.719 0.0647 0.8128 6.9100 80.0 25.0 1 0 1 12.800 6.400 0.0724 0.9093 5.4500 10.0 4.0 2 0 0 16.250 8.125 0.0917 1.1529 4.8900 10.0 5.0 2 1 0 18.126 9.063 0.1022 1.2849 4.6600 80.0 38.0 2 0 1 19.029 9.514 0.1073 1.3483 4.4700 60.0 30.0 0 0 2 19.846 9.923 0.1119 1.4056 4.2900 40.0 21.0 2 1 1 20.687 10.344 0.1166 1.4646 4.1300 10.0 5.0 1 0 2 21.498 10.749 0.1211 1.5214 3.8700 80.0 46.0 1 1 2 22.962 11.481 0.1292 1.6236 3.4600 60.0 38.0 2 0 2 25.726 12.863 0.1445 1.8159 3.3700 40.0 26.0 3 0 1 26.426 13.213 0.1484 1.8644 3.3000 80.0 53.0 2 1 2 26.997 13.498 0.1515 1.9040 3.2200 100.0 68.0 3 1 1 27.681 13.840 0.1553 1.9513 2.9210 80.0 60.0 2 2 2 30.580 15.290 0.1712 2.1510 2.8700 80.0 61.0 3 2 1 31.137 15.568 0.1742 2.1893 2.8240 80.0 62.0 3 0 2 31.657 15.829 0.1771 2.2249 2.7330 60.0 48.0 3 1 2 32.741 16.370 0.1829 2.2990 2.6510 10.0 8.0 4 1 0 33.783 16.892 0.1886 2.3701 2.6140 80.0 67.0 2 0 3 34.276 17.138 0.1913 2.4037 2.5760 10.0 9.0 3 3 0 34.798 17.399 0.1941 2.4391 2.5420 10.0 9.0 2 1 3 35.278 17.639 0.1967 2.4717 2.5070 40.0 35.0 3 2 2 35.787 17.894 0.1994 2.5063 2.4440 60.0 54.0 4 2 0 36.742 18.371 0.2046 2.5709 2.3560 80.0 75.0 4 2 1 38.167 19.083 0.2122 2.6669 2.3310 60.0 57.0 4 0 2 38.592 19.296 0.2145 2.6955 2.2810 40.0 39.0 4 1 2 39.473 19.736 0.2192 2.7546 2.2560 10.0 10.0 3 1 3 39.929 19.964 0.2216 2.7851 2.1440 80.0 82.0 4 2 2 42.111 21.056 0.2332 2.9306 2.1230 80.0 83.0 5 0 1 42.548 21.274 0.2355 2.9596 2.0840 20.0 21.0 5 1 1 43.384 21.692 0.2399 3.0150 2.0670 20.0 21.0 2 0 4 43.759 21.880 0.2419 3.0398 2.0150 10.0 11.0 4 0 3 44.949 22.475 0.2481 3.1182 1.9790 10.0 11.0 5 2 1 45.813 22.906 0.2527 3.1749 1.9330 60.0 68.0 2 2 4 46.968 23.484 0.2587 3.2505 1.8890 60.0 70.0 4 2 3 48.130 24.065 0.2647 3.3262 1.8750 60.0 70.0 3 1 4 48.512 24.256 0.2667 3.3510 1.8490 40.0 48.0 5 2 2 49.239 24.620 0.2704 3.3982 1.8340 80.0 96.0 5 3 1 49.669 24.835 0.2726 3.4259 1.8220 60.0 73.0 6 0 0 50.019 25.009 0.2744 3.4485 1.7980 10.0 12.0 3 2 4 50.733 25.367 0.2781 3.4945 1.7850 10.0 12.0 6 0 1 51.129 25.565 0.2801 3.5200 1.7620 80.0 100.0 5 0 3 51.846 25.923 0.2838 3.5659 1.7410 10.0 13.0 5 1 3 52.519 26.259 0.2872 3.6090 |
2楼2009-12-04 18:19:46