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jim5362

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氧瓶燃烧离子色谱测定片剂中的氨氯地平
摘要 目的:氧瓶燃烧离子色谱测定氨氯地平中的硫,然后根据化学式得到氨氯地平的含量。方法:用氧气瓶然后将氨氯地平中的硫氧化成硫的氧化物,用含有过氧化氢的水溶液吸收成硫酸根,离子色谱测定。结果:回收率为98%-102%之间, 线性范围为0.02 -60ug/ml,检测下限为0.00324ug/ml。结论:与其他方法相比,具有简单,快速,准确,可靠。
关键词:氧瓶燃烧,离子色谱,氨氯地平,硫
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jim5362(金币+3,VIP+0): 11-22 09:47
use oxygen cylinder combustion ion chromatograph determination tablet to text the ammonia chlorine horizontal abstract goal: use The oxygen cylinder combustion ion chromatograph determination ammonia chlorine horizontal sulfur, then obtains the ammonia chlorine horizontal content according to the chemical formula. Method: Then oxidizes with the oxygen cylinder the ammonia chlorine horizontal sulfur to be the oxide compound, with includes the hydrogen peroxide peroxide solution to absorb to be the sulfate radical, the ion chromatograph determination. Finally: The returns-ratio is between 98%-102%, the linearity range is 0.02 -60ug/ml, the examination lower limitation is 0.00324ug/ml. Conclusion: Compares with other methods,it express more simply, fast, accurate, reliable. Key word: Oxygen cylinder combustion, ion chromatograph, ammonia chlorine horizontal, sulfur
2楼2009-11-20 20:09:57
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