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求助cif语法错误（附cif原文及错误提示）
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cif原文 data_global _audit_update_record ; 2009-10-12 # Formatted by publCIF ; #============================================================================== _audit_creation_method 'form.cif (version 2.0)' # PROCESSING SUMMARY (IUCr Office Use Only) _journal_data_validation_number ? _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_paper_category ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #============================================================================== # SUBMISSION DETAILS _publ_contact_author # Name and address of author for correspondence ; **** Faculty of Chemical Engineering and Light Industry Guangdong University of Technology Guangzhou, 510006 China ; _publ_contact_author_email kzhang@gdut.edu.cn _publ_contact_author_fax ? _publ_contact_author_phone '86 020 13342885654' _publ_requested_journal 'Acta Crystallogr., Sect. E' _publ_requested_category EM _publ_contact_letter ; Dear Sir, Please consider this CIF submission for publication as a Regular Structure Paper in Acta Crystallogr., Sect. E. ***** ; #============================================================================== # 3. TITLE AND AUTHOR LIST _publ_section_title ; ; loop_ _publ_author_name _publ_author_address 'Zhang, Kun' ; Faculty of Chemical Engineering and Light Industry Guangdong University of Technology Guangzhou, 510006 People's Republic of China ; 'Wei, Xing-Chuan' ; School of Chemistry and Chemical Engineering Guangzhou University Guangzhou, 510006 People's Republic of China ; 'Dong, Wen' ; School of Chemistry and Chemical Engineering Guangzhou University Guangzhou, 510006 People's Republic of China ; 'Zheng, Xi' ; School of Chemistry and Chemical Engineering Ernest Mario School of Pharmacy Rutgers New Jersey, 08854-8020 United States ; 'Guan, Yang-fan' ; School of Chemistry and Chemical Engineering Guangzhou University Guangzhou, 510006 People's Republic of China ; 'Du, Zhi-yun' ; Faculty of Chemical Engineering and Light Industry Guangdong University of Technology Guangzhou, 510006 People's Republic of China ; #============================================================================== # 4. TEXT _publ_section_abstract ; The title complex C~26~H~30~O~7~ contains two 2,3,4 three-substituted benzylidene units which differ in the orientations of the cyclohexanone ring system. The crystal structure is stabilized by intermolecular C—H...π interactions. ; _publ_section_comment ; The title compound was obtained by the reaction of acetic acid, tetrahydrofuran, cyclohexanone and 2,3,4-tri-methoxy-benzaldehyde. Bond lengths are normal and are comparable to the corresponding values observed in (2E,6E)-2,6-Bis(3,5-di-ter-butyl-4-hydroxy-benzylidene) cyclohexanone acetic acid solvate(Zhi-Yun Du et al., 2005). No hydrogen bonds were observed in the complex. The crystal structure is stabilized by intermolecular C—H...π interactions. ; _publ_section_acknowledgements ; We acknowledge financial support by the Science and Technology Program Foundation of Guang Zhou(2006B13501002). ; _publ_section_related_literature ; ; _publ_section_references ; Youssef, K. M.; El-Sherbeny, M. A.; El-Sha?e, F. S.; Farag, H. A.; Al-Deeb, O. A.; Awadalla, S. A. A. (2004). Arch. Pharm. Pharm. Med. Chem. 337, 42–54. Sardjiman, S. S; Reksohadiprodjo, M. S.; Hakim, L.; Van der Goot, H.; Timmerman, H. (1997). Eur. J. Med. Chem. 32, 625–630. Murthy, M. S.; Mohan, S. (2006). Asian Journal of Chemistry. 18, 2963–2968. ; _publ_section_figure_captions ; Fig. 1. Perspective view of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme. ; _publ_section_exptl_prep ; A mixture of acetic acid saturated by sodium hydroxide (5ml), dihydrofuran (10mL), cyclohexanone (0.01mol)and 2,3,4-tri-methoxy-benzaldehyde (0.02mol) was stirred at 20-25℃ for 1h.Later,the reaction mixture was kept in romm temperature for five days.Yellow crystal appeared.The product was filtered,washed with ice-cold water,dried and recrystallized from acetone.The yield 90.2%. Elemental analysis, calcd (%) for C~26~: C 68.71, H 6.65; found(%): C 68.02, H 6.60. ; 投稿时的提示 Your file is not in CIF format or has CIF syntax errors. WARNING: Non-printable ASCII character \0241 at line 130 >>> "system." *** The CIF should contain only alphanumeric or punctuation characters defined as printable in the ASCII character set. WARNING: Non-printable ASCII character \0252 at line 130 WARNING: Non-printable ASCII character \0246 at line 130 WARNING: Non-printable ASCII character \0320 at line 130 WARNING: Non-printable ASCII character \0241 at line 142 >>> "is" WARNING: Non-printable ASCII character \0252 at line 142 WARNING: Non-printable ASCII character \0246 at line 142 WARNING: Non-printable ASCII character \0320 at line 142 WARNING: Non-printable ASCII character \0250 at line 162 >>> "337," WARNING: Non-printable ASCII character \0250 at line 165 >>> "Timmerman," WARNING: Non-printable ASCII character \0250 at line 167 >>> "Murthy," WARNING: Non-printable ASCII character \0241 at line 184 >>> "20-25¡æ" WARNING: Non-printable ASCII character \0346 at line 184 谁能帮忙解决一下，不要说些空话，用什么软件的 就说哪里错了改成什么 |
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maomao11259
木虫 (小有名气)
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