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如何获得如下文红色粗体中所说的CCDC-616162 号码？ Crystal data for 6 C17H23ClN2O2 (322.82), orthorhombic, space group P212121, a=9.007(1), b=9.438(1), c= 20.601(3) Å, U=1751.36 (36) Å3, Z=4, specimen 0.54× 0.52×0.44 mm3, T=286(2) K, SIEMENS P4 diffractometer, absorption coefficient 0.227 mm1, reflections collected 4978, independent reflections 4027 [RACHTUNGTRENUNG(int)=0.0102], refinement by full- matrix least-squares on F2, data/restraints/parameters 4027/2/212, goodness-of-fit on F2=0.936, final R indices [I>2s(I)] R1=0.0375, wR2=0.0786, R indices (all data) R1=0.0622, wR2=0.0839, largest diff. peak and hole 0.119 and 0.127 eÅ3. Crystallographic data for the structure 6 have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-616162. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK [fax.: (internat.) + 44 1223/336–033; e-mail: deposit@ccdc.cam.ac.uk]. 停止求助，谢谢 [ Last edited by liuyuanxiu on 2009-10-12 at 21:03 ] |
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fengqian2004
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liuyuanxiu(金币+3,VIP+0):xiexie 10-13 15:03
liuyuanxiu(金币+3,VIP+0):xiexie 10-13 15:03
| 直接发邮件到，deposit@ccdc.cam.ac.uk 他会告知你一个网站，好现象一开始要先注册，然后就可以下载了，也可以找到这个杂志或对应的文章附件即可下载。 |
2楼2009-10-12 20:37:15
fmopily
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3楼2009-10-12 20:58:26