| 查看: 1395 | 回复: 4 | ||||
| 当前主题已经存档。 | ||||
lijianghua2007荣誉版主 (职业作家)
|
[交流]
A类错误，怎么解决？
|
|||
|
Alert level A CELL003_ALERT_1_A _cell_measurement_reflns_used is missing Number of reflections used to measure unit cell. CELL004_ALERT_1_A _cell_measurement_theta_min is missing Minimum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 CELL005_ALERT_1_A _cell_measurement_theta_max is missing Maximum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 DIFF019_ALERT_1_A _diffrn_standards_number is missing Number of standards used in measurement. DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards. DIFF022_ALERT_1_A _diffrn_standards_decay_% is missing Percentage decrease in standards intensity. 这些A类错误是什么意思？怎么解决？ |
回复此楼» 收录本帖的淘帖专辑推荐
 单晶解析 |
» 猜你喜欢
单晶结构解析，各类疑难晶体数据处理和答疑
已经有38人回复
-
这个水相反应有没有催化剂促进发生
已经有4人回复
-
无机化学论文润色/翻译怎么收费?
已经有283人回复
-
Mn Me3TACN
已经有5人回复
-
求助最新的CCDC数据库升级包
已经有0人回复
-
高中化学教师求助：配合物一水硫酸四氨合铜的紫外可见吸收光谱数据
已经有2人回复
-
ACS omega，返修返回去目前为in peer review，求助进度问题
已经有4人回复
-
南开大学化学学院招收电催化方向2027级博士生、博士后
已经有27人回复
-
单晶解析，可协助单晶解析、精修、CIF 修正、错误排查
已经有0人回复
-
深圳大学化学与环境工程学院超分子团队招收2027级申请-考核制博士生
已经有6人回复
★ ★ ★ ★ ★
eeqeeq0002(金币+2,VIP+0):谢谢参与 9-13 10:20
lijianghua2007(金币+1,VIP+0):谢谢你，很详细！ 9-14 09:12
lijianghua2007(金币+2,VIP+0):最后2个还是给你啊！ 9-14 09:14
eeqeeq0002(金币+2,VIP+0):谢谢参与 9-13 10:20
lijianghua2007(金币+1,VIP+0):谢谢你，很详细！ 9-14 09:12
lijianghua2007(金币+2,VIP+0):最后2个还是给你啊！ 9-14 09:14
|
CELL003_ALERT_1_A _cell_measurement_reflns_used is missing Number of reflections used to measure unit cell. 晶胞探测使用的衍射点数 CELL004_ALERT_1_A _cell_measurement_theta_min is missing Minimum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 晶胞探测的最小theta角 CELL005_ALERT_1_A _cell_measurement_theta_max is missing Maximum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 晶胞探测的最大theta角 这三个数据应该在给你的信息文件里，如： _cell_measurement_reflns_used 2919 _cell_measurement_theta_min 2.14 _cell_measurement_theta_max 28.24 DIFF019_ALERT_1_A _diffrn_standards_number is missing Number of standards used in measurement. DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards. DIFF022_ALERT_1_A _diffrn_standards_decay_% is missing Percentage decrease in standards intensity. 这三个是监测晶体的指标，多数仪器已经不用了。如果你采集数据是用CCD衍射仪，那这三个后面都填 “ ？ ” 就可以了，如： _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? [ Last edited by monoclinic on 2009-9-12 at 23:16 ] |
2楼2009-09-12 23:15:00
3楼2009-09-13 09:39:26
4楼2009-09-13 12:41:58
l_viking
木虫 (小有名气)
- 应助: 0 (幼儿园)
- 金币: 3117.3
- 帖子: 97
- 在线: 22.3小时
- 虫号: 754406
- 注册: 2009-04-22
- 性别: GG
- 专业: 无机超分子化学
5楼2009-09-13 13:16:32
