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lijianghua2007荣誉版主 (职业作家)
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A类错误，怎么解决？
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Alert level A CELL003_ALERT_1_A _cell_measurement_reflns_used is missing Number of reflections used to measure unit cell. CELL004_ALERT_1_A _cell_measurement_theta_min is missing Minimum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 CELL005_ALERT_1_A _cell_measurement_theta_max is missing Maximum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 DIFF019_ALERT_1_A _diffrn_standards_number is missing Number of standards used in measurement. DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards. DIFF022_ALERT_1_A _diffrn_standards_decay_% is missing Percentage decrease in standards intensity. 这些A类错误是什么意思？怎么解决？ |
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eeqeeq0002(金币+2,VIP+0):谢谢参与 9-13 10:20
lijianghua2007(金币+1,VIP+0):谢谢你，很详细！ 9-14 09:12
lijianghua2007(金币+2,VIP+0):最后2个还是给你啊！ 9-14 09:14
eeqeeq0002(金币+2,VIP+0):谢谢参与 9-13 10:20
lijianghua2007(金币+1,VIP+0):谢谢你，很详细！ 9-14 09:12
lijianghua2007(金币+2,VIP+0):最后2个还是给你啊！ 9-14 09:14
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CELL003_ALERT_1_A _cell_measurement_reflns_used is missing Number of reflections used to measure unit cell. 晶胞探测使用的衍射点数 CELL004_ALERT_1_A _cell_measurement_theta_min is missing Minimum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 晶胞探测的最小theta角 CELL005_ALERT_1_A _cell_measurement_theta_max is missing Maximum theta of reflections used to measure unit cell. The following tests will not be performed. CELLT_01 晶胞探测的最大theta角 这三个数据应该在给你的信息文件里，如： _cell_measurement_reflns_used 2919 _cell_measurement_theta_min 2.14 _cell_measurement_theta_max 28.24 DIFF019_ALERT_1_A _diffrn_standards_number is missing Number of standards used in measurement. DIFF020_ALERT_1_A _diffrn_standards_interval_count and _diffrn_standards_interval_time are missing. Number of measurements between standards or time (min) between standards. DIFF022_ALERT_1_A _diffrn_standards_decay_% is missing Percentage decrease in standards intensity. 这三个是监测晶体的指标，多数仪器已经不用了。如果你采集数据是用CCD衍射仪，那这三个后面都填 “ ？ ” 就可以了，如： _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? [ Last edited by monoclinic on 2009-9-12 at 23:16 ] |
2楼2009-09-12 23:15:00
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3楼2009-09-13 09:39:26
4楼2009-09-13 12:41:58
l_viking
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5楼2009-09-13 13:16:32