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1) In the case of SEM analysis, I think that all samples should be polished and chemically treated to distinguish the crystalline phases from the glass and observe the microstructure. For particle sizes around 100nm, TEM analysis seems appropriate. 2) Throughout the document, the expression crystal phase or grain is considered appropriate for crystalline phase or grain. ÎÒÊÇ×ö²£Á§Ìմɵģ¬Éó¸åÈ˸øÁËÒâ¼û£¬µ«ÊÇÕâÁ½Ìì²»ÖªµÀÔõô»Ø¸´¡£ 1¡¢ÓÉÓÚÎÒ×öµÄ²£Á§ÌÕ´É£¬¾§ÏàºÍ²£Á§ÏàÔÚTEMÖкÜÄÑÕÕ³ö£¬Æä´ÎÖÆ±¸ÑùÆ·Ò²ºÜ¸´ÔÓ£¬ÏëÎÊÒ»ÏÂÔõôίÍñµã˵²â²»ÁËTEM¡£ 2¡¢Õâ¾ä»°ÊÇʲôÒâ˼£¬¾§ÏàºÍ¾§Á££¬ÎÒ¸ÃÔõô½âÊÍ ´ó¼Ò°ïæ³ö³öÖ÷Òâ |
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