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【答案】应助回帖
★ ★ ★ ★ ★
感谢参与，应助指数 +1
liuaifeng260199: 金币+5, ★★★★★最佳答案 2021-05-18 13:59:34
PDF#29-0497: QM=Calculated(C); d=Calculated; I=Calculated
Cobalt Phosphide
Co P
Radiation=CuKa1 Lambda=1.540598 Filter=
Calibration= 2T=23.662-139.814 I/Ic(RIR)=2.28
Ref: Natl. Bur. Stand. (U.S.) Monogr. 25, v15 p83 (1977)
Orthorhombic - Powder Diffraction, Pnma (62) Z=4 mp=
CELL: 5.077 x 3.281 x 5.587 <90.0 x 90.0 x 90.0> P.S=oP8 (Mn P)
Density(c)=6.417 Density(m)=5.63A Mwt=89.91 Vol=93.07 F(30)=54.9(.0140,39/0)
Ref: Rundqvist, S.
Acta Chem. Scand., v16 p287 (1962)
Strong Lines: 1.89/X 2.83/7 1.96/5 1.88/5 2.47/4 1.62/4 1.64/3 2.79/2 2.45/2 1.75/2
NOTE: Plus 6 reflections to 0.7917.
2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2
23.662 3.7570 7.0 ( 1 0 1) 11.831 0.1331 1.6724
31.600 2.8290 68.0 ( 0 1 1) 15.800 0.1767 2.2210
32.018 2.7930 20.0 ( 0 0 2) 16.009 0.1790 2.2496
35.336 2.5380 18.0 ( 2 0 0) 17.668 0.1970 2.4756
36.312 2.4720 41.0 ( 1 1 1) 18.156 0.2023 2.5417
36.696 2.4470 20.0 ( 1 0 2) 18.348 0.2043 2.5677
38.940 2.3110 2.0 ( 2 0 1) 19.470 0.2164 2.7188
45.114 2.0080 7.0 ( 2 1 0) 22.557 0.2490 3.1291
46.233 1.9620 51.0 ( 1 1 2) 23.116 0.2548 3.2024
48.130 1.8890 100.0 ( 2 1 1) 24.065 0.2647 3.3262
48.402 1.8790 46.0 ( 2 0 2) 24.201 0.2661 3.3439
52.292 1.7480 19.0 ( 1 0 3) 26.146 0.2860 3.5945
56.027 1.6400 26.0 ( 0 2 0) 28.014 0.3049 3.8312
56.364 1.6310 4.0 ( 2 1 2) 28.182 0.3066 3.8524
56.781 1.6200 38.0 ( 3 0 1) 28.391 0.3086 3.8785
61.706 1.5020 3.0 ( 2 0 3) 30.853 0.3329 4.1832
64.078 1.4520 1.0 ( 3 1 1) 32.039 0.3444 4.3273
65.963 1.4150 3.0 ( 0 2 2) 32.981 0.3534 4.4404
67.971 1.3780 3.0 ( 2 2 0) 33.986 0.3628 4.5596
68.823 1.3630 5.0 ( 1 2 2) 34.412 0.3668 4.6098
69.758 1.3470 2.0 ( 1 0 4) 34.879 0.3712 4.6646
70.297 1.3380 1.0 ( 2 2 1) 35.148 0.3737 4.6960
74.745 1.2690 4.0 ( 4 0 0) 37.373 0.3940 4.9513
75.867 1.2530 5.0 ( 3 0 3) 37.934 0.3990 5.0145
76.370 1.2460 9.0 ( 1 1 4) 38.185 0.4013 5.0427
77.101 1.2360 14.0 ( 2 2 2) 38.550 0.4045 5.0835
77.999 1.2240 2.0 ( 2 0 4) 39.000 0.4085 5.1333
80.188 1.1960 8.0 ( 1 2 3) 40.094 0.4181 5.2535
81.170 1.1840 2.0 ( 4 1 0) 40.585 0.4223 5.3067
83.392 1.1580 9.0 ( 4 1 1) 41.696 0.4318 5.4259
83.605 1.1556 8.0 ( 4 0 2) 41.802 0.4327 5.4372
83.836 1.1530 9.0 ( 3 2 1) 41.918 0.4337 5.4494
88.086 1.1080 2.0 ( 2 2 3) 44.043 0.4513 5.6707
89.826 1.0910 6.0 ( 1 0 5) 44.913 0.4583 5.7591
91.759 1.0730 2.0 ( 0 3 1) 45.879 0.4660 5.8557
94.378 1.0500 2.0 ( 1 3 1) 47.189 0.4762 5.9840
94.496 1.0490 2.0 ( 4 0 3) 47.248 0.4766 5.9897
95.453 1.0410 2.0 ( 1 2 4) 47.727 0.4803 6.0357
96.125 1.0355 2.0 ( 1 1 5) 48.062 0.4829 6.0678
97.695 1.0230 15.0 ( 2 0 5) 48.848 0.4888 6.1419
100.208 1.0040 4.0 ( 4 2 0) 50.104 0.4980 6.2582
100.897 0.9990 6.0 ( 4 1 3) 50.448 0.5005 6.2895
101.386 0.9955 6.0 ( 3 2 3) 50.693 0.5023 6.3116
102.368 0.9886 9.0 ( 2 3 1) 51.184 0.5058 6.3556
103.478 0.9810 2.0 ( 2 2 4) 51.739 0.5097 6.4049
109.197 0.9450 4.0 ( 2 3 2) 54.598 0.5291 6.6489
109.539 0.9430 5.0 ( 0 3 3) 54.770 0.5302 6.6630
111.388 0.9325 1.0 ( 3 0 5) 55.694 0.5362 6.7380
114.474 0.9160 7.0 ( 1 0 6) 57.237 0.5459 6.8594
115.939 0.9086 8.0 ( 1 2 5) 57.969 0.5503 6.9152
119.544 0.8915 2.0 ( 5 0 3) 59.772 0.5609 7.0479
121.234 0.8840 3.0 ( 2 3 3) 60.617 0.5656 7.1077
121.697 0.8820 5.0 ( 1 1 6) 60.848 0.5669 7.1238
123.557 0.8742 2.0 ( 2 0 6) 61.778 0.5720 7.1874
130.264 0.8490 3.0 ( 1 3 4) 65.132 0.5889 7.4007
131.089 0.8462 3.0 ( 6 0 0) 65.544 0.5909 7.4252
131.538 0.8447 1.0 ( 2 1 6) 65.769 0.5919 7.4384
136.785 0.8285 1.0 ( 4 3 0) 68.393 0.6035 7.5838
139.814 0.8202 4.0 ( 0 4 0) 69.907 0.6096 7.6606 |
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