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wgfz1979

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专业: 配位化学

[交流] 扫描方式求助

从这里看出扫描方式该怎麽描述？

-----------------------------------------------------------------------
diffrn_ambient_temperature    298(2)
_diffrn_radiation_wavelength    0.71073
_diffrn_radiation_type          MoK\a
_diffrn_radiation_source       'fine-focus sealed tube'
_diffrn_radiation_monochromator graphite
_diffrn_measurement_device_type 'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_detector_area_resol_mean  ?
_diffrn_standards_number       ?
_diffrn_standards_interval_count  ?
---------------------------------------------------------------------------
我表述为：
All measurements were made on a Bruker Smart-1000CCD diffractometer at 298(2) K with graphite monochromated Mo Kα radiation (λ = 0.71073 A) by using a
π-ω scan mode in the range of 1.87° < θ < 25.02°.

人家说扫描方式和CIF文件不符。

[ Last edited by wgfz1979 on 2009-8-6 at 11:00 ]

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