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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
wangch: 金币+20, ★★★很有帮助, 谢谢！ 2021-01-19 10:49:19
PDF#01-089-3736: QM=Uncommon(?); d=Calculated; I=(Unknown)
Iron Cobalt Cyanide Hydrate
Fe3(Co(CN)6)2(H2O)12
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= 2T=14.885-89.104 I/Ic(RIR)=4.42
Ref: Level-1 PDF
Cubic, F-43m (216) Z=2 mp=
CELL: 10.3 x 10.3 x 10.3 <90.0 x 90.0 x 90.0> P.S=
Density(c)=1.889 Density(m)= Mwt= Vol=1092.7
Ref: Ibid.
Strong Lines: 5.15/X 3.64/4 2.58/3 2.30/2 1.82/1 1.63/1 2.10/1 5.95/1
2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2
14.885 5.9467 6.8 ( 1 1 1) 7.443 0.0841 1.0566 3
17.204 5.1500 100.0 ( 2 0 0) 8.602 0.0971 1.2200 4
24.424 3.6416 40.2 ( 2 2 0) 12.212 0.1373 1.7254 8
28.723 3.1056 3.1 ( 3 1 1) 14.361 0.1610 2.0232 11
30.029 2.9734 1.6 ( 2 2 2) 15.015 0.1682 2.1132 12
34.812 2.5750 32.4 ( 4 0 0) 17.406 0.1942 2.4401 16
38.050 2.3630 1.4 ( 3 3 1) 19.025 0.2116 2.6590 19
39.079 2.3031 15.6 ( 4 2 0) 19.539 0.2171 2.7281 20
42.984 2.1025 6.9 ( 4 2 2) 21.492 0.2378 2.9885 24
45.735 1.9822 1.0 ( 5 1 1) 22.867 0.2522 3.1697 27
50.055 1.8208 11.6 ( 4 4 0) 25.027 0.2746 3.4508 32
52.519 1.7410 0.8 ( 5 3 1) 26.260 0.2872 3.6089 35
53.322 1.7167 6.3 ( 6 0 0) 26.661 0.2913 3.6601 36
56.457 1.6286 11.0 ( 6 2 0) 28.228 0.3070 3.8581 40
58.734 1.5707 0.3 ( 5 3 3) 29.367 0.3183 4.0001 43
59.481 1.5528 0.6 ( 6 2 2) 29.741 0.3220 4.0464 44
62.414 1.4867 2.1 ( 4 4 4) 31.207 0.3363 4.2263 48
64.563 1.4423 0.4 ( 7 1 1) 32.281 0.3467 4.3564 51
65.271 1.4283 4.6 ( 6 4 0) 32.635 0.3501 4.3989 52
68.062 1.3764 6.5 ( 6 4 2) 34.031 0.3633 4.5649 56
70.121 1.3410 0.4 ( 7 3 1) 35.060 0.3729 4.6856 59
73.495 1.2875 1.0 ( 8 0 0) 36.747 0.3883 4.8801 64
75.490 1.2584 0.1 ( 7 3 3) 37.745 0.3973 4.9932 67
76.151 1.2491 1.8 ( 6 4 4) 38.076 0.4003 5.0303 68
78.777 1.2139 2.5 ( 6 6 0) 39.389 0.4119 5.1762 72
80.732 1.1893 0.2 ( 7 5 1) 40.366 0.4204 5.2829 75
81.380 1.1815 0.7 ( 6 6 2) 40.690 0.4232 5.3180 76
83.965 1.1516 1.6 ( 8 4 0) 41.982 0.4342 5.4561 80
85.896 1.1306 0.2 ( 9 1 1) 42.948 0.4423 5.5575 83
86.538 1.1238 0.1 ( 8 4 2) 43.269 0.4449 5.5909 84
89.104 1.0980 2.0 ( 6 6 4) 44.552 0.4554 5.7225 88 |
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