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ÌâÄ¿Effect of nanocrystalline process on microstructure of Zr-based metallic glass ×÷ÕßJin Cai, Hui Liu, Jihong Zhu and Zheng Wang, DOI:https://doi.org/10.1088/2053-1591/aaf014 ÆÚ¿¯Mater. Res. Express ¾íºÅ£º2019 Vol.6 |
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Effect of nanocrystalline process on microstructure of Zr-based metallic glass ×÷Õß:Cai, J (Cai, Jin)[ 1 ] ; Liu, H (Liu, Hui)[ 2 ] ; Zhu, JH (Zhu, Jihong)[ 2 ] ; Wang, Z (Wang, Zheng)[ 3 ] ²é¿´ Web of Science ResearcherID ºÍ ORCID MATERIALS RESEARCH EXPRESS ¾í: 6 ÆÚ: 2 ÎÄÏ׺Å: 025044 DOI: 10.1088/2053-1591/aaf014 ³ö°æÄê: FEB 2019 ÎÄÏ×ÀàÐÍ:Article ²é¿´ÆÚ¿¯Ó°ÏìÁ¦ ÕªÒª This article focused on the microstructure changes of the Zirconium-based alloy with isothermal annealing close to the glass transition temperature. The differential scanning calorimetry (DSC) was used to measure the temperatures of crystallization and glass transition. The Small-angle neutron scattering (SANS) results revealed a peak associated with the interference in isothermal annealing. Under supercooling, crystallization was decomposed, in addition to transmission electron microscopy (TEM) results exhibited that a part of inhomogeneities formed at the early annealing of amorphous alloy had been crystallized later. TEM and x-ray diffraction (XRD) results illustrated that nanocrystalline phase formed after long time annealing, with decomposition of the initial phase. Nanoindentation experiments showed that the hardness descended on the increase of indentation loaded, while the excessive free-volume increased with the increasing indentation load. ¹Ø¼ü´Ê ×÷Õ߹ؼü´Ê:crystallization; glass transition; nanocrystalline phase; indentation load KeyWords Plus:ENHANCED PLASTICITY; CRYSTALLIZATION; BEHAVIORS ×÷ÕßÐÅÏ¢ ͨѶ×÷ÕßµØÖ·: Shenyang Aerospace University Shenyang Aerosp Univ, Fac Aerosp Engn, Shenyang, Liaoning, Peoples R China. ͨѶ×÷ÕßµØÖ·: Cai, J (corresponding author) ÏÔʾ¸ü¶à Shenyang Aerosp Univ, Fac Aerosp Engn, Shenyang, Liaoning, Peoples R China. µØÖ·: ÏÔʾ¸ü¶à [ 1 ] Shenyang Aerosp Univ, Fac Aerosp Engn, Shenyang, Liaoning, Peoples R China ÏÔʾ¸ü¶à [ 2 ] Northwestern Polytech Univ, Sch Mech Engn, Xian, Shaanxi, Peoples R China [ 3 ] AECC Shenyang Liming Aeroengine Co Ltd, Ctr Tech, Shenyang, Liaoning, Peoples R China µç×ÓÓʼþµØÖ·:whitemark2001@126.com »ù½ð×ÊÖúÖÂл »ù½ð×ÊÖú»ú¹¹ÏÔʾÏêÇé ÊÚȨºÅ National Natural Science Foundation of China 11722219 National Key Research and Development Program 2017YFB1102800 ²é¿´»ù½ð×ÊÖúÐÅÏ¢ ³ö°æÉÌ IOP PUBLISHING LTD, TEMPLE CIRCUS, TEMPLE WAY, BRISTOL BS1 6BE, ENGLAND Àà±ð / ·ÖÀà Ñо¿·½Ïò:Materials Science Web of Science Àà±ð:Materials Science, Multidisciplinary ÎÄÏ×ÐÅÏ¢ ÓïÑÔ:English Èë²ØºÅ: WOS:000451086600006 ISSN: 2053-1591 ÆäËûÐÅÏ¢ IDS ºÅ: HB5GE Web of Science ºËÐĺϼ¯ÖÐµÄ "ÒýÓõIJο¼ÎÄÏ×": 33 Web of Science ºËÐĺϼ¯ÖÐµÄ "±»ÒýƵ´Î": 0 |
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