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【答案】应助回帖
PDF#01-071-2450: QM=Calculated; d=Calculated; I=(Unknown)
Tungsten Oxide
W18O49
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= 2T=5.323-56.144 I/Ic(RIR)=6.65
Ref: Level-1 PDF
Monoclinic, P2/m (10) Z=1 mp=
CELL: 18.334 x 3.786 x 14.044 <90.0 x 115.2 x 90.0> P.S=
Density(c)=7.704 Density(m)= Mwt= Vol=882.0
Ref: Ibid.
Strong Lines: 3.79/X 3.74/4 12.71/3 3.65/3 3.40/3 2.66/2 3.41/2 2.53/2
2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2
5.323 16.5891 0.1 ( 1 0 0) 2.661 0.0301 0.3788
6.719 13.1454 6.8 (-1 0 1) 3.359 0.0380 0.4780
6.951 12.7074 34.0 ( 0 0 1) 3.475 0.0393 0.4945
10.408 8.4923 4.5 ( 1 0 1) 5.204 0.0589 0.7399
10.657 8.2945 7.2 ( 2 0 0) 5.329 0.0603 0.7575
12.610 7.0142 0.4 (-1 0 2) 6.305 0.0713 0.8958
13.461 6.5727 1.8 (-2 0 2) 6.730 0.0761 0.9560
13.927 6.3537 0.1 ( 0 0 2) 6.963 0.0787 0.9889
14.483 6.1110 3.6 (-3 0 1) 7.241 0.0818 1.0282
15.025 5.8918 0.3 ( 2 0 1) 7.512 0.0849 1.0664
16.015 5.5297 0.2 ( 3 0 0) 8.007 0.0904 1.1363
16.922 5.2354 2.7 ( 1 0 2) 8.461 0.0955 1.2001
19.026 4.6609 0.5 (-2 0 3) 9.513 0.1073 1.3481
19.278 4.6004 3.4 (-1 0 3) 9.639 0.1087 1.3658
19.467 4.5561 2.7 (-4 0 1) 9.734 0.1097 1.3791
19.955 4.4458 3.6 (-4 0 2) 9.978 0.1125 1.4133
20.039 4.4274 4.1 ( 3 0 1) 10.019 0.1129 1.4192
20.250 4.3818 2.1 (-3 0 3) 10.125 0.1141 1.4339
20.904 4.2461 0.3 ( 2 0 2) 10.452 0.1178 1.4797
21.408 4.1473 0.5 ( 4 0 0) 10.704 0.1206 1.5150
22.722 3.9103 1.6 (-4 0 3) 11.361 0.1279 1.6068
23.479 3.7860 100.0 ( 0 1 0) 11.739 0.1321 1.6596
23.771 3.7401 40.6 ( 1 0 3) 11.885 0.1337 1.6799
24.393 3.6462 29.2 (-5 0 2) 12.196 0.1371 1.7232
25.247 3.5247 0.7 ( 4 0 1) 12.623 0.1419 1.7826
25.441 3.4983 1.8 (-2 0 4) 12.720 0.1429 1.7961
25.743 3.4579 1.1 (-3 0 4) 12.871 0.1446 1.8170
25.847 3.4442 1.7 ( 2 1 0) 12.924 0.1452 1.8243
26.109 3.4103 19.2 (-5 0 3) 13.054 0.1466 1.8424
26.197 3.3989 26.6 (-1 0 4) 13.099 0.1471 1.8486
26.850 3.3178 1.9 ( 5 0 0) 13.425 0.1507 1.8938
27.112 3.2864 0.9 (-4 0 4) 13.556 0.1521 1.9119
27.396 3.2529 4.6 ( 2 0 3) 13.698 0.1537 1.9316
27.695 3.2184 1.0 (-3 1 1) 13.848 0.1554 1.9523
28.065 3.1769 7.6 ( 0 0 4) 14.032 0.1574 1.9778
28.550 3.1240 0.1 ( 3 1 0) 14.275 0.1601 2.0113
29.083 3.0679 1.0 ( 1 1 2) 14.542 0.1630 2.0481
29.204 3.0555 3.7 (-6 0 2) 14.602 0.1636 2.0564
29.485 3.0270 3.9 (-5 0 4) 14.742 0.1652 2.0757
29.983 2.9778 2.0 (-6 0 1) 14.991 0.1679 2.1100
30.128 2.9639 6.5 (-6 0 3) 15.064 0.1687 2.1199
30.316 2.9459 7.2 ( 4 0 2) 15.158 0.1697 2.1328
30.392 2.9387 4.9 (-2 1 3) 15.196 0.1701 2.1381
30.585 2.9206 14.5 (-1 1 3) 15.292 0.1712 2.1513
30.679 2.9119 9.7 (-4 1 1) 15.339 0.1717 2.1578
31.055 2.8774 2.1 (-4 1 2) 15.528 0.1738 2.1836
31.196 2.8648 1.3 (-3 1 3) 15.598 0.1745 2.1933
31.857 2.8068 3.8 (-3 0 5) 15.928 0.1781 2.2385
31.982 2.7961 2.4 ( 4 1 0) 15.991 0.1788 2.2471
32.117 2.7847 1.7 (-2 0 5) 16.059 0.1796 2.2563
32.354 2.7648 8.6 ( 6 0 0) 16.177 0.1808 2.2725
32.525 2.7506 12.5 (-4 0 5) 16.263 0.1818 2.2843
32.624 2.7426 8.8 (-6 0 4) 16.312 0.1823 2.2910
32.902 2.7200 1.0 (-4 1 3) 16.451 0.1838 2.3100
33.657 2.6607 19.3 ( 1 1 3) 16.828 0.1879 2.3615
34.112 2.6263 14.9 (-5 0 5) 17.056 0.1904 2.3924
34.227 2.6177 9.4 ( 2 0 4) 17.113 0.1910 2.4003
34.590 2.5910 0.3 (-7 0 3) 17.295 0.1930 2.4250
34.746 2.5798 0.4 ( 4 1 1) 17.373 0.1938 2.4355
34.891 2.5694 1.0 (-2 1 4) 17.446 0.1946 2.4454
35.396 2.5339 12.3 (-5 1 3) 17.698 0.1973 2.4797
35.463 2.5292 15.6 (-1 1 4) 17.732 0.1977 2.4842
35.962 2.4953 1.3 ( 5 1 0) 17.981 0.2004 2.5180
36.036 2.4903 1.3 ( 6 0 1) 18.018 0.2008 2.5230
36.163 2.4818 1.3 ( 4 0 3) 18.082 0.2015 2.5317
36.384 2.4673 2.8 ( 2 1 3) 18.192 0.2027 2.5466
36.906 2.4336 4.5 ( 0 1 4) 18.453 0.2055 2.5818
37.805 2.3777 2.3 (-6 1 2) 18.903 0.2103 2.6425
37.936 2.3699 1.5 ( 7 0 0) 18.968 0.2110 2.6513
38.029 2.3642 2.3 ( 1 0 5) 19.015 0.2115 2.6576
38.179 2.3553 1.3 ( 3 0 4) 19.090 0.2123 2.6677
38.428 2.3406 1.3 (-6 1 1) 19.214 0.2136 2.6844
38.545 2.3338 4.3 (-6 1 3) 19.273 0.2142 2.6923
38.697 2.3250 5.5 ( 4 1 2) 19.348 0.2151 2.7024
38.914 2.3125 8.3 ( 5 1 1) 19.457 0.2162 2.7171
39.382 2.2861 0.6 (-8 0 3) 19.691 0.2187 2.7485
39.527 2.2780 0.4 (-5 0 6) 19.764 0.2195 2.7582
39.726 2.2671 0.2 ( 3 1 3) 19.863 0.2205 2.7715
39.952 2.2548 2.3 (-3 1 5) 19.976 0.2218 2.7866
40.167 2.2432 1.3 (-2 1 5) 20.083 0.2229 2.8010
40.362 2.2328 6.0 ( 6 1 0) 20.181 0.2239 2.8140
40.504 2.2253 9.5 (-4 1 5) 20.252 0.2247 2.8235
40.586 2.2210 5.6 (-6 1 4) 20.293 0.2251 2.8289
40.973 2.2009 0.2 (-8 0 1) 20.486 0.2272 2.8548
41.049 2.1970 0.2 ( 5 0 3) 20.525 0.2276 2.8599
41.169 2.1909 0.2 (-1 1 5) 20.584 0.2282 2.8679
41.315 2.1835 0.2 ( 2 0 5) 20.658 0.2290 2.8776
41.600 2.1692 0.7 ( 7 0 1) 20.800 0.2305 2.8966
41.796 2.1595 0.3 (-5 1 5) 20.898 0.2315 2.9096
41.924 2.1532 0.7 ( 2 1 4) 20.962 0.2322 2.9181
42.231 2.1382 0.1 (-7 1 3) 21.116 0.2338 2.9385
42.547 2.1231 0.1 ( 4 0 4) 21.274 0.2355 2.9595
42.656 2.1179 0.1 ( 0 0 6) 21.328 0.2361 2.9667
42.821 2.1101 0.4 ( 0 1 5) 21.410 0.2370 2.9776
42.942 2.1045 0.3 ( 5 1 2) 21.471 0.2376 2.9857
43.492 2.0791 0.9 ( 6 1 1) 21.746 0.2405 3.0220
43.569 2.0756 0.9 ( 4 1 3) 21.784 0.2409 3.0271
44.438 2.0370 0.1 (-9 0 3) 22.219 0.2455 3.0845
44.960 2.0146 0.5 (-9 0 2) 22.480 0.2482 3.1188
45.114 2.0081 3.4 (-9 0 4) 22.557 0.2490 3.1290
45.383 1.9968 2.0 ( 1 0 6) 22.692 0.2504 3.1467
45.563 1.9893 1.2 (-3 1 6) 22.782 0.2513 3.1585
45.677 1.9846 0.5 (-4 1 6) 22.839 0.2519 3.1660
46.196 1.9635 1.4 ( 6 0 3) 23.098 0.2546 3.2000
46.359 1.9570 1.1 (-8 1 3) 23.179 0.2555 3.2106
46.486 1.9519 0.6 (-5 1 6) 23.243 0.2562 3.2189
46.686 1.9440 3.0 (-9 0 1) 23.343 0.2572 3.2320
46.945 1.9339 0.5 (-9 0 5) 23.472 0.2585 3.2489
47.255 1.9219 1.6 ( 5 0 4) 23.628 0.2602 3.2692
47.383 1.9171 1.0 (-1 1 6) 23.692 0.2608 3.2775
47.542 1.9110 0.4 ( 6 1 2) 23.771 0.2616 3.2879
48.023 1.8930 15.2 ( 0 2 0) 24.011 0.2641 3.3192
48.317 1.8822 1.3 ( 7 1 1) 24.159 0.2657 3.3383
48.433 1.8779 1.9 (-7 0 7) 24.216 0.2663 3.3458
48.650 1.8701 4.6 ( 0 2 1) 24.325 0.2674 3.3599
49.353 1.8451 0.6 ( 4 0 5) 24.676 0.2710 3.4054
49.515 1.8394 0.4 (-8 1 5) 24.757 0.2718 3.4159
49.725 1.8321 0.5 (-10,0,3) 24.863 0.2729 3.4295
49.834 1.8284 0.5 (-9 0 6) 24.917 0.2735 3.4365
49.988 1.8231 1.3 (-10,0,4) 24.994 0.2743 3.4465
50.216 1.8153 3.9 ( 0 0 7) 25.108 0.2754 3.4612
50.561 1.8038 0.5 (-10,0,2) 25.280 0.2772 3.4834
50.775 1.7967 1.3 (-8 0 7) 25.387 0.2783 3.4971
50.860 1.7938 0.8 (-9 1 3) 25.430 0.2787 3.5026
51.337 1.7783 5.1 (-9 1 2) 25.668 0.2812 3.5332
51.471 1.7740 5.8 (-9 1 4) 25.735 0.2819 3.5418
51.716 1.7662 2.3 ( 1 1 6) 25.858 0.2831 3.5575
51.897 1.7604 1.4 ( 8 0 2) 25.948 0.2840 3.5691
52.257 1.7492 4.1 ( 6 0 4) 26.128 0.2859 3.5921
52.456 1.7430 6.8 (-10,0,1) 26.228 0.2869 3.6049
52.644 1.7372 4.0 (-2 1 7) 26.322 0.2878 3.6169
52.706 1.7353 3.1 (-3 0 8) 26.353 0.2881 3.6208
52.900 1.7294 4.0 (-6 1 7) 26.450 0.2891 3.6332
53.420 1.7138 1.5 ( 5 1 4) 26.710 0.2918 3.6663
53.657 1.7068 1.4 (-9 0 7) 26.829 0.2930 3.6814
54.267 1.6890 6.0 ( 1 2 3) 27.134 0.2960 3.7201
54.579 1.6801 5.5 (-5 2 2) 27.290 0.2976 3.7398
54.699 1.6767 6.5 ( 2 1 6) 27.350 0.2982 3.7474
55.119 1.6649 0.5 ( 3 2 2) 27.560 0.3003 3.7740
55.520 1.6538 5.4 (-5 2 3) 27.760 0.3023 3.7992
55.688 1.6492 3.5 (-1 0 8) 27.844 0.3032 3.8098
55.933 1.6426 1.7 (-8 0 8) 27.967 0.3044 3.8252
56.144 1.6369 4.9 ( 0 1 7) 28.072 0.3055 3.8385 |
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