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jinshanli至尊木虫 (知名作家)
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[求助]
单晶有不少错误解析困难，请求帮助，谢谢！
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测出来的单晶有不少错误，说是单晶无序，请各位单晶解析高手帮忙解析一下，谢谢啦！ 主要想确定结构中标红的两个基团相对构型，是顺式还是反式的，非常感谢！ |
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感谢参与，应助指数 +1
jinshanli: 金币+200, ★★★★★最佳答案, 谢谢啦！ 2020-01-08 20:10:12
感谢参与，应助指数 +1
jinshanli: 金币+200, ★★★★★最佳答案, 谢谢啦！ 2020-01-08 20:10:12
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链接: https://pan.baidu.com/s/1Zb4qaDgj1s04-5GCbGqxLw 提取码: yw9j 无序与否并不影响两个目标基团位置的判断 |
4楼2020-01-07 21:35:17
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感谢参与，应助指数 +1
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test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level A EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 DIFF003_ALERT_1_A _diffrn_measurement_device_type is missing Diffractometer make and type. Replaces _diffrn_measurement_type. PLAT183_ALERT_1_A Missing _cell_measurement_reflns_used Value .... Please Do ! PLAT184_ALERT_1_A Missing _cell_measurement_theta_min Value ...... Please Do ! PLAT185_ALERT_1_A Missing _cell_measurement_theta_max Value ...... Please Do ! PLAT699_ALERT_1_A Missing _exptl_crystal_description Value ....... Please Do ! Alert level C PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ Please Check PLAT043_ALERT_1_C Calculated and Reported Mol. Weight Differ by .. 2.02 Check PLAT052_ALERT_1_C Info on Absorption Correction Method Not Given Please Do ! PLAT053_ALERT_1_C Minimum Crystal Dimension Missing (or Error) ... Please Check |
2楼2020-01-07 21:31:19
羊倌
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jinshanli: 金币+100, ★★★很有帮助, 谢谢！ 2020-01-08 20:10:27
jinshanli: 金币+100, ★★★很有帮助, 谢谢！ 2020-01-08 20:10:27
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test-name_ALERT_alert-type_alert-level. Click on the hyperlinks for more details of the test. Alert level A EXPT005_ALERT_1_A _exptl_crystal_description is missing Crystal habit description. The following tests will not be performed. CRYSR_01 DIFF003_ALERT_1_A _diffrn_measurement_device_type is missing Diffractometer make and type. Replaces _diffrn_measurement_type. PLAT183_ALERT_1_A Missing _cell_measurement_reflns_used Value .... Please Do ! PLAT184_ALERT_1_A Missing _cell_measurement_theta_min Value ...... Please Do ! PLAT185_ALERT_1_A Missing _cell_measurement_theta_max Value ...... Please Do ! PLAT699_ALERT_1_A Missing _exptl_crystal_description Value ....... Please Do ! Alert level C PLAT041_ALERT_1_C Calc. and Reported SumFormula Strings Differ Please Check PLAT043_ALERT_1_C Calculated and Reported Mol. Weight Differ by .. 2.02 Check PLAT052_ALERT_1_C Info on Absorption Correction Method Not Given Please Do ! PLAT053_ALERT_1_C Minimum Crystal Dimension Missing (or Error) ... Please Check |
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