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wgfz1979

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[½»Á÷] Òª·¢E,ÕâÑùµÄ½á¹ûÄÜÐÞ¸ÄÂð?

ÎÒÏëͶ¸åE, check ºó,ÓиöB,»¹Óм¸¸öC¼¶´íÎó,ÇëÐֵܽãÃÃÃǰïÎÒ¿´¿´,ÄÜ·ñÔÙÐÞ¸Ä,Èô²»ÐèÐÞ¸Ä,ÕâÑùµÄ½á¹ûÄÜ·¢EÂð?


Click on the hyperlinks for more details of the test.

Alert level B
PLAT417_ALERT_2_B Short Inter D-H..H-D       H3     ..  H6      ..       1.83 Ang.

Alert level C
STRVA01_ALERT_4_C           Flack test results are ambiguous.
           From the CIF: _refine_ls_abs_structure_Flack    0.480
           From the CIF: _refine_ls_abs_structure_Flack_su    0.140
PLAT340_ALERT_3_C Low Bond Precision on C-C Bonds (x 1000) Ang ...          6      
PLAT033_ALERT_4_C Flack x Parameter Value Deviates from Zero .....       0.48      

Alert level G
REFLT03_ALERT_4_G Please check that the estimate of the number of Friedel pairs is
            correct. If it is not, please give the correct count in the
            _publ_section_exptl_refinement section of the submitted CIF.
           From the CIF: _diffrn_reflns_theta_max           25.01
           From the CIF: _reflns_number_total               2502
           Count of symmetry unique reflns         1495
           Completeness (_total/calc)            167.36%
           TEST3: Check Friedels for noncentro structure
           Estimate of Friedel pairs measured      1007
           Fraction of Friedel pairs measured     0.674
           Are heavy atom types Z>Si present        yes
PLAT066_ALERT_1_G Predicted and Reported Transmissions Identical .          ?

[ Last edited by wgfz1979 on 2009-6-8 at 09:07 ]
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paopaomeng(½ð±Ò+1,VIP+0):лл½»Á÷ 6-8 17:24
wgfz1979(½ð±Ò+1,VIP+0):лл! 6-9 10:12
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