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201620671

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[求助] 帮忙回复下这个审稿意见,,多谢了

The authors commented: "The experimental PXRD patterns of the as-synthesized samples agree well with their simulated ones, indicating the phase purity of the bulk samples (Fig. 4)." The experimental PXRD of the as-synthesized samples contain the signals for the uncoordinated solvent molecules. However, there are no signals for the uncoordinated solvent molecules in the simulated ones for complex 2 and 3. So where are the signals for the uncoordinated solvent molecules in the experimental PXRD patterns of the as-synthesized samples?
帮忙回答下这个问题,@jackdeng@lich666
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jackdeng

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请先告知你的晶体结构里是否有未配位的水。如果有,你在结构解析时,是否使用了squeeze?

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2楼2019-07-23 22:44:26
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201620671

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引用回帖:
2楼: Originally posted by jackdeng at 2019-07-23 22:44:26
请先告知你的晶体结构里是否有未配位的水。如果有,你在结构解析时,是否使用了squeeze?

有未配位的水,用了squeeze

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3楼2019-07-24 10:56:38
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