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[求助]
求37-1493XRD标准卡片！ 已有1人参与
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求37-1493XRD标准卡片。 或者得到XRD标准卡片的方法。 感谢！ @jackdeng @lich666 发自小木虫Android客户端 |
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ddtongda 
新虫 (著名写手)
- 应助: 49 (小学生)
- 金币: 9673.4
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- 虫号: 2826034
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- 专业: 活体与复杂样品分析
【答案】应助回帖
感谢参与，应助指数 +1
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PDF#00-037-1493: QM=Star(S); d=Diffractometer; I=Diffractometer Lanthanum orthoferrite FeLaO3 Dark brown Radiation=CuKa1 Lambda=1.5405981 Filter=Graph Calibration=Internal(W) 2T=22.606-112.542 I/Ic(RIR)= Ref: McMurdie, H., Morris, M., Evans, E., Paretzkin, B., Wong-Ng, W., Hubbard, C. Powder Diffraction, v1 p269 (1986) Orthorhombic - Powder Diffraction, Pn*a (62) Z=4 mp= CELL: 5.5669 x 7.8547 x 5.553 <90.0 x 90.0 x 90.0> P.S=oP20 (?) Density(c)=6.640 Density(m)=6.25A Mwt=242.75 Vol=242.81 F(30)=33.8(.0106,84/0) Ref: 1. Geller, S., Wood, E.A. Acta Crystallogr., v9 p563 (1956) Strong Lines: 2.78/X 1.60/4 1.97/3 2.27/2 3.93/2 1.39/2 1.05/1 1.24/1 NOTE: A stoichiometric mixture of La ( O H )3 and Fe2 O3 was heated overnight to 1000$DE, then 1 day each at 1200$DE and 1350$DE. The structure was qualitatively determined by Geller and Wood (1). A rhombohedral phase was found above 980$DE (Dalziel, 2). The mean temperature of data collection was 25.4$DE. To replace 00-015-0148, Geller and Wood (1). 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 22.606 3.9302 17.0 ( 1 0 1) 11.303 0.1272 1.5987 25.304 3.5169 4.0 ( 1 1 1) 12.652 0.1422 1.7866 32.190 2.7785 100.0 ( 1 2 1) 16.095 0.1799 2.2613 34.145 2.6238 3.0 ( 2 1 0) 17.072 0.1906 2.3947 36.090 2.4867 <1 ( 2 0 1) 18.045 0.2011 2.5267 37.938 2.3697 3.0 ( 1 1 2) 18.969 0.2110 2.6514 39.674 2.2700 18.0 ( 2 2 0) 19.837 0.2203 2.7680 41.389 2.1798 3.0 ( 1 3 1) 20.694 0.2294 2.8825 43.000 2.1018 <1 ( 2 2 1) 21.500 0.2379 2.9895 46.144 1.9656 30.0 ( 2 0 2) 23.072 0.2544 3.1966 47.638 1.9074 5.0 ( 2 3 0) 23.819 0.2621 3.2941 50.592 1.8027 1.0 ( 1 3 2) 25.296 0.2774 3.4854 51.999 1.7572 7.0 ( 1 4 1) 25.999 0.2845 3.5756 53.303 1.7173 4.0 ( 3 1 1) 26.651 0.2912 3.6588 57.399 1.6041 39.0 ( 2 4 0) 28.699 0.3117 3.9170 58.675 1.5722 1.0 ( 2 3 2) 29.338 0.3180 3.9965 59.945 1.5419 <1 ( 2 4 1) 29.972 0.3243 4.0750 61.288 1.5113 <1 ( 0 3 3) 30.644 0.3308 4.1576 63.660 1.4605 3.0 ( 3 3 1) 31.830 0.3423 4.3020 67.349 1.3892 15.0 ( 2 4 2) 33.674 0.3599 4.5228 68.398 1.3705 2.0 ( 4 1 0) 34.199 0.3648 4.5847 68.563 1.3676 <1 ( 2 5 0) 34.281 0.3656 4.5944 70.825 1.3293 <1 ( 3 3 2) 35.412 0.3761 4.7265 70.920 1.3278 <1 ( 1 5 2) 35.460 0.3766 4.7321 72.068 1.3094 4.0 ( 1 4 3) 36.034 0.3818 4.7984 73.177 1.2923 1.0 ( 3 1 3) 36.588 0.3869 4.8620 76.640 1.2423 11.0 ( 2 0 4) 38.320 0.4025 5.0577 77.637 1.2288 2.0 ( 4 1 2) 38.819 0.4069 5.1132 77.731 1.2276 2.0 ( 2 5 2) 38.866 0.4073 5.1184 80.065 1.1976 <1 ( 0 5 3) 40.032 0.4175 5.2467 81.115 1.1847 3.0 ( 2 6 0) 40.558 0.4221 5.3037 82.169 1.1721 2.0 ( 3 5 1) 41.084 0.4266 5.3604 85.434 1.1355 4.0 ( 4 4 0) 42.717 0.4403 5.5334 85.614 1.1336 3.0 ( 0 4 4) 42.807 0.4411 5.5428 86.553 1.1237 1.0 ( 4 3 2) 43.276 0.4450 5.5917 88.765 1.1013 <1 ( 4 1 3) 44.383 0.4540 5.7053 88.865 1.1003 <1 ( 2 5 3) 44.433 0.4544 5.7104 89.977 1.0896 2.0 ( 2 6 2) 44.989 0.4589 5.7666 90.852 1.0813 1.0 ( 5 1 1) 45.426 0.4624 5.8105 91.133 1.0788 1.0 ( 1 1 5) 45.566 0.4635 5.8245 94.389 1.0499 13.0 ( 2 4 4) 47.194 0.4762 5.9844 95.348 1.0419 <1 ( 4 5 0) 47.674 0.4799 6.0306 97.670 1.0232 <1 ( 3 3 4) 48.835 0.4887 6.1406 99.736 1.0075 1.0 ( 5 3 1) 49.868 0.4963 6.2364 99.904 1.0063 1.0 ( 3 5 3) 49.952 0.4969 6.2441 103.197 0.9829 2.0 ( 4 0 4) 51.599 0.5087 6.3924 103.352 0.9819 1.0 ( 0 8 0) 51.676 0.5092 6.3992 104.318 0.9754 2.0 ( 4 5 2) 52.159 0.5126 6.4416 107.744 0.9537 2.0 ( 4 6 0) 53.872 0.5243 6.5883 107.920 0.9526 1.0 ( 1 8 1) 53.960 0.5249 6.5957 108.840 0.9471 1.0 ( 5 1 3) 54.420 0.5279 6.6340 109.048 0.9459 <1 ( 3 1 5) 54.524 0.5286 6.6426 112.353 0.9272 4.0 ( 5 2 3) 56.177 0.5392 6.7764 112.542 0.9262 9.0 ( 3 6 3) 56.271 0.5398 6.7838 |
2楼2019-04-11 09:37:52
3楼2019-04-11 16:08:26
ddtongda
新虫 (著名写手)
- 应助: 49 (小学生)
- 金币: 9673.4
- 散金: 81
- 红花: 9
- 帖子: 2034
- 在线: 67.5小时
- 虫号: 2826034
- 注册: 2013-11-25
- 专业: 活体与复杂样品分析
4楼2019-04-12 08:09:24