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【求助】XPS表征Pt/C催化剂时遇到的问题! 审稿人的comments
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投了journal of materials chemistry一篇稿件,审稿人对XPS的结果提出了质疑.下面是原话.我对xps很不熟悉,审稿人所说的adsorbed species or contaminations over specimen是什么意思,我的两个Pt/C 催化剂是在同样条件下制备的啊,应该没有多余的吸附物的,而且审稿人结论说xps determination over an unclean surface......; 请问,这个不干净的表面是什么意思,做XPS的时候,什么情况下才会有不干净的表面.谢谢大侠赐教啊. 最后,请问该怎么回复审稿人下面的疑问,从哪些方面写. 奖金币 The problem is that, what’s the XPS experimental condition, for examples, the B.E., reference, the procedure of specimen pretreatment. The adsorbed species or contaminations over the specimen often cause a shift of B.E., so the XPS determination over an unclean surface may result in an incorrect conclusion. |
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