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[交流] 求助氧化锌银晶型晶胞参数及XRD衍射图

氧化锌银晶型晶胞参数及XRD衍射图

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ZnO 分析

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氧化锌银是个什么东西？

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氧化锌和银

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3楼2009-04-03 12:41:48

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warlen(金币+1,VIP+0):3q，辛苦了！ 4-3 14:51

PDF#36-1451: QM=Star(+); d=Diffractometer; I=Diffractometer
Zincite, syn
Zn O (Colorless)
Radiation=CuKa1 Lambda=1.5405981 Filter=Graph
Calibration= d-Cutoff=17.7 I/Ic(RIR)=
Ref= McMurdie, H., Morris, M., Evans, E., Paretzkin, B., Wong-Ng, W., Ettlinger, L., Hubbard, C.
Powder Diffraction, 1 76 (1986)
Hexagonal - Powder Diffraction,  P63mc (186) Z=2 mp=
Cell=3.2498x5.2066 Pearson=hP4 (S Zn)
Density(c)=5.675 Density(m)=6.43A Mwt=81.38 Vol=47.62 F(27)=129.6(.0072,29)
Ref= 1. Bragg, W.
Philos. Mag., 39 647 (1920)
Strong Line: 2.48/X 2.81/6 2.60/4 1.62/3 1.48/3 1.91/2 1.38/2 1.36/1 0.91/1 1.09/1
NOTE:  The sample was obtained from the New Jersey Zinc Co., Bethlehem, Pennsylvania, USA.
References to other early patterns may be found in reference (5).
The structure was determined by Bragg (1) and refined by Abrahams, Bernstein (2).
A high pressure cubic NaCl-type of ZnO is reported by Bates et al.
(3) and a cubic, sphalerite type is reported by Radczewski, Schicht (4).
The approximate temperature of data collection was 26 C.
To replace 00-005-0664 (5).
See ICSD 31052 (PDF 01-075-1526).
d(A)    I(f) I(v) h k l n^2 2-Theta Theta 1/(2d) 2pi/d
2.8143 57.0 50.0 1 0 0      31.769 15.885 0.1777 2.2326
2.6033 44.0 42.0 0 0 2      34.421 17.211 0.1921 2.4135
2.4759 100.0 100.0 1 0 1      36.252 18.126 0.2019 2.5377
1.9111 23.0 30.0 1 0 2      47.538 23.769 0.2616 3.2877
1.6247 32.0 49.0 1 1 0      56.602 28.301 0.3077 3.8672
1.4771 29.0 49.0 1 0 3      62.862 31.431 0.3385 4.2537
1.4072 4.0 7.0 2 0 0      66.378 33.189 0.3553 4.4652
1.3782 23.0 41.0 1 1 2      67.961 33.981 0.3628 4.5590
1.3583 11.0 20.0 2 0 1      69.098 34.549 0.3681 4.6259
1.3017 2.0 4.0 0 0 4      72.560 36.280 0.3841 4.8268
1.2380 4.0 8.0 2 0 2      76.953 38.476 0.4039 5.0752
1.1816 1.0 2.0 1 0 4      81.368 40.684 0.4231 5.3174
1.0931 7.0 16.0 2 0 3      89.604 44.802 0.4574 5.7479
1.0638 3.0 7.0 2 1 0      92.781 46.390 0.4700 5.9061
1.0423 6.0 14.0 2 1 1      95.301 47.650 0.4797 6.0284
1.0159 4.0 10.0 1 1 4      98.609 49.305 0.4922 6.1845
0.9846 2.0 5.0 2 1 2      102.942 51.471 0.5078 6.3812
0.9766 5.0 13.0 1 0 5      104.130 52.065 0.5120 6.4335
0.9556 1.0 3.0 2 0 4      107.426 53.713 0.5232 6.5751
0.9381 3.0 8.0 3 0 0      110.388 55.194 0.5330 6.6976
0.9069 8.0 22.0 2 1 3      116.274 58.137 0.5513 6.9279
0.8826 4.0 11.0 3 0 2      121.567 60.783 0.5665 7.1193
0.8677 1.0 3.0 0 0 6      125.183 62.591 0.5762 7.2414
0.8370 3.0 9.0 2 0 5      133.925 66.963 0.5973 7.5065
0.8293 1.0 3.0 1 0 6      136.513 68.257 0.6029 7.5767
0.8237 2.0 6.0 2 1 4      138.505 69.253 0.6070 7.6280
0.8125 3.0 9.0 2 2 0      142.910 71.455 0.6154 7.7334

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4楼2009-04-03 14:05:34

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