| 查看: 1359 | 回复: 2 | ||
竹外一枝轩银虫 (正式写手)
|
[求助]
麻烦大神帮忙提供JCPDS 44-1246的XRD数据 已有1人参与
|
| 麻烦大神帮忙提供JCPDS 44-1246的XRD数据，非常感谢 |
回复此楼» 猜你喜欢
中南大学易小艺课题组诚招2026申请-考核制博士生
已经有0人回复
-
海南师范大学招收化学博士（光电功能材料课题组招收博士研究生）
已经有10人回复
-
无机化学论文润色/翻译怎么收费?
已经有95人回复
-
求助几个团簇的cif
已经有0人回复
-
急求该反应的详细机理
已经有4人回复
竹外一枝轩
银虫 (正式写手)
- 应助: 0 (幼儿园)
- 金币: 2505.1
- 红花: 4
- 帖子: 548
- 在线: 321.1小时
- 虫号: 1385404
- 注册: 2011-08-31
- 性别: GG
- 专业: 配位化学
2楼2018-04-14 15:12:15
kaifeng838
铜虫 (正式写手)
- 应助: 95 (初中生)
- 金币: 463.2
- 散金: 5792
- 红花: 25
- 帖子: 610
- 在线: 852.7小时
- 虫号: 549036
- 注册: 2008-04-20
- 性别: GG
- 专业: 无机材料化学
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
竹外一枝轩: 金币+20, ★★★★★最佳答案, 非常感谢！ 2018-04-16 16:57:03
感谢参与，应助指数 +1
竹外一枝轩: 金币+20, ★★★★★最佳答案, 非常感谢！ 2018-04-16 16:57:03
|
PDF#44-1246: QM=Indexed(I); d=Diffractometer; I=Diffractometer Bismuth Bi Gray Radiation=CuKa1 Lambda=1.54056 Filter=Graph Calibration=Internal(Si) 2T=22.467-119.194 I/Ic(RIR)=2.57 Ref: Sailer, R., McCarthy, G., North Dakota State University, Fargo, North Dakota, USA. Rhombohedral - Powder Diffraction, R-3m (166) Z=6 mp= CELL: 4.547 x 4.547 x 11.8616 <90.0 x 90.0 x 120.0> P.S=hR2 (As) Density(c)=9.804 Density(m)=9.80A Mwt=208.98 Vol=212.39 F(30)=60.4(.0166,30/0) Ref: Ibid. Strong Lines: 3.28/X 2.27/3 2.37/3 1.87/1 1.44/1 1.49/1 1.65/1 3.95/1 1.98/1 1.97/1 NOTE: Sample was obtained from Fisher Scientific Company. Average relative standard deviation in intensity for the ten strongest reflections for three specimen mounts = 8.3%. Validated by a calculated pattern. To replace 00-005-0519. 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 22.467 3.9540 6.0 ( 0 0 3) 11.234 0.1265 1.5891 23.790 3.7370 2.0 ( 1 0 1) 11.895 0.1338 1.6813 27.165 3.2800 100.0 ( 0 1 2) 13.582 0.1524 1.9156 37.949 2.3690 27.0 ( 1 0 4) 18.975 0.2111 2.6523 39.618 2.2730 29.0 ( 1 1 0) 19.809 0.2200 2.7643 44.553 2.0320 5.0 ( 0 1 5) 22.276 0.2461 3.0921 45.872 1.9766 6.0 ( 0 0 6) 22.936 0.2530 3.1788 46.007 1.9711 6.0 ( 1 1 3) 23.003 0.2537 3.1877 46.729 1.9423 <1 ( 0 2 1) 23.365 0.2574 3.2349 48.689 1.8686 13.0 ( 2 0 2) 24.345 0.2676 3.3625 55.640 1.6505 7.0 ( 0 2 4) 27.820 0.3029 3.8068 59.324 1.5565 3.0 ( 1 0 7) 29.662 0.3212 4.0367 61.119 1.5150 1.0 ( 2 0 5) 30.560 0.3300 4.1473 62.174 1.4918 8.0 ( 1 1 6) 31.087 0.3352 4.2118 62.887 1.4766 1.0 ( 2 1 1) 31.444 0.3386 4.2552 64.496 1.4436 10.0 ( 1 2 2) 32.248 0.3464 4.3524 67.443 1.3875 2.0 ( 0 1 8) 33.722 0.3604 4.5284 70.764 1.3303 5.0 ( 2 1 4) 35.382 0.3759 4.7231 71.532 1.3179 1.0 ( 0 0 9) 35.766 0.3794 4.7676 71.865 1.3126 2.0 ( 3 0 0) 35.933 0.3809 4.7868 73.706 1.2843 1.0 ( 0 2 7) 36.853 0.3893 4.8923 75.316 1.2608 <1 ( 1 2 5) 37.658 0.3966 4.9835 76.399 1.2456 <1 ( 3 0 3) 38.199 0.4014 5.0443 81.145 1.1843 <1 ( 2 0 8) 40.572 0.4222 5.3054 84.978 1.1404 1.0 ( 1 1 9) 42.489 0.4384 5.5096 85.320 1.1367 1.0 ( 2 2 0) 42.660 0.4399 5.5276 85.404 1.1358 1.0 ( 1 0 10) 42.702 0.4402 5.5319 87.079 1.1182 <1 ( 2 1 7) 43.540 0.4471 5.6190 89.565 1.0935 1.0 ( 3 0 6) 44.782 0.4572 5.7459 89.669 1.0925 <1 ( 2 2 3) 44.835 0.4577 5.7512 91.638 1.0741 1.0 ( 3 1 2) 45.819 0.4655 5.8497 94.331 1.0504 <1 ( 1 2 8) 47.165 0.4760 5.9817 95.562 1.0401 <1 ( 0 1 11) 47.781 0.4807 6.0409 97.465 1.0248 1.0 ( 1 3 4) 48.733 0.4879 6.1311 98.576 1.0162 <1 ( 0 2 10) 49.288 0.4920 6.1830 101.909 0.9918 <1 ( 3 1 5) 50.955 0.5041 6.3351 102.388 0.9885 <1 ( 0 0 12) 51.194 0.5058 6.3565 102.824 0.9855 <1 ( 2 2 6) 51.412 0.5074 6.3760 104.963 0.9712 <1 ( 0 4 2) 52.481 0.5148 6.4698 109.066 0.9458 <1 ( 2 0 11) 54.533 0.5287 6.6435 111.063 0.9343 <1 ( 4 0 4) 55.531 0.5352 6.7249 111.833 0.9300 <1 ( 3 0 9) 55.917 0.5376 6.7558 112.261 0.9277 <1 ( 2 1 10) 56.131 0.5390 6.7729 114.087 0.9180 <1 ( 1 3 7) 57.044 0.5447 6.8444 115.804 0.9093 <1 ( 0 4 5) 57.902 0.5499 6.9101 116.367 0.9065 <1 ( 1 1 12) 58.183 0.5516 6.9313 119.194 0.8931 <1 ( 2 3 2) 59.597 0.5599 7.0353 |
3楼2018-04-16 10:23:36