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求助各位虫友谁能提供JCPDS 45-0339这张pdf卡片，不胜感激！！邮箱zhangzerong@muncs.org 发自小木虫Android客户端 |
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2楼2017-12-27 18:53:28
【答案】应助回帖
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PDF#45-0339: QM=Star(S); d=Diffractometer; I=Diffractometer Sodium Calcium Phosphate Ca10 Na ( P O4 )7 White Radiation=CuKa1 Lambda=1.540598 Filter=Quartz Calibration=External(Si) 2T=10.868-67.474 I/Ic(RIR)=1.0 Ref: Lazoryak, B., Morozov, V., Novomlinsky, L., Khasanov, S., Moscow State Univ., Russia. ICDD Grant-in-Aid (1993) Rhombohedral - (Unknown), R3c (161) Z=6 mp=>1500 CELL: 10.4402 x 10.4402 x 37.3034 <90.0 x 90.0 x 120.0> P.S=hR92 (?) Density(c)=3.080 Density(m)=3.020 Mwt=1088.59 Vol=3521.25 F(30)=252.6(.0031,38/0) Ref: Oralkov, S., Lazoryak, B. Zh. Neorg. Khim., v33 p73 (1988) Strong Lines: 2.88/X 2.61/6 3.21/6 1.72/3 1.93/3 3.45/2 2.76/2 1.90/2 5.22/2 1.88/2 NOTE: Prepared by heating a mixture of Ca3 ( P O4 )2, Na2 C O3 and ( N H4 )2 H P O4 at 950-1000 C for 40 hours in Al2 O3 foil. Specimen was provided by Lazoryak, B., Morozov, V., Chemistry Dept., Moscow State Univ., Russia. Chemical analysis (wt.%): CaO 51.52, Na2 O 2.87, P2 O5 45.63. Pattern taken at 24(1) C. 2-Theta d(?) I(f) ( h k l) Theta 1/(2d) 2pi/d n^2 10.868 8.1342 8.0 ( 0 1 2) 5.434 0.0615 0.7724 13.631 6.4910 13.0 ( 1 0 4) 6.815 0.0770 0.9680 14.236 6.2164 3.0 ( 0 0 6) 7.118 0.0804 1.0107 16.975 5.2190 16.0 ( 1 1 0) 8.487 0.0958 1.2039 18.417 4.8135 2.0 ( 1 1 3) 9.208 0.1039 1.3053 20.198 4.3927 5.0 ( 2 0 2) 10.099 0.1138 1.4304 21.423 4.1442 1.0 ( 0 1 8) 10.712 0.1206 1.5161 21.834 4.0672 11.0 ( 0 2 4) 10.917 0.1229 1.5449 22.226 3.9963 2.0 ( 1 1 6) 11.113 0.1251 1.5723 25.813 3.4485 23.0 ( 1 0 10) 12.907 0.1450 1.8220 26.169 3.4024 4.0 ( 2 1 1) 13.085 0.1470 1.8467 26.497 3.3611 8.0 ( 1 2 2) 13.249 0.1488 1.8694 27.457 3.2457 6.0 ( 1 1 9) 13.729 0.1541 1.9359 27.457 3.2457 6.0 ( 2 0 8) 13.729 0.1541 1.9359 27.783 3.2083 55.0 ( 2 1 4) 13.892 0.1558 1.9584 28.693 3.1086 1.0 ( 0 0 12) 14.347 0.1608 2.0212 29.620 3.0134 13.0 ( 3 0 0) 14.810 0.1659 2.0851 31.054 2.8775 100.0 ( 2 1 7) 15.527 0.1738 2.1836 31.054 2.8775 100.0 ( 0 2 10) 15.527 0.1738 2.1836 32.453 2.7566 22.0 ( 1 2 8) 16.227 0.1814 2.2794 33.003 2.7118 9.0 ( 3 0 6) 16.502 0.1844 2.3169 33.520 2.6712 7.0 ( 1 1 12) 16.760 0.1872 2.3522 34.333 2.6098 64.0 ( 2 2 0) 17.167 0.1916 2.4075 35.094 2.5549 11.0 ( 2 2 3) 17.547 0.1957 2.4592 35.598 2.5199 11.0 ( 2 1 10) 17.799 0.1984 2.4934 35.868 2.5015 4.0 ( 1 3 1) 17.934 0.1999 2.5117 37.095 2.4216 <1 ( 1 3 4) 18.548 0.2065 2.5947 37.335 2.4065 10.0 ( 2 2 6) 18.668 0.2078 2.6109 37.820 2.3768 6.0 ( 3 1 5) 18.910 0.2104 2.6435 39.215 2.2954 <1 ( 2 0 14) 19.608 0.2178 2.7373 39.892 2.2580 13.0 ( 1 0 16) 19.946 0.2214 2.7826 40.132 2.2450 4.0 ( 1 1 15) 20.066 0.2227 2.7987 40.821 2.2087 <1 ( 2 2 9) 20.410 0.2264 2.8447 40.821 2.2087 <1 ( 3 1 8) 20.410 0.2264 2.8447 41.052 2.1968 13.0 ( 4 0 4) 20.526 0.2276 2.8601 41.703 2.1640 11.0 ( 3 0 12) 20.851 0.2311 2.9035 42.997 2.1019 1.0 ( 1 2 14) 21.498 0.2379 2.9893 43.444 2.0813 5.0 ( 1 3 10) 21.722 0.2402 3.0189 43.641 2.0723 7.0 ( 0 0 18) 21.820 0.2413 3.0320 43.641 2.0723 7.0 ( 0 2 16) 21.820 0.2413 3.0320 43.879 2.0616 5.0 ( 2 3 2) 21.939 0.2425 3.0477 44.505 2.0341 8.0 ( 0 4 8) 22.252 0.2458 3.0890 44.719 2.0248 4.0 ( 3 2 4) 22.359 0.2469 3.1031 44.916 2.0164 2.0 ( 3 1 11) 22.458 0.2480 3.1160 45.327 1.9991 7.0 ( 2 2 12) 22.663 0.2501 3.1430 45.956 1.9732 1.0 ( 4 1 0) 22.978 0.2534 3.1843 46.566 1.9487 2.0 ( 4 1 3) 23.283 0.2566 3.2242 46.961 1.9333 25.0 ( 3 2 7) 23.480 0.2586 3.2500 46.961 1.9333 25.0 ( 4 0 10) 23.480 0.2586 3.2500 47.962 1.8952 17.0 ( 2 3 8) 23.981 0.2638 3.3153 48.362 1.8805 15.0 ( 4 1 6) 24.181 0.2659 3.3413 49.884 1.8266 6.0 ( 0 1 20) 24.942 0.2737 3.4398 50.292 1.8127 5.0 ( 3 2 10) 25.146 0.2758 3.4661 50.679 1.7998 8.0 ( 5 0 2) 25.339 0.2778 3.4910 51.239 1.7814 5.0 ( 4 1 9) 25.620 0.2807 3.5271 51.436 1.7751 8.0 ( 0 5 4) 25.718 0.2817 3.5396 51.612 1.7694 <1 ( 2 3 11) 25.806 0.2826 3.5509 52.552 1.7400 4.0 ( 3 3 0) 26.276 0.2874 3.6110 53.068 1.7243 32.0 ( 2 0 20) 26.534 0.2900 3.6439 53.625 1.7076 11.0 ( 1 3 16) 26.813 0.2928 3.6794 53.625 1.7076 11.0 ( 3 0 18) 26.813 0.2928 3.6794 53.805 1.7024 2.0 ( 2 1 19) 26.902 0.2937 3.6908 54.374 1.6859 7.0 ( 5 0 8) 27.187 0.2966 3.7269 54.555 1.6807 2.0 ( 2 4 4) 27.277 0.2975 3.7383 54.736 1.6756 <1 ( 3 3 6) 27.368 0.2984 3.7498 55.088 1.6657 4.0 ( 4 2 5) 27.544 0.3002 3.7721 55.088 1.6657 4.0 ( 4 1 12) 27.544 0.3002 3.7721 56.144 1.6369 5.0 ( 2 3 14) 28.072 0.3055 3.8385 56.508 1.6272 3.0 ( 0 5 10) 28.254 0.3073 3.8614 56.508 1.6272 3.0 ( 2 4 7) 28.254 0.3073 3.8614 56.673 1.6228 3.0 ( 4 0 16) 28.337 0.3081 3.8717 56.673 1.6228 3.0 ( 2 2 18) 28.337 0.3081 3.8717 57.388 1.6043 6.0 ( 4 2 8) 28.694 0.3117 3.9165 57.388 1.6043 6.0 ( 3 3 9) 28.694 0.3117 3.9165 57.566 1.5998 4.0 ( 5 1 4) 28.783 0.3125 3.9276 58.058 1.5874 2.0 ( 0 2 22) 29.029 0.3150 3.9582 59.452 1.5534 8.0 ( 5 1 7) 29.726 0.3219 4.0447 59.452 1.5534 8.0 ( 2 4 10) 29.726 0.3219 4.0447 59.609 1.5497 10.0 ( 3 2 16) 29.805 0.3226 4.0544 59.785 1.5456 1.0 ( 4 1 15) 29.893 0.3235 4.0653 60.305 1.5335 3.0 ( 1 5 8) 30.153 0.3261 4.0973 60.952 1.5187 5.0 ( 2 1 22) 30.476 0.3292 4.1371 61.485 1.5069 4.0 ( 6 0 0) 30.743 0.3318 4.1697 61.961 1.4964 <1 ( 5 0 14) 30.981 0.3341 4.1988 61.961 1.4964 <1 ( 3 1 20) 30.981 0.3341 4.1988 62.298 1.4891 2.0 ( 5 1 10) 31.149 0.3358 4.2194 62.489 1.4850 1.0 ( 4 3 1) 31.245 0.3367 4.2310 63.306 1.4678 5.0 ( 4 3 4) 31.653 0.3406 4.2806 63.463 1.4646 <1 ( 1 5 11) 31.732 0.3414 4.2901 63.463 1.4646 <1 ( 6 0 6) 31.732 0.3414 4.2901 63.796 1.4577 1.0 ( 3 4 5) 31.898 0.3430 4.3103 64.292 1.4477 1.0 ( 5 2 0) 32.146 0.3454 4.3402 64.746 1.4386 3.0 ( 0 4 20) 32.373 0.3476 4.3675 65.238 1.4289 3.0 ( 0 5 16) 32.619 0.3499 4.3971 65.238 1.4289 3.0 ( 4 1 18) 32.619 0.3499 4.3971 65.399 1.4258 <1 ( 3 2 19) 32.699 0.3507 4.4067 65.399 1.4258 <1 ( 3 3 15) 32.699 0.3507 4.4067 65.898 1.4162 3.0 ( 3 4 8) 32.949 0.3530 4.4366 66.224 1.4101 8.0 ( 5 2 6) 33.112 0.3546 4.4560 67.474 1.3869 6.0 ( 2 3 20) 33.737 0.3605 4.5303 |
3楼2018-01-02 19:52:47
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