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Mass Spectrometry for the Novice 作者John Greaves and John Roboz 页数306 出版社 CRC press International Standard Book Number-13: 978-1-4200-9420-6 (eBook - PDF) Contents List of Figures......................................................................................................... xiii List of Tables............................................................................................................xix Acknowledgments....................................................................................................xxi About the Authors................................................................................................. xxiii Abbreviations..........................................................................................................xxv To the Reader.........................................................................................................xxix Chapter 1 An Overview.........................................................................................1 1.1 A Brief History...........................................................................1 1.2 Definitions Concerning Instruments, Mass, m/z, and Ions........2 1.3 Components of Instruments and Their Functions.................... 11 1.3.1 Sample Introduction.................................................... 11 1.3.2 Ion Sources.................................................................. 13 1.3.3 Mass Analyzers........................................................... 17 1.3.4 Ion Current Detectors.................................................. 21 1.3.5 Vacuum Systems.........................................................22 1.3.6 Data Systems...............................................................23 1.4 Definitions Concerning Instrument Performance....................23 1.5 Definitions Concerning Applications.......................................26 1.6 Information from Mass Spectra...............................................28 1.7 Diversity and Scope of Applications........................................ 31 Chapter 2 Instrumentation................................................................................... 35 2.1 Sample Introduction.................................................................37 2.1.1 Pure Samples or Simple Mixtures...............................37 2.1.1.1 Introduction of Gases and Volatile Liquids Using Batch Inlets..........................37 2.1.1.2 Semipermeable Polymer Membrane Inlets.... 38 2.1.1.3 Direct (Static) Insertion Probes...................38 2.1.2 Chromatographic Separation of Complex Mixtures...39 2.1.2.1 Gas Chromatography–Mass Spectrometry (GC-MS)...............................40 2.1.2.2 Liquid Chromatography–Mass Spectrometry (LC-MS)................................ 43 2.1.2.3 Capillary Electrophoresis (CE).................... 45 2.2 Ion Sources and Methods of Ionization.................................... 45 2.2.1 Electron Ionization (EI)..............................................49 2.2.2 Soft Ionization............................................................. 52 2.2.2.1 Chemical Ionization (CI)............................. 53 2.2.2.2 Electrospray Ionization (ESI)......................56 ? 2014 Taylor & Francis Group, LLC viii Contents 2.2.2.3 Atmospheric Pressure Chemical Ionization (APCI)........................................ 61? 发自小木虫Android客户端 |
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