| ²é¿´: 601 | »Ø¸´: 13 | |||
| µ±Ç°Ö÷ÌâÒѾ´æµµ¡£ | |||
| µ±Ç°Ö»ÏÔʾÂú×ãÖ¸¶¨Ìõ¼þµÄ»ØÌû£¬µã»÷ÕâÀï²é¿´±¾»°ÌâµÄËùÓлØÌû | |||
guohs2004½ð³æ (СÓÐÃûÆø)
|
[½»Á÷]
ÇóÖúXPS±íÕ÷½ð±íÃæ×é×°·½ÃæÎÊÌ⣡
|
||
|
Õæ³ÏÇë½ÌXPS·½Ãæ¾Ñé·á¸»µÄר¼Ò£¡ ×î½üÔÚ½ð»ùµ×±íÃæÉϽøÐвã²ã×é×°£¬ÏëÓÃXPS½øÐзÖÎö±íÕ÷×é×°Çé¿ö¡£Ëù²âµÄΪS2p, N1s, O1s, ºÍC1sÇø¡£ Ä¿µÄÊÇ£º 1£©ÒÔS2p·åµÄ³öÏÖ±íÃ÷Au-S¼üµÄÐγɣ» 2£©ÒÔC1s·å×÷ΪBE²ÎÕÕ£» 3£©ÒÔN1sÇøÓÃÓÚÁ˽â-NH2ºÍ-N-N=N-½á¹¹µÄ´æÔÚ£¬ÒÔÖ¤Ã÷µÚ¶þ²ãÊÇ·ñ×é×°ÉÏÈ¥¡£ 4£©ÒÔO1sÓÃÓÚÖ¤Ã÷µÚ¶þ²ã³É¹¦×é×°Óë·ñ£¬ÒòΪµÚÒ»²ãµÄ·Ö×ÓÖв»º¬ÓÐOµ«º¬N£¬¶øµÚ¶þ²ãÖÐÓÐ-NH2ºÍ-COOH»ù¡£ ½á¹ûΪ£º 1£©ÓÐS2p·å£¬Ö¤Ã÷µÚÒ»²ã³É¹¦×é×°¡£ 2£©N1sÇøÓÐ-NH2µÄ399.4eV·å³öÏÖ£¬ËµÃ÷µÚÒ»²ã×é×°³É¹¦£»µ«×é×°µÚ¶þ²ãºó£¬³ý¸Ã·åÍâÔö¼Ó402eV£¬403eV£¬405eV×óÓҵķ塣 3£©Î´ÐÞÊεĴ¿½ð±íÃæÓÐÃ÷ÏÔO1sºÍC1s·å£¬µ«×é×°ºó¸ÃÁ½Çø¶Ô¾Í·åÔöǿԼ1±¶ÒÔÉÏ£¬·åλÄÑÒÔÅж¨ÊÇ·ñÒÆ¶¯¡£ Çë½ÌµÄÎÊÌâÊÇ£º 1£©ÓÉÓÚδÐÞÊεĴ¿½ð±íÃæÒ²ÓÐÃ÷ÏÔO1sºÍC1s·å£¬ËùÒÔÏëÒÔ×é×°ºóµÄÐźſ۳ýδÐÞÊεĴ¿½ð±íÃæµÄ¶ÔÓ¦±³¾°Ðźţ¬È»ºóÔÙ½øÐзַåÄâºÏ£¬ÇëÎÊÕâÖÖ´¦Àí·½Ê½ÊÇ·ñÕýÈ·£¿ 2£©×é×°µÚ¶þ²ãºó£¬N1sÇøÔö¼ÓµÄ405eV×óÓҵķåÓ¦¸ÃÈçºÎ½âÊÍ£¬ÎÒ²éÁËhttp://srdata.nist.gov/xps/ºÍhttp://www.lasurface.com/database/spectrexps.phpÉÏÃæµÄ×ÊÁÏ£¬Ã»Óз¢ÏÖÓжԸ÷åµÄ½âÊÍ¡£ 3£©µÚ¶þ²ãÖеÄ-COOH»ùÖеÄÁ½¸öOÔÚO1sÇøÖеķåÇ¿¶ÈÓ¦¸ÃÊÇÏàͬ»¹ÊÇ»áÓÐÇø±ð£¿ÓÐÇø±ðµÄ»°Äĸö»á¸ßЩ£¿ Çë»Ø´ðʱ×îºÃÄܸ½ÉÏÏàÓ¦ÎÄÏ×£¬¼±Ðèר¼ÒµÄ°ïÖú£¡ÖÔÐĸÐл£¡ |
» ²ÂÄãϲ»¶
Çóµ÷¼Á
ÒѾÓÐ3È˻ظ´
265Çóµ÷¼Á
ÒѾÓÐ4È˻ظ´
085700×ÊÔ´Óë»·¾³308Çóµ÷¼Á
ÒѾÓÐ6È˻ظ´
Ò»Ö¾Ô¸¼ªÁÖ´óѧ²ÄÁÏѧ˶321Çóµ÷¼Á
ÒѾÓÐ12È˻ظ´
286·ÖÈ˹¤ÖÇÄÜרҵÇëÇóµ÷¼ÁÔ¸Òâ¿ç¿¼£¡
ÒѾÓÐ3È˻ظ´
329Çóµ÷¼Á
ÒѾÓÐ5È˻ظ´
ÉêÇë»Ø¸åÑÓÆÚÒ»¸öÔ£¬±à¼Í¬ÒâÁË¡£µ«ÏµÍ³ÉϵÄʱ¼äû±ä£¬¸ø±à¼ÓÖдÓʼþÁË£¬Ã»»Ø¸´
ÒѾÓÐ4È˻ظ´
²ÄÁÏѧ˶318Çóµ÷¼Á
ÒѾÓÐ5È˻ظ´
Ò»Ö¾Ô¸Öйúº£Ñó´óѧ£¬ÉúÎïѧ£¬301·Ö£¬Çóµ÷¼Á
ÒѾÓÐ6È˻ظ´
081700»¯¹¤Ñ§Ë¶µ÷¼Á
ÒѾÓÐ3È˻ظ´
guohs2004
½ð³æ (СÓÐÃûÆø)
- Ó¦Öú: 0 (Ó×¶ùÔ°)
- ½ð±Ò: 1203.5
- É¢½ð: 480
- ºì»¨: 1
- Ìû×Ó: 289
- ÔÚÏß: 50.5Сʱ
- ³æºÅ: 347012
- ×¢²á: 2007-04-15
- רҵ: ÑùƷǰ´¦Àí·½·¨Óë¼¼Êõ
9Â¥2009-01-05 09:45:18
guohs2004
½ð³æ (СÓÐÃûÆø)
- Ó¦Öú: 0 (Ó×¶ùÔ°)
- ½ð±Ò: 1203.5
- É¢½ð: 480
- ºì»¨: 1
- Ìû×Ó: 289
- ÔÚÏß: 50.5Сʱ
- ³æºÅ: 347012
- ×¢²á: 2007-04-15
- רҵ: ÑùƷǰ´¦Àí·½·¨Óë¼¼Êõ
4Â¥2008-12-19 09:37:52
guohs2004
½ð³æ (СÓÐÃûÆø)
- Ó¦Öú: 0 (Ó×¶ùÔ°)
- ½ð±Ò: 1203.5
- É¢½ð: 480
- ºì»¨: 1
- Ìû×Ó: 289
- ÔÚÏß: 50.5Сʱ
- ³æºÅ: 347012
- ×¢²á: 2007-04-15
- רҵ: ÑùƷǰ´¦Àí·½·¨Óë¼¼Êõ
5Â¥2008-12-19 14:08:17
guohs2004
½ð³æ (СÓÐÃûÆø)
- Ó¦Öú: 0 (Ó×¶ùÔ°)
- ½ð±Ò: 1203.5
- É¢½ð: 480
- ºì»¨: 1
- Ìû×Ó: 289
- ÔÚÏß: 50.5Сʱ
- ³æºÅ: 347012
- ×¢²á: 2007-04-15
- רҵ: ÑùƷǰ´¦Àí·½·¨Óë¼¼Êõ
6Â¥2008-12-21 21:00:03













»Ø¸´´ËÂ¥

