| 查看: 1486 | 回复: 4 | ||
[求助]
高价求助Cr-MIL-88B的合成方法 已有1人参与
|
高价求助Cr-MIL-88B的合成方法! |
回复此楼» 猜你喜欢
江西科技师范大学物理化学课题组接收调剂生，12点开启，速来
已经有0人回复
-
【2026 考研调剂】哈尔滨工程大学 招收学硕调剂生（英语一、数学一）
已经有0人回复
-
无机化学论文润色/翻译怎么收费?
已经有99人回复
-
四川轻化工大学化学与环境工程学院 付昱教授课题组招收调剂硕士研究生
已经有11人回复
-
大连化物所招收有机背景的博士候选人
已经有0人回复
-
在MOF中，有没有羧基参加配位的情况
已经有2人回复
-
招2026年入学上海交通大学博士生，急！！！
已经有1人回复
-
理论计算合作
已经有0人回复
那抹国防绿
新虫 (正式写手)
- 应助: 0 (幼儿园)
- 金币: 1176.8
- 散金: 90
- 红花: 7
- 帖子: 329
- 在线: 59.3小时
- 虫号: 2134821
- 注册: 2012-11-19
- 性别: MM
- 专业: 配位化学
2楼2016-10-01 19:30:25
3楼2016-10-02 19:44:07
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ...
感谢参与，应助指数 +1
hanzhen77: 金币+100, ★★★很有帮助, 多谢了 2016-10-05 15:40:54
感谢参与，应助指数 +1
hanzhen77: 金币+100, ★★★很有帮助, 多谢了 2016-10-05 15:40:54
|
a mixture of chromium chloride (CrCl3·6H2O: 70 mg, 0.4 mmol), terephthalic acid (1,4-BDC, 66 mg, 0.4 mmol), hydrofluoric acid (HF, 1 mmol), and N,N-dimethylformamide (DMF, 5.0 mL) was placed in a Teflon autoclave and heated in a conventional oven at 2108C for 24 h. The resulting powder sample was collected by filtration, washed with purified DMF, and dried at RT. Prior to the application, the MIL-88B(Cr) samples were calcined overnight in air at 1508C to evacuate the solvent. Yung-Han Shih, Sheng-Han Lo, Ni-Shin Yang, Brenda Singco, Yi-Jie Cheng, Cheng-You Wu, I-Hsin Chang, Hsi- Ya Huang,* and Chia-Her Lin*, ChemPlusChem, Volume 77, Issue 11, pages 982–986, November 2012. |
4楼2016-10-04 13:17:45
【答案】应助回帖
|
a mixture of chromium chloride (CrCl3·6H2O: 70 mg, 0.4 mmol), terephthalic acid (1,4-BDC, 66 mg, 0.4 mmol), hydrofluoric acid (HF, 1 mmol), and N,N-dimethylformamide (DMF, 5.0 mL) was placed in a Teflon autoclave and heated in a conventional oven at 210 oC for 24 h. The resulting powder sample was collected by filtration, washed with purified DMF, and dried at RT. Prior to the application, the MIL-88B(Cr) samples were calcined overnight in air at 150 oC to evacuate the solvent. Yung-Han Shih, Sheng-Han Lo, Ni-Shin Yang, Brenda Singco, Yi-Jie Cheng, Cheng-You Wu, I-Hsin Chang, Hsi- Ya Huang,* and Chia-Her Lin*, ChemPlusChem, Volume 77, Issue 11, pages 982–986, November 2012. |
5楼2016-10-04 13:19:01
20