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xinsuihou木虫 (著名写手)
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[求助]
帮忙翻译一下
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The glycine ethyl ester hydrochloride ，triethylamine and dichloromethanewere taken in a round bottom flask and stirred magnetically for 15 min. at ambient temperature. The aldehyde and anhydrous magnesium sulphate were added and the content was stirred at room temperature for overnight. Completion of the reaction was confirmed by monitoring TLC. The post reaction mixture was filtered and solvent was removed in a rotary evaporator under reduced pressure at room temperature. The thick residue was triturated with ether and the triethylamine-hydrochloride salt was filtered off. The filtrate was concentrated under reduced pressure and cooled to remove remaining part of the salt. The mother liquor was concentrated under reduced pressure to obtain desired aldimine as a reddish-yellow semisolid. 主要是从 The thick residue 翻译，后面这部分不太理解，附上全部翻译 |
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genhunter
至尊木虫 (著名写手)
- 翻译EPI: 387
- 应助: 259 (大学生)
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- 专业: 肿瘤化学药物治疗
【答案】应助回帖
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xinsuihou: 金币+5, ★有帮助 2016-03-28 21:12:04
xinsuihou(fjtony163代发): 金币+5, 代发 2016-04-29 14:16:12
fjtony163: 翻译EPI+1, 代发 2016-04-29 14:16:22
xinsuihou: 金币+5, ★有帮助 2016-03-28 21:12:04
xinsuihou(fjtony163代发): 金币+5, 代发 2016-04-29 14:16:12
fjtony163: 翻译EPI+1, 代发 2016-04-29 14:16:22
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