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412003280木虫 (职业作家)
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[求助]
求助一篇文章的Accession number？
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求助文章的Accession number？ 文章信息 题目：Palladium-Catalyzed Nucleophilic Substitution/C–H Activation/Aromatization Cascade Reaction: One Approach To Construct 6-Unsubstituted Phenanthridines doi：10.1021/acs.joc.5b02145 连接：https://pubs.acs.org/doi/abs/10.1021/acs.joc.5b02145 |
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阿呆呆呆
铁杆木虫 (知名作家)
囧囧虫
- 应助: 23 (小学生)
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【答案】应助回帖
感谢参与，应助指数 +1
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Palladium-Catalyzed Nucleophilic Substitution/C-H Activation/Aromatization Cascade Reaction: One Approach To Construct 6-Unsubstituted Phenanthridines 作者:Han, WY (Han, Wenyong)[ 1 ] ; Zhou, XJ (Zhou, Xiaojian)[ 1 ] ; Yang, SY (Yang, Siyi)[ 1 ] ; Xiang, GY (Xiang, Guangyan)[ 1 ] ; Cui, BD (Cui, Baodong)[ 1 ] ; Chen, YZ (Chen, Yongzheng)[ 1 ] JOURNAL OF ORGANIC CHEMISTRY 卷: 80 期: 22 页: 11580-11587 DOI: 10.1021/acs.joc.5b02145 出版年: NOV 20 2015 查看期刊信息 摘要 A facile and practical palladium-catalyzed nucleophilic substitution/CH activation/aromatization cascade reaction has been developed. A range of 6-unsubstituted phenanthridines could be obtained in moderate to good yields (3185%) with readily prepared N-Ms arylamines and commercially available 2-bromobenzyl bromide derivatives as starting materials. The potential application of the protocol was also demonstrated by the expeditious synthesis of the natural alkaloid trisphaeridine. 关键词 KeyWords Plus  OLYCYCLIC AROMATIC-HYDROCARBONS; INTRAMOLECULAR DIRECT ARYLATION; TRANSITION-METAL-FREE; ONE-POT SYNTHESIS; EFFICIENT SYNTHESIS; NITROGEN-HETEROCYCLES; FUSED PHENANTHRIDINES; EXPEDITIOUS SYNTHESIS; COUPLING REACTION; CYCLIZATION作者信息 通讯作者地址: Han, WY (通讯作者) Zunyi Med Univ, Sch Pharm, Zunyi 563000, Peoples R China. 地址: [ 1 ] Zunyi Med Univ, Sch Pharm, Zunyi 563000, Peoples R China 电子邮件地址:hanwy@zmc.edu.cn; yzchen@zmc.edu.cn 基金资助致谢 基金资助机构 授权号 Science and Technology Department of Guizhou Province 2015GZ18284 QKHRCTD-2014-4002 Education Department of Guizhou Province QJHRCTDZ-2012-03 New Century Excellent Talent of the Ministry of Education NCET-13-1069 查看基金资助信息 出版商 AMER CHEMICAL SOC, 1155 16TH ST, NW, WASHINGTON, DC 20036 USA 类别 / 分类 研究方向:Chemistry Web of Science 类别:Chemistry, Organic 文献信息 文献类型:Article 语种:English 入藏号: WOS:000365462600040 PubMed ID: 26513449 ISSN: 0022-3263 期刊信息 Impact Factor (影响因子): Journal Citation Reports® 其他信息 IDS 号: CX1NJ Web of Science 核心合集中的 "引用的参考文献": 83 Web of Science 核心合集中的 "被引频次": 0 |
2楼2016-03-05 15:41:39
阿呆呆呆
铁杆木虫 (知名作家)
囧囧虫
- 应助: 23 (小学生)
- 贵宾: 1.851
- 金币: 9284.6
- 散金: 76507
- 红花: 229
- 沙发: 171
- 帖子: 5941
- 在线: 2693.6小时
- 虫号: 2147790
- 注册: 2012-11-25
- 性别: GG
- 专业: 中药质量评价
【答案】应助回帖
★ ★ ★ ★ ★
412003280: 金币+5, ★★★★★最佳答案, 速度非常快，谢谢 2016-03-05 18:31:41
心静_依然: LS-EPI+1, 感谢应助 2016-03-05 18:40:46
412003280: 金币+5, ★★★★★最佳答案, 速度非常快，谢谢 2016-03-05 18:31:41
心静_依然: LS-EPI+1, 感谢应助 2016-03-05 18:40:46
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Accession number: 20154801620710 Title: Palladium-Catalyzed Nucleophilic Substitution/C-H Activation/Aromatization Cascade Reaction: One Approach to Construct 6-Unsubstituted Phenanthridines Authors: Han, Wenyong1 Email author hanwy@zmc.edu.cn; Zhou, Xiaojian1; Yang, Siyi1; Xiang, Guangyan1; Cui, Baodong1; Chen, Yongzheng1 Email author yzchen@zmc.edu.cn Author affiliation: 1 School of Pharmacy, Zunyi Medical University, Zunyi, China Corresponding author: Han, Wenyong (hanwy@zmc.edu.cn) Source title: Journal of Organic Chemistry Abbreviated source title: J. Org. Chem. Volume: 80 Issue: 22 Issue date: November 20, 2015 Publication year: 2015 Pages: 11580-11587 Language: English ISSN: 00223263 E-ISSN: 15206904 CODEN: JOCEAH Document type: Journal article (JA) Publisher: American Chemical Society Abstract: A facile and practical palladium-catalyzed nucleophilic substitution/C-H activation/aromatization cascade reaction has been developed. A range of 6-unsubstituted phenanthridines could be obtained in moderate to good yields (31-85%) with readily prepared N-Ms arylamines and commercially available 2-bromobenzyl bromide derivatives as starting materials. The potential application of the protocol was also demonstrated by the expeditious synthesis of the natural alkaloid trisphaeridine. © 2015 American Chemical Society. Number of references: 83 Main heading: Catalysis Controlled terms: Chemical activation Uncontrolled terms: Aryl amines - Cascade reactions - Expeditious synthesis - Nucleophilic substitutions - Palladium-catalyzed Classification code: 802.2 Chemical Reactions DOI: 10.1021/acs.joc.5b02145 Database: Compendex Compilation and indexing terms, © 2016 Elsevier Inc. |
3楼2016-03-05 15:41:49
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