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六月de雨

木虫 (著名写手)

[求助] 固体粉末质子传导率测试装置 已有1人参与

最近想做固体粉末质子传导率方面的实验,看了一些文献,了解了测试方法,但是不知道具体的测试装置是什么样的,有哪位大神做过这方面的实验,可以推荐一下在哪里可以买到测试装置吗?或者如何搭建测试装置?
附上一段文献中看到的测量固体粉末质子传导率的测试方法,求详解?

All pellets were prepared by first grinding the samples into a homogeneous powder with a mortar and pestle. The powders (0.3 g) were then added to a standard 13 mm die, sandwiched between two porous carbon electrodes (Sigracet, GDL 10 BB, 1.222 cm diameter) and pressed at 5,000 kg for 2 min. All pellets were 13 mm in diameter and ranged in thickness from 1.30 to 1.38 mm. Measurements were performed using an impedance and gain-phase analyser (SI model 1260), 1 Hz–1 MHz, with a two-probe electrochemical cell equipped with platinum current collectors and an applied a.c. voltage of 10–100 mV (unless otherwise stated). Measurements were taken in the temperature range of 23 to 150 ℃ in either an anhydrous H2 or D2 atmosphere.
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jiekecheng

铁虫 (小有名气)

【答案】应助回帖

LZ找到测试方法了吗?同求!!
2楼2016-04-19 02:15:06
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余晓云

铜虫 (小有名气)

找到方法了吗
3楼2017-01-04 20:53:18
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