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lo@丹丹@ve金虫 (小有名气)
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[求助]
C3N4沉积镍
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最近想在C3N4上沉积镍，参考下边这篇文献在石墨烯上沉积镍的方法，方法如下： Preparation of GOCNTs.A series of GOCNT samples containing different amounts and lengths of CNTs were prepared. In a typical preparation,2g of sodium dodecyl sulfate (SDS, Merck) was dissolved in 40 mL of DI water. Twenty milliliters of GO dispersion of concentration 5 mg/mL was added into the above solution. The mixture was sonicated for about 20 min. Then, 1.74 g of nickel nitrate hexahydrate (Ni(NO3)2·6H2O, Alfa Aesar) dissolved in 20 mL of DI water was added dropwise under vigorous stirring. The resulting mixture was diluted with DI water to have a total volume of 120 mL and heated to 90 °C under stirring. After 16 h, the mixture was evaporated and dried in air with a Petri dish at 60 °C for 24 h to obtain Ni-loaded GO platelets. 在实验过程中并没有还原剂的存在，想问一下，在这个条件下会有Ni生成么？如果不能，需要加什么还原剂呢？ 参考文献题目：Pillaring Chemically Exfoliated Graphene Oxide with Carbon Nanotubes for Photocatalytic Degradation of Dyes under Visible Light Irradiation 作者：Li Li Zhang, Zhigang Xiong, and X. S. Zhao 参考文献见附件 请教各路大神 前边那个帖子的文献有误，重新上传下，请各位在这个帖子回复，谢谢！ |
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2015-12-06 22:02:07, 3.75 M
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