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lo@丹丹@ve

金虫 (小有名气)

[求助] C3N4沉积镍

最近想在C3N4上沉积镍,参考下边这篇文献在石墨烯上沉积镍的方法,方法如下:
Preparation of GOCNTs.A series of GOCNT samples containing different amounts and lengths of CNTs were prepared. In a typical preparation,2g of sodium dodecyl sulfate (SDS, Merck) was dissolved in 40 mL of DI water. Twenty milliliters of GO dispersion of concentration 5 mg/mL was added into the above solution. The mixture was sonicated for about 20 min. Then, 1.74 g of nickel nitrate hexahydrate (Ni(NO3)2·6H2O, Alfa Aesar) dissolved in 20 mL of DI water was added dropwise under vigorous stirring. The resulting mixture was diluted with DI water to have a total volume of 120 mL and heated to 90 °C under stirring. After 16 h, the mixture was evaporated and dried in air with a Petri dish at 60 °C for 24 h to obtain Ni-loaded GO platelets. 在实验过程中并没有还原剂的存在,想问一下,在这个条件下会有Ni生成么?如果不能,需要加什么还原剂呢?

参考文献题目:Pillaring Chemically Exfoliated Graphene Oxide with Carbon Nanotubes for Photocatalytic Degradation of Dyes under Visible Light Irradiation
作者:Li Li Zhang, Zhigang Xiong, and X. S. Zhao

参考文献见附件

请教各路大神

前边那个帖子的文献有误,重新上传下,请各位在这个帖子回复,谢谢!
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  • 2015-12-06 22:02:07, 3.75 M

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