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IS£¨Internal Standard) ÄÚ±ê MF (matrix factor£©»ùÖÊЧӦÒò×Ó IS normalized MF£ºÄÚ±ê¹éÒ»»¯»ùÖÊЧӦÒò×Ó the IS normalized MF was calculated by dividing the MF of the analyte by the MF of the IS. ´ý²âÎïÓëÄÚ±êµÄMFµÄ±ÈֵΪÄÚ±ê¹éÒ»»¯»ùÖÊЧӦÒò×Ó The stability tests were conducted on the bench-top for 6 h, 3 freeze/thaw cycles, post-preparative for 8 days in the autosampler (set at 10 ?C) and in a freezer set at ?30 ?C for 1 month. Îȶ¨ÐÔÊÔÑ飺 ÊÒÎÂÎȶ¨ÐÔ£ºÊÔÑę́ÉÏ·ÅÖÃ6h ¶³ÈÚÎȶ¨ÐÔ£º3¸ö¶³ÈÚÑ»· ´¦ÀíºóÑùÆ·Îȶ¨ÐÔ£º×Ô¶¯½øÑùÆ÷ÄÚ·ÅÖÃ8Ì죨ijζȣ©¡¢±ùÏäÄÚ·ÅÖÃ1¸öÔ£¨Ä³Î¶ȣ©¡£ Analyte concentrations were calculated using a 1/x2 weighted linear least-square regres-sion analysis of the standard curve. ´ý²âÎïŨ¶ÈÓɱê×¼ÇúÏß¼ÆË㣬ÏßÐÔÄâºÏ£º×îС¶þ³Ë·¨£¬¼ÓȨÒò×Ó1/x^2 ¡£ |
2Â¥2015-11-16 12:47:35
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