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xuxiaodai铁杆木虫 (职业作家)
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[求助]
审稿人让我测CO2或者Ar吸附，不是很理解这俩测试的作用，求帮助已有1人参与
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审稿意见如下： On page 10, (starting in line 48) you ascribe the higher surface area as contribution of mesopores. This might be, but figure 6 also shows the highest amount of pores in the transition area of mesopores to micropores. However, you also have to consider the total amount of these micropores and compare these results with the evolution of mesopores. By skipping this comparison a clear statement is not possible. We would suggest to deliver further measurements in order to calculate the amount of micropores,e.g., by CO2 or Ar adsorption and to include a more detailed discussion on your results. 求大神指导。有人做过CO2或者Ar吸附没？这些测试能得到哪些信息？ |
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2楼2015-11-06 14:50:46
xuxiaodai
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3楼2015-11-06 23:35:04
【答案】应助回帖
感谢参与，应助指数 +1
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就是测BET吧，吸附质换成氩气。一般用氮气，由于氩气比氮气更小，极性也小，更容易进入孔内，可能测试的结果也更好！对于介孔两者差别不大，微孔可能相差稍大。 发自小木虫Android客户端 |
4楼2015-11-07 07:31:30