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qinaiajun木虫 (小有名气)
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[求助]
初次测试薄膜的压汞分析，求高人指点怎么分析平均孔径、孔隙率和孔径分布情况 已有1人参与
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MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Summary Report Penetrometer parameters Penetrometer: 13-0229 3 Bulb, 0.412 Stem, Solid Pen. Constant: 11.117 礚/pF Pen. Weight: 61.7660 g Stem Volume: 0.4120 mL Max. Head Pressure: 4.6800 psia Pen. Volume: 3.6163 mL Assembly Weight: 108.9620 g Hg Parameters Adv. Contact Angle: 130.000 degrees Rec. Contact Angle: 130.000 degrees Hg Surface Tension: 485.000 dynes/cm Hg Density: 13.5335 g/mL User Parameters Param 1: 0.000 Param 2: 0.000 Param 3: 0.000 Low Pressure: Evacuation Pressure: 50 祄Hg Evacuation Time: 5 mins Mercury Filling Pressure: 1.50 psia Equilibration Time: 10 secs High Pressure: Equilibration Time: 10 secs Blank Correction Sample: C:9500DATA 00-910.SMP Blank Correction ID: 13-0229, blank (From Pressure 1.50 to 33000.00 psia) Intrusion Data Summary Total Intrusion Volume = 0.0279 mL/g Total Pore Area = 5.571 m?g Median Pore Diameter (Volume) = 29.5 nm Median Pore Diameter (Area) = 9.4 nm Average Pore Diameter (4V/A) = 20.0 nm Bulk Density at 1.50 psia = 1.1170 g/mL Apparent (skeletal) Density = 1.1529 g/mL Porosity = 3.1113 % Stem Volume Used = 1 % **** Pore Structure Summary Threshold Pressure: 8.34 psia (Calculated) Characteristic length = 21687.1 nm Conductivity formation factor = 0.003 Permeability constant = 0.00442 Permeability = 6.8981 mdarcy BET Surface Area = 230.0000 m?g Pore shape exponent = 1.00 Tortuosity factor = 0.001 Tortuosity = 12.4555 Percolation Fractal dimension = 2.708 Backbone Fractal dimension = 2.741 Mayer Stowe Summary Interstitial porosity = 47.6300 % Breakthrough pressure ratio = 3.3512 Material Compressibility Linear Coefficient = N/A 1/psia Quadratic Coefficient = N/A 1/psia? MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Tabular Report Cumulative Incremental dV/dD Pore Pore Pore Pressure Pore dV/dlogD Pore Volume Volume Volume (psia) Diameter (nm) Volume (mL/g) (mL/g/nm) (mL/g) (mL/g) ------ 1.50 120396.8 0.000e+00 0.000e+00 -0.0000 0.0000 1.99 90767.2 1.017e-02 4.210e-08 0.0012 0.0012 2.99 60455.1 5.647e-03 3.288e-08 0.0022 0.0010 3.99 45310.2 2.987e-03 2.470e-08 0.0026 0.0004 5.49 32953.7 3.602e-03 4.031e-08 0.0031 0.0005 5.99 30191.3 0.000e+00 0.000e+00 0.0031 0.0000 7.48 24178.1 5.167e-03 8.288e-08 0.0036 0.0005 8.48 21319.4 0.000e+00 0.000e+00 0.0036 0.0000 10.47 17269.6 2.723e-03 6.152e-08 0.0039 0.0002 12.97 13942.2 1.341e-03 3.745e-08 0.0040 0.0001 15.96 11335.3 1.386e-03 4.779e-08 0.0041 0.0001 19.98 9052.7 2.550e-03 1.091e-07 0.0044 0.0002 24.97 7244.0 1.289e-03 6.900e-08 0.0045 0.0001 29.96 6037.2 1.574e-03 1.032e-07 0.0046 0.0001 37.39 4837.1 5.305e-03 4.255e-07 0.0051 0.0005 46.34 3903.3 4.762e-03 4.750e-07 0.0056 0.0004 57.27 3157.9 6.368e-03 7.863e-07 0.0062 0.0006 71.03 2546.4 2.932e-03 4.482e-07 0.0064 0.0003 86.30 2095.8 4.767e-03 8.947e-07 0.0068 0.0004 111.70 1619.3 2.532e-03 5.953e-07 0.0071 0.0003 136.25 1327.4 2.548e-03 7.535e-07 0.0073 0.0002 170.88 1058.4 2.959e-03 1.082e-06 0.0076 0.0003 217.14 832.9 3.379e-03 1.559e-06 0.0080 0.0004 267.11 677.1 4.165e-03 2.404e-06 0.0083 0.0004 330.22 547.7 3.829e-03 2.726e-06 0.0087 0.0004 417.17 433.5 1.865e-03 1.658e-06 0.0089 0.0002 516.23 350.4 2.122e-03 2.360e-06 0.0091 0.0002 637.94 283.5 4.052e-03 5.573e-06 0.0095 0.0004 797.89 226.7 2.965e-03 5.069e-06 0.0097 0.0003 987.38 183.2 4.737e-03 1.008e-05 0.0102 0.0004 1197.48 151.0 2.938e-03 7.658e-06 0.0104 0.0002 1497.15 120.8 2.192e-03 7.034e-06 0.0106 0.0002 1895.97 95.4 3.482e-03 1.405e-05 0.0110 0.0004 2348.30 77.0 2.947e-03 1.490e-05 0.0113 0.0003 2893.20 62.5 4.191e-03 2.618e-05 0.0117 0.0004 3591.96 50.4 4.753e-03 3.672e-05 0.0121 0.0004 4489.93 40.3 6.991e-03 6.728e-05 0.0128 0.0007 5586.56 32.4 8.735e-03 1.048e-04 0.0136 0.0008 6882.87 26.3 8.421e-03 1.252e-04 0.0144 0.0008 8581.92 21.1 1.903e-02 3.504e-04 0.0162 0.0018 10581.26 17.1 2.014e-02 4.601e-04 0.0180 0.0018 13181.19 13.7 1.108e-02 3.134e-04 0.0191 0.0011 14776.23 12.2 0.000e+00 0.000e+00 0.0191 0.0000 16374.24 11.0 1.867e-02 6.971e-04 0.0199 0.0008 19973.50 9.1 3.907e-02 1.694e-03 0.0233 0.0034 24991.38 7.2 2.211e-02 1.184e-03 0.0254 0.0022 29994.01 6.0 1.824e-02 1.198e-03 0.0269 0.0014 32995.21 5.5 2.315e-02 1.748e-03 0.0279 0.0010 27297.95 6.6 3.757e-02 2.703e-03 0.0248 -0.0031 21014.59 8.6 2.376e-02 1.363e-03 0.0221 -0.0027 16014.85 11.3 7.657e-03 3.363e-04 0.0212 -0.0009 12415.89 14.6 0.000e+00 0.000e+00 0.0212 0.0000 9616.96 18.8 0.000e+00 0.000e+00 0.0212 0.0000 7322.72 24.7 0.000e+00 0.000e+00 0.0212 0.0000 5708.81 31.7 0.000e+00 0.000e+00 0.0212 0.0000 4304.60 42.0 0.000e+00 0.000e+00 0.0212 0.0000 3307.53 54.7 0.000e+00 0.000e+00 0.0212 0.0000 2609.11 69.3 0.000e+00 0.000e+00 0.0212 0.0000 2000.21 90.4 0.000e+00 0.000e+00 0.0212 0.0000 1503.65 120.3 0.000e+00 0.000e+00 0.0212 0.0000 1201.82 150.5 0.000e+00 0.000e+00 0.0212 0.0000 902.98 200.3 0.000e+00 0.000e+00 0.0212 0.0000 703.10 257.2 0.000e+00 0.000e+00 0.0212 0.0000 501.29 360.8 4.679e-03 6.638e-06 0.0205 -0.0007 403.16 448.6 8.088e-03 8.714e-06 0.0197 -0.0008 303.19 596.5 7.893e-03 6.604e-06 0.0187 -0.0010 242.93 744.5 8.765e-03 5.700e-06 0.0179 -0.0008 192.76 938.3 8.770e-03 4.547e-06 0.0170 -0.0009 148.87 1214.9 7.454e-03 3.023e-06 0.0162 -0.0008 113.06 1599.7 5.806e-03 1.803e-06 0.0155 -0.0007 87.23 2073.4 6.470e-03 1.538e-06 0.0147 -0.0007 69.54 2600.9 2.432e-03 4.539e-07 0.0145 -0.0002 53.20 3399.7 0.000e+00 0.000e+00 0.0145 -0.0000 33.39 5416.2 0.000e+00 0.000e+00 0.0145 -0.0000 18.44 9806.4 0.000e+00 0.000e+00 0.0145 -0.0000 MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Cumulative Intrusion vs Pressure Intrusion for Cycle 1 Pressure (psia) Cumulative Intrusion (mL/g) 1.50223 -1.55738e-006 1.99261 0.00124596 2.9917 0.00224262 3.99168 0.00261675 5.48842 0.00311481 5.99058 0.00311512 7.48046 0.00361349 8.48351 0.00361349 10.473 0.00386265 12.9724 0.00398727 15.9558 0.00411186 19.9789 0.00436085 24.9675 0.00448565 29.9583 0.00461024 37.3906 0.00512085 46.3365 0.00556447 57.2736 0.00615053 71.0282 0.00642462 86.298 0.00682775 111.695 0.00711146 136.253 0.00733138 170.881 0.00762237 217.142 0.00797394 267.107 0.00834853 330.22 0.00870127 417.174 0.0088906 516.227 0.00908692 637.944 0.00945947 797.894 0.00974754 987.378 0.0101859 1197.48 0.0104321 1497.15 0.0106447 1895.97 0.0110018 2348.3 0.0112756 2893.2 0.0116554 3591.96 0.012102 4489.93 0.0127795 5586.56 0.0136085 6882.87 0.0143716 8581.92 0.0161947 10581.3 0.0180269 13181.2 0.0190836 14776.2 0.0190936 16374.2 0.0199263 19973.5 0.0232976 24991.4 0.02545 29994 0.0268956 32995.2 0.0278544 Extrusion for Cycle 1 Pressure (psia) Cumulative Intrusion (mL/g) 32995.2 0.0278544 27297.9 0.0247616 21014.6 0.0220623 16014.9 0.0211587 12415.9 0.0211587 9616.96 0.0211587 7322.72 0.0211587 5708.81 0.0211587 4304.6 0.0211587 3307.53 0.0211587 2609.11 0.0211587 2000.21 0.0211587 1503.65 0.0211587 1201.82 0.0211587 902.977 0.0211587 703.102 0.0211587 501.294 0.0204713 403.164 0.0197061 303.185 0.0187292 242.925 0.0178856 192.755 0.0170045 148.871 0.0161682 113.06 0.0154744 87.2301 0.0147456 69.5396 0.0145062 53.1994 0.0145062 33.3933 0.0145062 18.4434 0.0145062 MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Incremental Intrusion vs Pressure Intrusion for Cycle 1 Pressure (psia) Incremental Intrusion (mL/g) 1.50223 0 1.99261 0.00124751 2.9917 0.000996666 3.99168 0.000374127 5.48842 0.000498064 5.99058 3.08532e-007 7.48046 0.000498373 8.48351 8.30479e-011 10.473 0.000249159 12.9724 0.00012462 15.9558 0.000124587 19.9789 0.000248986 24.9675 0.000124799 29.9583 0.000124593 37.3906 0.000510614 46.3365 0.000443619 57.2736 0.000586055 71.0282 0.000274094 86.298 0.000403132 111.695 0.000283707 136.253 0.000219917 170.881 0.000290989 217.142 0.000351574 267.107 0.000374586 330.22 0.00035274 417.174 0.000189332 516.227 0.000196323 637.944 0.000372547 797.894 0.000288076 987.378 0.000438376 1197.48 0.000246131 1497.15 0.000212634 1895.97 0.00035711 2348.3 0.000273802 2893.2 0.00037983 3591.96 0.000446532 4489.93 0.000677515 5586.56 0.000828984 6882.87 0.000763154 8581.92 0.00182312 10581.3 0.00183215 13181.2 0.00105676 14776.2 9.90423e-006 16374.2 0.000832769 19973.5 0.00337127 24991.4 0.0021524 29994 0.0014456 32995.2 0.000958781 MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Differential Intrusion vs Pore size Intrusion for Cycle 1 Pore size Diameter (nm) Differential Intrusion (mL/g/nm) 120397 0 90767.2 4.21036e-008 60455.1 3.28802e-008 45310.2 2.47031e-008 32953.7 4.03079e-008 30191.3 0 24178.1 8.28803e-008 21319.4 0 17269.6 6.15228e-008 13942.2 3.74526e-008 11335.3 4.77918e-008 9052.73 1.09082e-007 7243.96 6.89967e-008 6037.19 1.03244e-007 4837.14 4.25496e-007 3903.26 4.75029e-007 3157.89 7.86256e-007 2546.36 4.48214e-007 2095.8 8.94734e-007 1619.26 5.95344e-007 1327.41 7.5353e-007 1058.42 1.08176e-006 832.927 1.55916e-006 677.12 2.40417e-006 547.707 2.72568e-006 433.544 1.65845e-006 350.356 2.35999e-006 283.51 5.57319e-006 226.676 5.06874e-006 183.176 1.00775e-005 151.036 7.65827e-006 120.805 7.03367e-006 95.3939 1.40531e-005 77.019 1.49008e-005 62.5132 2.61848e-005 50.3523 3.67187e-005 40.282 6.72785e-005 32.3747 0.000104838 26.2774 0.000125161 21.075 0.000350439 17.0928 0.000460093 13.7213 0.000313441 12.2402 0 11.0456 0.000697137 9.05517 0.00169373 7.23704 0.00118385 6.02999 0.00119763 5.48151 0.00174807 MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Cumulative Pore Area vs Pore size Intrusion for Cycle 1 Pore size Diameter (nm) Cumulative Pore Area (m?g) 120397 0 90767.2 4.72624e-005 60455.1 9.99882e-005 45310.2 0.000128287 32953.7 0.000179198 30191.3 0.000179237 24178.1 0.000252569 21319.4 0.000252569 17269.6 0.000304223 13942.2 0.000336164 11335.3 0.000375595 9052.73 0.000473294 7243.96 0.000534557 6037.19 0.000609607 4837.14 0.000985254 3903.26 0.00139129 3157.89 0.00205527 2546.36 0.00243968 2095.8 0.00313441 1619.26 0.00374534 1327.41 0.0043424 1058.42 0.00531812 832.927 0.00680521 677.12 0.00878971 547.707 0.0110936 433.544 0.0126372 350.356 0.0146408 283.51 0.0193427 226.676 0.0238599 183.176 0.0324167 151.036 0.0383083 120.805 0.0445658 95.3939 0.0577799 77.019 0.0704844 62.5132 0.0922618 50.3523 0.123912 40.282 0.183714 32.3747 0.274991 26.2774 0.379083 21.075 0.687093 17.0928 1.07111 13.7213 1.34547 12.2402 1.34852 11.0456 1.63463 9.05517 2.97637 7.23704 4.03327 6.02999 4.90497 5.48151 5.57128 MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Log Differential Intrusion vs Pore size Intrusion for Cycle 1 Pore size Diameter (nm) Log Differential Intrusion (mL/g) 120397 0 90767.2 0.0101683 60455.1 0.00564697 45310.2 0.00298734 32953.7 0.00360155 30191.3 0 24178.1 0.00516668 21319.4 0 17269.6 0.00272322 13942.2 0.0013407 11335.3 0.00138588 9052.73 0.00254971 7243.96 0.0012892 6037.19 0.0015743 4837.14 0.00530531 3903.26 0.00476186 3157.89 0.00636802 2546.36 0.00293223 2095.8 0.00476684 1619.26 0.00253233 1327.41 0.00254796 1058.42 0.00295873 832.927 0.00337891 677.12 0.00416479 547.707 0.00382922 433.544 0.00186507 350.356 0.00212187 283.51 0.004052 226.676 0.00296489 183.176 0.00473724 151.036 0.00293761 120.805 0.00219222 95.3939 0.00348176 77.019 0.00294655 62.5132 0.00419119 50.3523 0.00475275 40.282 0.0069913 32.3747 0.00873486 26.2774 0.00842105 21.075 0.0190275 17.0928 0.020144 13.7213 0.0110752 12.2402 0 11.0456 0.018673 9.05517 0.0390677 7.23704 0.0221131 6.02999 0.0182423 5.48151 0.0231498 MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Differential Intrusion vs Pore size Intrusion for Cycle 1 Pore size Diameter (nm) Differential Intrusion (mL/g/nm) 120397 0 90767.2 4.21036e-008 60455.1 3.28802e-008 45310.2 2.47031e-008 32953.7 4.03079e-008 30191.3 0 24178.1 8.28803e-008 21319.4 0 17269.6 6.15228e-008 13942.2 3.74526e-008 11335.3 4.77918e-008 9052.73 1.09082e-007 7243.96 6.89967e-008 6037.19 1.03244e-007 4837.14 4.25496e-007 3903.26 4.75029e-007 3157.89 7.86256e-007 2546.36 4.48214e-007 2095.8 8.94734e-007 1619.26 5.95344e-007 1327.41 7.5353e-007 1058.42 1.08176e-006 832.927 1.55916e-006 677.12 2.40417e-006 547.707 2.72568e-006 433.544 1.65845e-006 350.356 2.35999e-006 283.51 5.57319e-006 226.676 5.06874e-006 183.176 1.00775e-005 151.036 7.65827e-006 120.805 7.03367e-006 95.3939 1.40531e-005 77.019 1.49008e-005 62.5132 2.61848e-005 50.3523 3.67187e-005 40.282 6.72785e-005 32.3747 0.000104838 26.2774 0.000125161 21.075 0.000350439 17.0928 0.000460093 13.7213 0.000313441 12.2402 0 11.0456 0.000697137 9.05517 0.00169373 7.23704 0.00118385 6.02999 0.00119763 5.48151 0.00174807 Extrusion for Cycle 1 Pore size Diameter (nm) Differential Intrusion (mL/g/nm) 5.48151 0.00174807 6.62554 0.00270344 8.60657 0.00136257 11.2935 0.000336278 14.5671 0 18.8067 0 24.699 0 31.6815 0 42.0163 0 54.6824 0 69.3201 0 90.4221 0 120.283 0 150.491 0 200.297 0 257.237 0 360.794 6.63808e-006 448.61 8.71356e-006 596.545 6.60393e-006 744.524 5.70046e-006 938.307 4.54694e-006 1214.9 3.02343e-006 1599.72 1.80301e-006 2073.41 1.53849e-006 2600.87 4.53899e-007 3399.73 0 5416.16 0 9806.42 0 MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Log Differential Intrusion vs Pore size Intrusion for Cycle 1 Pore size Diameter (nm) Log Differential Intrusion (mL/g) 120397 0 90767.2 0.0101683 60455.1 0.00564697 45310.2 0.00298734 32953.7 0.00360155 30191.3 0 24178.1 0.00516668 21319.4 0 17269.6 0.00272322 13942.2 0.0013407 11335.3 0.00138588 9052.73 0.00254971 7243.96 0.0012892 6037.19 0.0015743 4837.14 0.00530531 3903.26 0.00476186 3157.89 0.00636802 2546.36 0.00293223 2095.8 0.00476684 1619.26 0.00253233 1327.41 0.00254796 1058.42 0.00295873 832.927 0.00337891 677.12 0.00416479 547.707 0.00382922 433.544 0.00186507 350.356 0.00212187 283.51 0.004052 226.676 0.00296489 183.176 0.00473724 151.036 0.00293761 120.805 0.00219222 95.3939 0.00348176 77.019 0.00294655 62.5132 0.00419119 50.3523 0.00475275 40.282 0.0069913 32.3747 0.00873486 26.2774 0.00842105 21.075 0.0190275 17.0928 0.020144 13.7213 0.0110752 12.2402 0 11.0456 0.018673 9.05517 0.0390677 7.23704 0.0221131 6.02999 0.0182423 5.48151 0.0231498 Extrusion for Cycle 1 Pore size Diameter (nm) Log Differential Intrusion (mL/g) 5.48151 0.0231498 6.62554 0.0375702 8.60657 0.0237595 11.2935 0.00765735 14.5671 0 18.8067 0 24.699 0 31.6815 0 42.0163 0 54.6824 0 69.3201 0 90.4221 0 120.283 0 150.491 0 200.297 0 257.237 0 360.794 0.00467867 448.61 0.00808786 596.545 0.00789301 744.524 0.00876545 938.307 0.0087703 1214.9 0.0074536 1599.72 0.00580598 2073.41 0.00646979 2600.87 0.00243224 3399.73 0 5416.16 0 9806.42 0 MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Difference from reference % volume vs Pore size MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Out of specification % volume vs Pressure MICROMERITICS INSTRUMENT CORPORATION AutoPore IV 9500 V1.07 Serial: 738 Port: 1/1 Page 1 Sample ID: 000-919 Operator: lvtong Submitter: qilu-1# File: C:9500DATA 00-919.SMP LP Analysis Time: 2015-9-22 12:40:17下午 Sample Weight: 0.1570 g HP Analysis Time: 2015-9-22 14:27:15下午 Correction Type: Blank Report Time: 2015-10-21 15:28:34下午 Show Neg. Int: No Differential Intrusion vs Pore size Intrusion for Cycle 1 Pore size Diameter (nm) Differential Intrusion (mL/g/nm) 120397 0 90767.2 4.21036e-008 60455.1 3.28802e-008 45310.2 2.47031e-008 32953.7 4.03079e-008 30191.3 0 24178.1 8.28803e-008 21319.4 0 17269.6 6.15228e-008 13942.2 3.74526e-008 11335.3 4.77918e-008 9052.73 1.09082e-007 7243.96 6.89967e-008 6037.19 1.03244e-007 4837.14 4.25496e-007 3903.26 4.75029e-007 3157.89 7.86256e-007 2546.36 4.48214e-007 2095.8 8.94734e-007 1619.26 5.95344e-007 1327.41 7.5353e-007 1058.42 1.08176e-006 832.927 1.55916e-006 677.12 2.40417e-006 547.707 2.72568e-006 433.544 1.65845e-006 350.356 2.35999e-006 283.51 5.57319e-006 226.676 5.06874e-006 183.176 1.00775e-005 151.036 7.65827e-006 120.805 7.03367e-006 95.3939 1.40531e-005 77.019 1.49008e-005 62.5132 2.61848e-005 50.3523 3.67187e-005 40.282 6.72785e-005 32.3747 0.000104838 26.2774 0.000125161 21.075 0.000350439 17.0928 0.000460093 13.7213 0.000313441 12.2402 0 11.0456 0.000697137 9.05517 0.00169373 7.23704 0.00118385 6.02999 0.00119763 5.48151 0.00174807 Extrusion for Cycle 1 Pore size Diameter (nm) Differential Intrusion (mL/g/nm) 5.48151 0.00174807 6.62554 0.00270344 8.60657 0.00136257 11.2935 0.000336278 14.5671 0 18.8067 0 24.699 0 31.6815 0 42.0163 0 54.6824 0 69.3201 0 90.4221 0 120.283 0 150.491 0 200.297 0 257.237 0 360.794 6.63808e-006 448.61 8.71356e-006 596.545 6.60393e-006 744.524 5.70046e-006 938.307 4.54694e-006 1214.9 3.02343e-006 1599.72 1.80301e-006 2073.41 1.53849e-006 2600.87 4.53899e-007 3399.73 0 5416.16 0 9806.42 0@hwweven |
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