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yangyunking银虫 (初入文坛)
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[求助]
求助一个XRD的pdf卡
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| 求助一个Jade的pdf卡参数，01-075-1140，物质为V6O13。。。。。。。。。。SOS!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!!! |
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gonnow
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【答案】应助回帖
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yangyunking: 金币+2, 博学EPI+1 2015-11-02 08:57:45
yangyunking: 金币+2, 博学EPI+1 2015-11-02 08:57:45
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PDF#71-2235: QM=Calculated; d=Calculated; I=(Unknown) Vanadium Oxide V6O13 Radiation=CuKa1 Lambda=1.5406 Filter= Calibration= 2T=8.875-89.875 I/Ic(RIR)=1.78 Ref: Level-1 PDF Monoclinic, C2/m(12) Z=2 mp= CELL: 11.922 x 3.68 x 10.138 <90.0 x 100.87 x 90.0> P.S= Density(c)=3.905 Density(m)= Mwt= Vol=436.8 Ref: Ibid. Strong Lines: 3.51/X 3.32/8 5.85/5 1.99/4 2.96/4 2.67/3 1.84/3 4.98/3 2-Theta d(?) I(f) ( h k l ) Theta 1/(2d) 2pi/d n^2 8.875 9.9561 28.9 ( 0 0 1) 4.437 0.0502 0.6311 15.122 5.8540 45.5 ( 2 0 0) 7.561 0.0854 1.0733 16.038 5.5218 9.8 (-2 0 1) 8.019 0.0906 1.1379 17.803 4.9781 30.5 ( 0 0 2) 8.901 0.1004 1.2622 18.964 4.6758 5.2 ( 2 0 1) 9.482 0.1069 1.3438 21.117 4.2036 2.0 (-2 0 2) 10.559 0.1189 1.4947 25.349 3.5107 100.0 ( 1 1 0) 12.674 0.1424 1.7897 25.561 3.4821 9.4 ( 2 0 2) 12.780 0.1436 1.8044 26.416 3.3712 3.9 (-1 1 1) 13.208 0.1483 1.8638 26.842 3.3187 75.1 ( 0 0 3) 13.421 0.1507 1.8933 27.389 3.2537 4.2 ( 1 1 1) 13.694 0.1537 1.9311 28.277 3.1534 4.7 (-2 0 3) 14.139 0.1586 1.9925 30.131 2.9635 36.4 (-4 0 1) 15.066 0.1687 2.1202 30.516 2.9270 8.1 ( 4 0 0) 15.258 0.1708 2.1466 31.989 2.7955 5.1 ( 1 1 2) 15.994 0.1789 2.2476 32.401 2.7609 3.0 (-4 0 2) 16.200 0.1811 2.2758 33.487 2.6738 33.3 ( 3 1 0) 16.743 0.1870 2.3499 35.809 2.5055 4.8 ( 3 1 1) 17.904 0.1996 2.5077 35.942 2.4966 7.1 (-3 1 2) 17.971 0.2003 2.5167 36.055 2.4890 7.9 ( 0 0 4) 18.027 0.2009 2.5244 36.148 2.4828 15.0 (-1 1 3) 18.074 0.2014 2.5307 36.887 2.4348 3.2 (-4 0 3) 18.443 0.2054 2.5806 38.330 2.3464 5.8 ( 1 1 3) 19.165 0.2131 2.6778 38.474 2.3379 7.8 ( 4 0 2) 19.237 0.2139 2.6875 40.223 2.2402 2.6 ( 3 1 2) 20.111 0.2232 2.8048 40.423 2.2295 1.9 (-3 1 3) 20.212 0.2243 2.8182 42.003 2.1493 0.1 ( 2 0 4) 21.001 0.2326 2.9234 42.998 2.1018 2.5 (-4 0 4) 21.499 0.2379 2.9894 43.320 2.0869 0.3 (-1 1 4) 21.660 0.2396 3.0107 45.516 1.9912 27.1 ( 0 0 5) 22.758 0.2511 3.1554 45.619 1.9869 39.6 (-6 0 1) 22.810 0.2516 3.1622 46.198 1.9634 1.5 ( 3 1 3) 23.099 0.2547 3.2002 46.449 1.9533 2.6 (-3 1 4) 23.225 0.2560 3.2166 48.334 1.8815 0.1 ( 5 1 1) 24.167 0.2657 3.3395 49.206 1.8502 1.6 ( 6 0 1) 24.603 0.2702 3.3960 49.496 1.8400 30.8 (-6 0 3) 24.748 0.2717 3.4148 50.283 1.8130 0.4 (-4 0 5) 25.142 0.2758 3.4656 50.392 1.8094 0.6 ( 0 2 1) 25.196 0.2763 3.4726 51.120 1.7853 2.3 ( 2 0 5) 25.560 0.2801 3.5194 51.418 1.7756 2.0 (-1 1 5) 25.709 0.2816 3.5385 52.058 1.7553 2.0 ( 2 2 0) 26.029 0.2848 3.5795 52.369 1.7456 0.6 (-2 2 1) 26.184 0.2864 3.5994 52.518 1.7410 0.5 ( 4 0 4) 26.259 0.2872 3.6089 53.015 1.7259 1.9 ( 0 2 2) 26.507 0.2897 3.6406 53.356 1.7156 0.8 ( 3 1 4) 26.678 0.2914 3.6623 53.530 1.7105 5.7 ( 2 2 1) 26.765 0.2923 3.6734 53.646 1.7070 3.8 (-3 1 5) 26.823 0.2929 3.6807 53.917 1.6991 5.7 (-6 0 4) 26.958 0.2943 3.6979 54.181 1.6915 7.2 ( 1 1 5) 27.090 0.2956 3.7147 54.384 1.6856 3.9 (-2 2 2) 27.192 0.2966 3.7276 54.516 1.6818 1.2 (-5 1 4) 27.258 0.2973 3.7359 55.318 1.6594 2.5 ( 0 0 6) 27.659 0.3013 3.7865 56.522 1.6268 0.8 ( 2 2 2) 28.261 0.3073 3.8622 57.197 1.6092 12.0 ( 0 2 3) 28.598 0.3107 3.9045 57.984 1.5892 1.0 ( 5 1 3) 28.992 0.3146 3.9536 58.489 1.5767 5.6 (-4 0 6) 29.244 0.3171 3.9850 59.044 1.5632 7.2 (-4 2 1) 29.522 0.3199 4.0194 59.270 1.5578 4.7 ( 6 0 3) 29.635 0.3210 4.0334 59.795 1.5454 16.6 (-7 1 1) 29.897 0.3235 4.0658 60.279 1.5341 3.5 (-1 1 6) 30.139 0.3259 4.0957 60.408 1.5311 2.6 (-4 2 2) 30.204 0.3266 4.1036 60.778 1.5227 1.4 ( 2 0 6) 30.389 0.3284 4.1264 60.960 1.5186 4.3 ( 4 0 5) 30.480 0.3293 4.1376 61.075 1.5160 2.3 ( 4 2 1) 30.538 0.3298 4.1446 61.473 1.5071 8.2 ( 3 1 5) 30.736 0.3318 4.1689 61.797 1.5000 7.9 (-3 1 6) 30.898 0.3333 4.1888 62.308 1.4889 0.5 (-8 0 1) 31.154 0.3358 4.2200 62.543 1.4839 0.3 (-7 1 3) 31.272 0.3370 4.2343 62.745 1.4796 1.2 ( 0 2 4) 31.373 0.3379 4.2465 63.298 1.4680 3.6 ( 7 1 1) 31.649 0.3406 4.2801 63.515 1.4635 1.9 ( 8 0 0) 31.757 0.3416 4.2932 64.381 1.4459 2.5 (-2 0 7) 32.190 0.3458 4.3455 64.509 1.4433 1.4 (-8 0 3) 32.254 0.3464 4.3532 65.582 1.4223 0.3 ( 0 0 7) 32.791 0.3515 4.4176 66.162 1.4112 8.2 ( 6 0 4) 33.081 0.3543 4.4523 66.696 1.4012 3.2 (-6 0 6) 33.348 0.3568 4.4841 66.883 1.3978 1.7 ( 2 2 4) 33.442 0.3577 4.4952 67.260 1.3908 2.2 ( 7 1 2) 33.630 0.3595 4.5176 67.612 1.3844 1.1 (-4 2 4) 33.806 0.3612 4.5384 67.834 1.3805 0.6 (-8 0 4) 33.917 0.3622 4.5515 69.500 1.3514 10.6 ( 0 2 5) 34.750 0.3700 4.6495 69.579 1.3500 11.9 (-6 2 1) 34.789 0.3704 4.6541 70.223 1.3392 0.5 ( 4 0 6) 35.111 0.3733 4.6916 70.465 1.3352 0.3 ( 3 1 6) 35.233 0.3745 4.7058 70.823 1.3293 0.1 (-3 1 7) 35.412 0.3761 4.7265 71.138 1.3242 0.2 (-7 1 5) 35.569 0.3776 4.7448 72.372 1.3047 0.5 ( 6 2 1) 36.186 0.3832 4.8160 72.553 1.3018 0.9 ( 7 1 3) 36.277 0.3841 4.8264 73.232 1.2914 0.2 (-4 2 5) 36.616 0.3872 4.8653 73.908 1.2813 1.0 ( 2 2 5) 36.954 0.3902 4.9038 74.105 1.2784 1.0 ( 6 0 5) 37.052 0.3911 4.9150 74.751 1.2689 0.5 (-6 0 7) 37.375 0.3940 4.9516 75.884 1.2528 2.7 ( 6 2 2) 37.942 0.3991 5.0154 76.205 1.2483 3.0 (-6 2 4) 38.102 0.4005 5.0334 76.478 1.2445 2.9 ( 0 0 8) 38.239 0.4018 5.0487 76.705 1.2414 1.6 (-2 2 6) 38.353 0.4028 5.0614 77.378 1.2323 2.6 ( 0 2 6) 38.689 0.4058 5.0989 77.808 1.2265 0.2 ( 9 1 0) 38.904 0.4077 5.1228 78.048 1.2234 0.3 (-9 1 3) 39.024 0.4087 5.1360 78.304 1.2200 1.9 ( 1 3 0) 39.152 0.4098 5.1502 78.505 1.2174 1.0 (-8 0 6) 39.252 0.4107 5.1612 78.780 1.2138 0.2 (-1 3 1) 39.390 0.4119 5.1764 79.097 1.2097 5.3 ( 7 1 4) 39.549 0.4133 5.1938 80.086 1.1973 3.3 (-4 2 6) 40.043 0.4176 5.2479 80.314 1.1945 2.1 (-1 1 8) 40.157 0.4186 5.2603 80.606 1.1909 1.8 (-10 0 2) 40.303 0.4199 5.2762 80.736 1.1893 1.2 ( 6 2 3) 40.368 0.4204 5.2832 81.156 1.1842 0.4 (-6 2 5) 40.578 0.4222 5.3060 81.385 1.1814 0.2 ( 5 1 6) 40.693 0.4232 5.3184 81.538 1.1796 0.3 ( 1 3 2) 40.769 0.4239 5.3266 81.850 1.1759 0.2 (-10 0 3) 40.925 0.4252 5.3434 82.246 1.1712 2.7 ( 4 2 5) 41.123 0.4269 5.3647 82.357 1.1699 2.2 ( 3 3 0) 41.178 0.4274 5.3706 82.441 1.1689 1.5 ( 8 0 4) 41.220 0.4277 5.3751 83.156 1.1607 0.1 ( 6 0 6) 41.578 0.4308 5.4133 83.442 1.1574 0.3 (-8 2 1) 41.721 0.4320 5.4285 83.765 1.1538 0.7 (-8 2 2) 41.882 0.4334 5.4456 83.868 1.1526 1.5 ( 1 1 8) 41.934 0.4338 5.4511 84.470 1.1459 0.2 (-10 0 4) 42.235 0.4363 5.4829 84.852 1.1418 2.3 (-7 1 7) 42.426 0.4379 5.5030 85.184 1.1382 1.6 (-9 1 5) 42.592 0.4393 5.5204 85.418 1.1356 0.5 (-8 2 3) 42.709 0.4403 5.5327 85.735 1.1323 0.2 (-8 0 7) 42.867 0.4416 5.5492 86.414 1.1251 0.7 ( 0 2 7) 43.207 0.4444 5.5846 86.545 1.1237 0.5 (-3 3 3) 43.272 0.4449 5.5914 86.895 1.1201 2.6 ( 7 1 5) 43.447 0.4464 5.6095 87.415 1.1148 2.2 (-6 2 6) 43.707 0.4485 5.6363 88.280 1.1061 0.9 ( 0 0 9) 44.140 0.4521 5.6806 88.452 1.1044 0.6 (-10 0 5) 44.226 0.4528 5.6894 89.448 1.0946 0.1 ( 10 0 2) 44.724 0.4568 5.7400 89.875 1.0905 0.1 (-5 3 1) 44.938 0.4585 5.7616 |
2楼2015-10-30 17:00:03
yangyunking
银虫 (初入文坛)
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3楼2015-11-02 08:57:08