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??D???...?@?????C??????????N??????? Friedel-Craft reaction?????? ?????????Y????paper?????????AlCl3 16g (0.12mole)???Anisole 32.454g (0.3mole)??????????????????70???????????Dichloro(phenyl)phosphine 10.7388g (0.06mole)??μ????????????30min???μ?Y???????????????110?淴??8hr??????F??????????????????HCl?????????????(?????????N??AlCl3)???????S??????????????^?V????????????????????????(?@???E?????????N??Anisole)??????????????????@??????N???????????????D???l??????????????????н??S????????????????????????FTIR???????????P-Cl bond(??D??s550??λ??)???F?????MS??????Y????Σ????λ????????????? ?????????????@??????f????????????????????AlCl3 10g (0.075mole)???Anisole 19.4652g (0.18mole)?У???????????????μ?Dichloro(phenyl)phosphine 5.3694g (0.03mole) ?s30min???μ?Y?????S???????У????????oHCl???w?a???????沽?E?t?c????E?????????HCl?_?.... ???????λ??????????x?x??  ???.jpg  С??xIR.jpg |
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