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| Samples are analyzed in a set referred to as an analysis sequence. The sequence begins with calibration verification followed by sample extract analyses. Additional analyses of the verification standard(s) throughout a 12-hour shift are strongly recommended, especially for samples that contain visible concentrations of oily material. A verification standard is also necessary at the end of a set (unless internal standard calibration is used). The sequence ends when the set of samples has been injected or when retention time and/or % difference QC criteria are exceeded. |
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