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维普数据求助 已有1人参与
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| 13C NMR (126 MHz, CDCl3) δ 14.0, 17.1, 17.9, 19.3, 19.9, 20.1, 20.2, 21.4, 24.6, 25.2, 28.1, 28.6, 33.3, 36.5, 38.2, 39.6, 40.0, 40.4, 43.1, 43.7, 56.2, 67.7, 75.9, 124.1, 125.3, 131.9, 132.5, 135.5, 149.2 |
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【答案】应助回帖
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感谢参与，应助指数 +1
莫之俊: 金币+8, ★★★★★最佳答案 2015-06-16 17:26:23
感谢参与，应助指数 +1
莫之俊: 金币+8, ★★★★★最佳答案 2015-06-16 17:26:23
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ergosta-4,6,8(14),22-tetraen-3??-ol C28H42O ?????:75.8% Natural Product Research 1993 3 193-196 The Isolation of Ergosta-4, 6, 8 (14), 22-tetraen-3??-ol from Injured Fruit Bodies of Marasmius oreades Zijie Pang; Olov Sterner Structure 13C NMR ??????? -------------------------------------------------------------------------------- 2 . 5??,6??-epoxy-(22E,24R)-ergosta-8(14),22-diene-3??,7??-diol ?????:72.4% Archives of Pharmacal Research 2002 25 851-855 Cytotoxic ergosterols from paecilomyces sp. J300 Hak Cheol Kwon, Sang Deuk Zee, Sae Yun Cho, Sang Un Choi and Kang Ro Lee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 3 . (3??,5??),(8??,11??)-diepidioxy-ergost-22E-en-12-one C28H42O5 ?????:72.4% Journal of the Chinese Chemical Society 1995 42 97-100 Constituents of Fruit Bodies of Tramete orientalis ??????(Huey-Ling Chen);??????(Hung-Cheh Chiang) Structure 13C NMR ??????? -------------------------------------------------------------------------------- 4 . 5??,6??-epoxy-ergosta-8(14),22-diene-3??,7??-diol C28H44O3 ?????:72.4% Natural product sciences 2011 17 85-89 Cytotoxicity of Ergosterol Derivatives from the Fruiting Bodies of Hygrophorus russula Lee, Ik-Soo; Kim, Jin-Pyo; Na, Min-Kyun; Jung, Hyun-Ju; Min, Byung-Sun; Bae, Ki-Hwan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 5 . 22E,24R-5??,6??-epoxyergosta-8(14),22-diene-3??,7??-diol ?????:72.4% Acta Botanica Boreali-Occidentalia Sinica 2013 33 1473-1477 Chemical Constituents from an Endophytic Fungus Aspergillus sp.12Y03 Isolated from Perilla frutescens GAO Yi, LI Huqiang, ZHANG Zhijun, LI Xiaojun* Structure 13C NMR ??????? -------------------------------------------------------------------------------- 6 . 5-Hydroxy-5??-ergosta-6,8(14)-22-trien-3??-ylacetate C30H46O3 ?????:70% Steroids 2006 71 565-577 Regio and stereoselective oxidations of unsaturated steroidal compounds with H2O2 mediated by CH3ReO3 Francesco P. Ballistreri, Rosa Chillemi, Sebastiano Sciuto, Gaetano A. Tomaselli, Rosa M. Toscano Structure 13C NMR ??????? -------------------------------------------------------------------------------- 7 . (22E,24R)-3??-ureido-ergosta-4,6,8(14),22-tetraene C29H44N2O ?????:68.9% Chemical & Pharmaceutical Bulletin 2001 49(8) 1030-1032 Two New Steroidal Derivatives from the Fruit Body of Chlorophyllum molybdites Kazuko YOSHIKAWA,Mizuho IKUTA, Shigenobu ARIHARA,Eiko MATSUMURA,and Satoshi KATAYAMA Structure 13C NMR ??????? -------------------------------------------------------------------------------- 8 . 5??,6??-epoxy-(22E,24R)-ergosta-8(14),22-diene-3??,7??-diol C28H44O3 ?????:68.9% Chemistry of Natural Compounds 2009 45 759-761 STEROIDS AND OTHER CONSTITUENTS FROMTHE MUSHROOM Armillaria lueo-virens Hui-Yan Xiong, Dong-Qing Fei, Jin-Song Zhou,Chun-Jiang Yang,and Guo-Liang Ma Structure 13C NMR ??????? -------------------------------------------------------------------------------- 9 . 6,9-epoxyergosta-7,22-dien-3-ol ?????:68.9% Acta Botanica Sinica 2002 44 1239-1242 Chemical Constituents of One Species of Endophytic Fungus in Taxus chinensis ZHANGJi-Hui, GUO Shun-Xing YANGJun-Shan, XIAO Pei-Gen Structure 13C NMR ??????? -------------------------------------------------------------------------------- 10 . Stylisterol A C28H46O3 ?????:68.9% Steroids 2005 70 63-70 New polyhydroxylated sterols stylisterols A?CC and a novel 5,19-cyclosterol hatomasterol from the Okinawan marine sponge Stylissa sp. Hidemichi Mitome, Nao Shirato, Ayako Hoshino, Hiroaki Miyaoka, Yasuji Yamada, Rob W.M. Van Soest Structure 13C NMR ??????? -------------------------------------------------------------------------------- 11 . 5??,8??-epidioxyergosta-6,22E-dien-3??-ol ?????:68.9% Journal of Asian Natural Products Research 2005 7 165-169 Sterols from the pericarp of Sphaerophysa salsula DC GUO-YU LI, JIN-HUI WANG and XIAN LI Structure 13C NMR ??????? -------------------------------------------------------------------------------- 12 . ergosta-8(14),22-diene-3,5,6,7-tetraol(3??,5??,6??,7??,22E) C28H46O4 ?????:68.9% Natural Product Research 2006 20 381-384 Cytotoxic sterols from marine-derived fungus Pennicillium sp. Yi Sun; Li Tian; Jian Huang; Wen Li; Yue-hu Pei Structure 13C NMR ??????? -------------------------------------------------------------------------------- 13 . stigmasta-4,6,8(14),22-tetraen-3-one ?????:68.9% China Journal of Chinese Materia Medica 2008 33 909-911 Studies on chemical constituents of Ranunculus ternatus XIONG Ying, DENG Kezhong, GAO Wenyuan, GUO Yuanqiang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 14 . ergosterol peroxide C28H44O3 ?????:68.9% Natural Product Sciences 2009 15 173-179 Steroids and Triterpenoid from the Fruit Bodies of Ganoderma lucidum and Their Cytotoxic Activity Lee, Joon-Seok; Lee, Mi-Kyoung; Hung, Tran-Manh; Lee, Ik-Soo; Min, Byung-Sun; Bae, Ki-Hwan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 15 . 9(11)-dehydroergosterol peroxide C28H44O3 ?????:68.9% Natural Product Sciences 2009 15 173-179 Steroids and Triterpenoid from the Fruit Bodies of Ganoderma lucidum and Their Cytotoxic Activity Lee, Joon-Seok; Lee, Mi-Kyoung; Hung, Tran-Manh; Lee, Ik-Soo; Min, Byung-Sun; Bae, Ki-Hwan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 16 . ergosterolperoxide(3??-hydroxy-5,8-epidioxyergosta-6,22-diene) C28H44O3 ?????:68.9% Phytochemistry 1991 30 4117-4120 Glycosides of ergosterol derivatives from Hericum erinacens Yoshihisa Takaishi, Minoru Uda, Takashi Ohashi, Kimiko Nakano, Koutarou Murakami, Toshiaki Tomimatsu Structure 13C NMR ??????? -------------------------------------------------------------------------------- 17 . (3??,5??,6??,7??,22E)-5,6-epoxyergosta-8(14),22-diene-3,7-diol C28H44O3 ?????:68.9% Chinese Journal of Marine Drugs 2008 27(4) 9-13 Studies on the chemical constituents from the endophytic fungus Penicillium sp.091402 of managrove plant Brugurera sexangula HAN Zhuang, MEI Wen-li, CUI Hai-bin, LIN Hai-peng, HONG Kui, DAI Hao-fu Structure 13C NMR ??????? -------------------------------------------------------------------------------- 18 . (3??,5??,22E,24R)-5,8-Epidioxyergosta-6,22-dien-3-ol ?????:68.9% Helvetica Chimica Acta 2010 93 1737-1741 Two New Sesquiterpenes from the Fungus Stereum sp. Fang-Fang Liu, Guo-Hong Li, Zhong-Shan Yang, Xi Zheng, Yue Yang and Ke-Qin Zhang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 19 . (22E)-5??-Ergosta-2,22-dien-6-one ?????:68.9% Steroids 1996 61 540-543 New synthetic strategy for the synthesis of 24-epibrassinolide Carme Brosa, Rita Puig, Xavier Comas, Cristina Fern??ndez Structure 13C NMR ??????? -------------------------------------------------------------------------------- 20 . Ergosterol peroxide ?????:68.9% Archives of Pharmacal Research 1997 20 201-205 Anticomplementary activity of ergosterol peroxide fromNaematoloma fasciculare and reassignment of NMR data Dong Seon Kim, Nam-In Baek, Sei Ryang Oh, Keun Young Jung and Im Seon Lee, et al. Structure 13C NMR ??????? -------------------------------------------------------------------------------- 21 . Ergosta-4,6,8(14),22-tetraene-3-one ?????:68.9% Archives of Pharmacal Research 2002 25 851-855 Cytotoxic ergosterols from paecilomyces sp. J300 Hak Cheol Kwon, Sang Deuk Zee, Sae Yun Cho, Sang Un Choi and Kang Ro Lee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 22 . Ergosterol peroxide ?????:68.9% Archives of Pharmacal Research 2006 29 479-483 Constituents from the fruiting bodies of Ganoderma applanatum and their aldose reductase inhibitory activity Sang Hyun Lee, Sang Hee Shim, Ju Sun Kim and Sam Sik Kang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 23 . Ergosterol peroxide ?????:68.9% Archives of Pharmacal Research 2009 32 1573-1579 Steroids and triterpenes from the fruit bodies of Ganoderma lucidum and their anti-complement activity Hyo Won Seo, Tran Manh Hung, MinKyun Na, Hyun Ju Jung and Jin Cheol Kim, et al. Structure 13C NMR ??????? -------------------------------------------------------------------------------- 24 . 22E-5??,6??-epoxyergosta-8(14),22-diene-3??,7??-diol ?????:68.9% Chinese Journal of Medicinal Chemistry 2006 16 93-97 Bioactive alkaloids and sterols from a marine fungus 96F197 SONG Shan-shan, WANG Nai-li, GAO Hao, LIU Hong-wei, ZHANG Qing-hua, MICHIO Namikoshi, YAO Xin-sheng Structure 13C NMR ??????? -------------------------------------------------------------------------------- 25 . (3??,5??,6??,7??,22E)-5,6-?????????-8(14),22-???-3,7-???? C28H44O3 ?????:68.9% Chinese Journal of Medicinal Chemistry 2009 19 200-205 Chemical constituents from the endophytic fungus Acremonium sp. J1 of Antiaris toxicaria QUE Dong-mei, DAI Hao-fu, ZENG Yan-bo, WU Jiao, MEI Wen-li Structure 13C NMR ??????? -------------------------------------------------------------------------------- 26 . citrcoanthrasteroid C29H44O2 ?????:68.9% Tetrahedron Letters 1995 36 7481-7482 Citreoanthrasteroid, a new metabolite of a hybrid strain KO 0011 derived from Penicillium citreo-viride B. IFO 6200 and 4692 Seiji Kosemura, Sota Uotsu, Shosuke Yamamura Structure 13C NMR ??????? -------------------------------------------------------------------------------- 27 . 24-Ethylcholesta-7,22-diene-3??,5??,6??-triol ?????:68.9% Bulletin of the Korean Chemical Society 2011 32 697-700 Isolation of Protein Tyrosine Phosphatase 1B Inhibitory Constituents from the Sclerotia of Polyporus umbellatus Fries Hee Sang Lee, In Hyun Hwang, Jeong Ah Kim, Ji Young Choi, Tae Su Jang, Hiruyuki Osada, Jong Seog Ahn*, MinKyun Na*, Seung Ho Lee* Structure 13C NMR ??????? -------------------------------------------------------------------------------- 28 . 5??,8??-epidioxy-(20S,22E,24R-)-ergosta-6,22-dien-3??-ol C28H44O3 ?????:68.9% Natural Product Research and Development 2004 16 277-280 METABOLITES OF RHIZOPUS ARRHIZUS 3078 LI Guo-you; LI Bo-gang; LIU Guang-ye; ZHANG Guo-lin Structure 13C NMR ??????? -------------------------------------------------------------------------------- 29 . ergosta-4,6,8(14),22-tetraen-3-one ?????:68.9% Natural Product Research and Development 2000 12(6) 33-36 STUDIES ON THE CHEMICAL CONSTITUENTS OF PHELLINUS YAMANOI He Jian; Feng Xiaozhang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 30 . Citreoanthrasteroid A C28H40O2 ?????:68.9% Tetrahedron 2000 56 2595-2602 Three New Metabolites of Hybrid Strain KO 0231, Derived from Penicillium citreo-viride IFO 6200 and 4692 Takashi Nakada, Shosuke Yamamura Structure 13C NMR ??????? -------------------------------------------------------------------------------- 31 . 5??,6??-epoxy-5??-ergosta-8(14),22E-diene-3??,7??-diol ?????:68.9% Journal of the Chinese Chemical Society 1995 42 97-100 Constituents of Fruit Bodies of Tramete orientalis ??????(Huey-Ling Chen);??????(Hung-Cheh Chiang) Structure 13C NMR ??????? -------------------------------------------------------------------------------- 32 . 5??,6??-epoxy-(22E,24R)-ergosta-8(14),22-diene-3??,7??-diol ?????:68.9% Journal of the Chinese Chemical Society 2011 58 893-898 Sterols from the Stems of Momordica charantia Yun-Wen Liao,Chiy-Rong Chen,Jue-Liang Hsu, Hsueh-Ling Cheng, Wen-Ling Shih,Yueh-Hsiung Kuo, Tzou-Chi Huanga,* and Chi-I Chang* Structure 13C NMR ??????? -------------------------------------------------------------------------------- 33 . ergosterol peroxide C28H44O3 ?????:68.9% Natural product sciences 2011 17 85-89 Cytotoxicity of Ergosterol Derivatives from the Fruiting Bodies of Hygrophorus russula Lee, Ik-Soo; Kim, Jin-Pyo; Na, Min-Kyun; Jung, Hyun-Ju; Min, Byung-Sun; Bae, Ki-Hwan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 34 . (22E,24S)-ergost-5,22-dien-3??-ol ?????:68.9% Academic Journal of Second Military Medical University 2010 31 421-424 Studies on chemical constituents of Anthogorgia sp. XU Yuan-yuan, LI Ling, YI Yang-hua, ZHANG Wen Structure 13C NMR ??????? -------------------------------------------------------------------------------- 35 . 22E-5??,6??-epoxyergosta-8(14),22-diene-3??,7??-diol C28H44O3 ?????:68.9% Journal of Shenyang Pharmaceutical University 2012 29 678-684 A new disecosteroid from an endolichenic fungal stain Sporormiella irregularis(No.71-11-4-1) LI Yan-jun; LI Xiao-xia; CHEN Guo-dong; GAO Hao; GUO Liang-dong; YAO Xin-sheng Structure 13C NMR ??????? -------------------------------------------------------------------------------- 36 . 5??,8??-Epidioxy-(20S,22E,24R)-ergosta-6,22-dien-3??-ol C28H44O3 ?????:68.9% Chinese Journal of Applied & Environmental Biology 2005 11 67-70 STEROLS FROM ASPERGILLUS OCHRACEUS 43 LI Guoyou; LI Bogang; LIU Guangye & ZHANG Guolin Structure 13C NMR ??????? -------------------------------------------------------------------------------- 37 . 5??,8??-Epidioxy-(22E,24R)-ergosta-6,22-diene-3??-ol C28H44O3 ?????:68.9% Chinese Journal of Applied & Environmental Biology 2006 12 30-33 Chemical Study on Poikilospermum naucleiforum ZHANG Ailian; & ZHANG Guolin Structure 13C NMR ??????? -------------------------------------------------------------------------------- 38 . 5??,8??-Epidioxy-(20S,22E,24R)-ergosta-6,22-diene-3??-ol C28H44O3 ?????:68.9% Chinese Journal of Applied & Environmental Biology 2007 13 66-68 Chemical Study on Aspergillus sp.136 QIN Ling; LI Bogang; GUAN Jiafa & ZHANG Guolin Structure 13C NMR ??????? -------------------------------------------------------------------------------- 39 . ergosterol peroxide ?????:68.9% Lishizhen Medicine and Materia Medica Research 2006 17 1178-1181 Chemical Constituents of Inonotus obliquus ZHAO Fen-qin, PIAO Hui-shan Structure 13C NMR ??????? -------------------------------------------------------------------------------- 40 . 3??-hydroxy-5??,8??-epidiocyergosta-6E,22E-diene C28H44O3 ?????:68.9% Journal of Chinese Medicinal Materials 2006 29 1186-1187 ???????????о? ????, ????, ÷???, ????? Structure 13C NMR ??????? -------------------------------------------------------------------------------- 41 . 5??,6??-epoxyergost-8(14),22-dien-3??,7??-diol ?????:68.9% Journal of Chinese Medicinal Materials 2010 33 1262-1265 Studies on the Chemical Constituents from Petroleum Ether Portion of Abelmoschus esculentus JIA Lu, LI Dong, JING Lin-lin, GUO Ming-ming Structure 13C NMR ??????? -------------------------------------------------------------------------------- 42 . 22E,24R-5??,6??-epoxyergosta-8(14),22-diene-3??,7??-diol ?????:68.9% European Journal of Plant Pathology 2012 134 239-247 Toxins from a symbiotic fungus, Leptographium qinlingensis associated with Dendroctonus armandi and their in vitro toxicities to Pinus armandi seedlings Xiao-Jun Li, Jin-Ming Gao, Hui Chen, An-Ling Zhang, Ming Tang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 43 . ergosta-5,77,22-trien-3-ol ?????:68.9% Periodical of Ocean University of China 2011 41 086-090 Chemical Constituents of Sponge Xestospongia testudinaria from the South China sea KONG Wen-Wen, HAN Lei, LI Liang, SHAO Chang-Lun, ZHANG Rong, Nicole J.de Voogd, WANG Chang-Yun Structure 13C NMR ??????? -------------------------------------------------------------------------------- 44 . (22E,24S)-24-methylcholest-4,22-diene-3??,6??-diol C28H46O2 ?????:68.9% Phytochemistry Letters 2014 9 1-6 New 3??,6??-dihydroxy and 3??,5??,6??-trihydroxy sterols from marine bryozoan Bugula neritina in South China Sea and their cytotoxicity Xiang-Rong Tian, Hai-Feng Tang, Yu-Shan Li, Hou-Wen Lin, Xiao-Pei Fan, Jun-Tao Feng, Xing Zhang Structure 13C NMR ??????? -------------------------------------------------------------------------------- 45 . stigmast-4,6,8(14),22-tetra-en-3-one ?????:68.9% Chinese Joumal of Experimental Traditional Medical Fomulae 2011 17 113-115 Studies on Chemical Constituents of Chloroform Portion of Cortex Ailanthi MAI Jing-biao, FENG Jian, HE Yu, XI Xiao-lan Structure 13C NMR ??????? |
2楼2015-06-15 15:46:30
