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高尚胜

新虫 (小有名气)

[求助] 微谱求助 谢谢 已有1人参与

13C NMR (101 MHz, DMSO)
31.26, 34.47, 55.66, 60.13, 60.72, 69.73, 73.28, 76.88, 76.99, 100.35, 112.90, 115.45, 120.12, 135.98, 144.61, 148.80

[ Last edited by 卓越_先锋 on 2015-6-15 at 20:28 ]
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高尚胜

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2楼: Originally posted by 乔金为 at 2015-06-15 14:56:40
2-methoxy-4-(3'-hydroxy-n-butyl)-phenol-1-O-β-D-glucopyranoside
C17H26O8     相似度:82.3%
Journal of Asian Natural Products Research          2002          4          43-46
PHENOLIC GLUCOSIDES  ...

您好,能不能再帮我查一下这个,非常感谢,急用。13C NMR (151 MHz, CD3OD)
62.13, 64.55, 70.17, 73.16, 73.99, 75.16, 77.26, 94.91, 105.15, 105.80, 116.26, 122.83, 132.51, 135.73, 158.62, 159.22, 161.75, 163.17, 166.21, 170.73, 179.81
3楼2015-06-15 15:39:56
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乔金为

新虫 (小有名气)

【答案】应助回帖

感谢参与,应助指数 +1
2-methoxy-4-(3'-hydroxy-n-butyl)-phenol-1-O-β-D-glucopyranoside
C17H26O8     相似度:82.3%
Journal of Asian Natural Products Research          2002          4          43-46
PHENOLIC GLUCOSIDES FROM OXYTROPIS MYRIOPHYLLA
JIANG-HAI LU, YI LIU, GUANG-ZHONG TU and YU-YING ZHAO
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

2 .     1-O-(β-D-Glucosyl)-2-[2-methoxy-4-(-hydroxypropyl)-phenoxy]-propan-3-ol
    相似度:78.9%
Chemistry of Natural Compounds          2010          46          308-309
Chemical constituents from the roots of Actinidia chinensis
Xuefeng Zhou, Yonghong Liu, Lan Tang, Peng Zhang and Jizhou Wu
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

3 .     carthamoside B3
C18H26O9     相似度:77.7%
Journal of Asian Natural Products Research          2008          10          817-821
New aromatic glucosides from Carthamus tinctorius
Yu-Zhi Zhoua, Li Qiaoa, Huan Chena, Rui-Feng Lib, Hui-Ming Huaa and Yue-Hu Peia
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

4 .     eugenyl-O-β-D-glucopyranoside
C16H22O7     相似度:75%
Acta Botanica Yunnanica          1999          21(4)          505-511
Chemical Constituents from the Flowers of Eupatorium adenophorum
DING Zhi-Hui,GUO Yu-Bin,DINGJing-Kai
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

5 .     2-methoxy-4-(2'-hydroxyethyl)-phenyl-1-O-β-D-glucopyranoside
    相似度:75%
China Journal of Chinese Materia Medica          2003          28          1153-1155
Studies on the Constituents rom the Stems of Spatholobus suberectus
CHENG Jun, LIANG Hong, WANG Yuan, ZHAO YuYing
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

6 .     eugenylglucoside
    相似度:75%
Journal of Natural Products          1988          Vol 51          496
Eugenylglucoside, a New Natural Phenylpropanoid Heteroside from Melissa officinalis
Aurore Mulkens, Ilias Kapetanidis
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

7 .     2-Methoxy-4-(2-propenyl) phenyl-β-D-glucoside
    相似度:75%
Archives of Pharmacal Research          2007          30          1067-1074
Lignan and terpene constituents from the aerial parts of saussurea pulchella
Sang Un Choi, Min Cheol Yang, Kyu Ha Lee, Ki Hyun Kim and Kang Ro Lee
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

8 .     Eugenyl-β-D-glucopyranoside
    相似度:75%
Archives of Pharmacal Research          2007          30          1471-1475
Two new phenolic constituents ofHumulus japonicus and their cytotoxicity testIn Vitro
Byung Chul Yu, Min Cheol Yang, Kyu Ha Lee, Ki Hyun Kim and Sang Un Choi, et al.
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

9 .     citrusin C
C16H22O7     相似度:75%
Natural Product Research and Development          2010          22          419-421
Chemical Constituents from the Leaves of Phellodendron chinense Schneid var.glabriusculum Schneid
WANG Nan-nan;WANG Ye; YANG Jian-qiong
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

10 .     4-allyl-2-methoxyphenyl β-D-glucopyranoside
    相似度:75%
Medicinal Chemistry Research          2014          23          496–502
Synthesis and in vitro evaluation of antifungal and cytotoxic activities of eugenol glycosides
Thiago Belarmino de Souza, Marina Orlandi, Luiz Felipe Leomil Coelho, Luiz Cosme Cotta Malaquias, Amanda Latercia Tranches Dias, Roberta Ribeiro de Carvalho, Naiara Chaves Silva, Diogo Teixeira Carvalho
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

11 .     eugenyl-O-β-D-glucopyranoside
    相似度:75%
Chinese Journal of Pharmaceuticals          2014          45          626-645
Chemical Constituents from the n-Butanol Fraction of Senecio solidagineus
LI Dingxiang, CHOU Guixin, WANG Zhengtao
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

12 .     Adenophoraside A
C15H19NO7     相似度:68.7%
Journal of Natural Medicines          2010          64          245-251
Novel phenolic glycosides, adenophorasides A–E, from Adenophora roots
Yuka Koike, Motonori Fukumura, Yasuaki Hirai, Yumiko Hori and Shiho Usui, et al.
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

13 .     4-O-β-D-glucopyranosylvanillyl alcohol
    相似度:68.7%
Molecules          2012          17          5013-5020
Glycosylation of Vanillin and 8-Nordihydrocapsaicin by Cultured Eucalyptus perriniana Cells
Daisuke Sato, Yuki Eshita, Hisashi Katsuragi, Hiroki Hamada, Kei Shimoda and Naoji Kubota
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

14 .     pinoresinol-4,4'-di-O-β-D-glucopyranoside
    相似度:68.7%
Journal of Chinese Medicinal Materials          2014          37          809-812
Chemical Constituents of Eucommia ulmoide
WANG Shuang-yan, DINGLin-fen, WU Xing-de, WANG Hai-yin, ZHAO Qin-shi, SONG Liu-dong
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

15 .     androsin
    相似度:62.5%
Helvetica Chimica Acta          2004          Vol. 87          598
Phenyl and Phenylethyl Glycosides from Picrorhiza scrophulariiflora
Sheng-Xiong Huang, Xun Liao, Quan-Jiang Nie, Li-Sheng Ding, and Shu-Lin Peng
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

16 .     (-)-(7R,8S)-guaiacylglycerol 8-O-β-D-glucopyranoside
    相似度:62.5%
Journal of Natural Products          2008          71(4)          647-654
Glycosides from the Root of Iodes cirrhosa
Maoluo Gan, Yanling Zhang, Sheng Lin, Mingtao Liu, Weixia Song, Jiachen Zi, Yongchun Yang, Xiaona Fan, Jiangong Shi, Jinfeng Hu, Jiandong Sun, and Naihong Chen
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

17 .     2-(3-hydroxy-4-methoxyphenyl)ethyl 1-O-β-D-glucopyranoside
C15H22O8     相似度:62.5%
Chemical & Pharmaceutical Bulletin          1991          39          1047-1050
Studies on the Nepalese Crude Drugs. XII. On the Phenolic Compounds from the Root of Scutellaria prostrata JACQ. ex BENTH.
Yuichi KIKUCHI,Yukinori MIYAICHI,Yumi YAMAGUCHI,Haruhisa KIZU and Tsuyoshi TOMIMORI
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

18 .     kalopanaxin A
C16H20O8     相似度:62.5%
Chemical & Pharmaceutical Bulletin          1991          39          865-870
Studies on the Constituents of the Bark of Kalopanax pictus NAKAI
Kazuko SANO,Shuichi SANADA,Yoshiteru IDA and Junzo SHOJI
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

19 .     coniferin
C16H22O8     相似度:62.5%
Chemical & Pharmaceutical Bulletin          1991          39          865-870
Studies on the Constituents of the Bark of Kalopanax pictus NAKAI
Kazuko SANO,Shuichi SANADA,Yoshiteru IDA and Junzo SHOJI
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

20 .     scopolin
C16H18O9     相似度:62.5%
Chemical & Pharmaceutical Bulletin          1985          33          396-399
Coumarin and Secoiridoid Glucosides from Bark of Olea africana and Olea capensis
HIROKI TSUKAMOTO,SUEO HISADA and SANSEI NISHIBE
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

21 .     (+)-pinoresinol di-O-β-D-glucopyranoside
C32H42O16     相似度:62.5%
Chemical & Pharmaceutical Bulletin          1983          31          2993-2997
The Constituents of Eucommia ulmoides OLIV. I. Isolation of (+)-Medioresinol Di-O-β-D-glucopyranoside
TAKESHI DEYAMA
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

22 .     2-(3-Hydroxy-4-methoxyphenyl)ethyl-1-O-β-D-glucopyranoside
C15H22O8     相似度:62.5%
Chemistry of Natural Compounds          2002          38          473-519
PHENOLIC COMPOUNDS OF PLANTS OF THE Scutellaria GENUS. DISTRIBUTION, STRUCTURE, AND PROPERTIES
V. M. Malikov and M. P. Yuldashev
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

23 .     2-(3-Hydroxy-4-methoxyphenyl)ethyl-1-O-β-D-glucopyranoside
C15H22O8     相似度:62.5%
Chemistry of Natural Compounds          2002          38          473-519
PHENOLIC COMPOUNDS OF PLANTS OF THE Scutellaria GENUS.DISTRIBUTION, STRUCTURE, AND PROPERTIES
V. M. Malikov and M. P. Yuldashev
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

24 .     7-O-β-D-glucopyranoside
    相似度:62.5%
Chemistry of Natural Compounds          1987          23          660-662
13C NMR SPECTRA OF SOME COUMARINS OF Haplophyllum obtusifolium
A. D. Vdovin, E. Kh. Batirov, A. D. Matkarimov, M. R. Yagudaev, and V. M. Malikov
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

25 .     scopolin
    相似度:62.5%
Chemistry of Natural Compounds          1986          22          267-269
A CHEMICAL STUDY OF PLANTS OF THE MONGOLIAN FLORA LARISIDE - A NEW SCOPOLETIN GLYCOSIDE FROM Salsola larioifolia
S. Narantuyaa, D. Batsuren, E. Kh. Batirov, and V. M. Malikov
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

26 .     vanillic acid 4-O-β-glucoside(3-methoxy 4-glucosyl-benzoic acid)
    相似度:62.5%
China Journal of Chinese Materia Medica          2008          33          1021-1023
Water-soluble constituents from roots of Capparis tenera
SU Dongmin, TANG Wenzhao, YU Shishan, LIU Yunbao, QU Jing, YU Dequan
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

27 .     scopolin
    相似度:62.5%
China Journal of Chinese Materia Medica          2008          33          1032-1035
Studies on chemical constituents of Saussurea laniceps
DAWA Zhuoma, ZHOU Yan, BAI Yang, GESANG Suolang, XIE Ping, DING Lisheng
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

28 .     7-hydroxylnaphthalide-O-β-D-glucopyranoside
    相似度:62.5%
China Journal of Chinese Materia Medica          2008          33          269-272
Chemical constituents in roots of Hemerocallis fulva
YANG Zhongduo, LI Tao, LI Yuanchao
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

29 .     pinoresinol-di-O-β-D-glucopyranoside
    相似度:62.5%
China Journal of Chinese Materia Medica          2002          27          199-201
Chemical Constituents from Alyxia sinensis
WANG Gangli, YAN Hua, HOU Qingyun, LU Yang, GONG Ningbo, LIN Ruichao
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

30 .     geniposidic acid
C16H22O10     相似度:62.5%
China Journal of Chinese Materia Medica          2000          25          728-730
Studies on Chemical Costituents of Cistanche tubulosa (Schenk)R. Wight
SONG Zhihong, MO Shaohong, CHEN Yan, TU Pengfei, ZHAO Yuying, ZHENG Junhua
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

31 .     scopolin
C15H20O10     相似度:62.5%
China Journal of Chinese Materia Medica          1994          19          166-167
Studies on the Chemcial Constituents of Artmisia dalailamae Kraschen
Yang Fuquan, Ou Qingyu and Yu Weile
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

32 .     mentzeloside
C15H22O9     相似度:62.5%
Journal of Natural Products          1980          Vol 43          649-707
Iridoids. A Review
Leticia J. El-Naggar, Jack L. Beal
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

33 .     mentzeloeide
    相似度:62.5%
Journal of Natural Products          1982          Vol 45          539-550
Iridoid Glycosides From Mentzelia decapetala
Leticia J. El-Naggar, Jack L. Bell, Raymond W. Doskotch
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

34 .     deutzioside
    相似度:62.5%
Journal of Natural Products          1983          Vol 46          614-618
Scabrosidol, A New Highly Oxygenated Iridoid Glucoside from Deutzia scabra
Paola Esposito, Carlo Iavarone, Alina Sen, Corrado Trogolo
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

35 .     scopoletin 7-glucoside
    相似度:62.5%
Journal of Natural Products          1987          Vol 50          774
Flavonol and Coumarin Glycosides from Artemisia incanescens
J. Alberto Marco, Oscar Barberá, J. Sánchez-Parareda
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

36 .     feruloyl sucrose
    相似度:62.5%
Acta Pharmaceutica Sinica          1999          Vol 34          839-841
STUDIES ON CHEMICAL CONSTITUENTS FROM ACANTHOPANAX SENTICOSUS (RUPR.ET MAXIM.) HARMS
Wu Lijun(Wu LJ); Ruan Lijun(Ruan LJ); Zheng Jian(Zheng J); Wang Feifei(Wang FF); Ding Fuli(Ding FL) and Gong Haiping(Gong HP)
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

37 .     scopolin
    相似度:62.5%
Phytochemistry          1992          31          4376-4377
A Furanocoumarin glucoside from stembark of Skimmia japonica
Johannes Reisch, Stefan H. Achenbach
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

38 .     scopolin
    相似度:62.5%
Korean Journal of Pharmacognosy          1999          30(3)          295-300
Chemical Components from the Stem Bark of Rhus javanica L.
Chung, Sun-Chae; Hwang, Bang-Yeon; Oh, Gab-Jin; Kang, Shin-Jung; Kim, Mi-Jeong; Choi, Woo-Hoi; Lee, Kyong-Soon; Ro, Jai-Seup
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

39 .     Scopolin
    相似度:62.5%
Archives of Pharmacal Research          2011          Vol 34, No 9          1561-1569
Inhibition of 5-Lipoxygenase and Skin Inflammation by the Aerial Parts of Artemisia capillaris and its Constituents
Oh Song Kwon, Jae Sue Choi, Md. Nurul Islam, Yeong Shik Kim, and Hyun Pyo Kim
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

40 .     scopolin
    相似度:62.5%
Phytochemistry          1989          28          1550-1552
A coumarin glucoside from xeromphis obovata
S. Sibanda,B. Ndengu,G. Multari,V. Pompi,C. Galeffi
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

41 .     (+)-(7S,8S)-guaiacylglycerol 8-O-β-D-glucopyranoside
    相似度:62.5%
China Journal of Chinese Materia Medica          2010          35          456-467
Constituents from a water-soluble portion of ethanolic extract of Iodes cirrhosa
GAN Maoluo; ZHU Chenggen; ZHANG Yanling; ZI Jiachen; SONG Weixia; YANG Yongchun; SHI Jiangong
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

42 .     Deutzioside
    相似度:62.5%
Phytochemistry          1981          20          71-83
Iridoid mono- and di-glycosides in Mentzelia
Søren Rosendal Jensen, Carl Bjarne Mikkelsen, Bent Juhl Nielsen
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

43 .     compound
    相似度:62.5%
Phytochemistry          2010          71          598-604
Constituents and secondary metabolite natural products in fresh and deteriorated cassava roots
Soad A.L. Bayoumi, Michael G. Rowan, John R. Beeching, Ian S. Blagbrough
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

44 .     东莨菪苷
C16H18O9     相似度:62.5%
Chinese Traditional and Herbal Drugs          2008          39          823-825
灰毡毛忍冬花蕾的化学成分研究
陈雨;冯煦;贾晓东;董云发;梁敬钰;王鸣;孙浩
Structure      13C NMR   碳谱模拟图
--------------------------------------------------------------------------------

45 .     东莨若苷
C16H18O9     相似度:62.5%
Chinese Traditional and Herbal Drugs          2007          38          1795-1797
天山雪莲的化学成分研究
王晓玲;李启发;丁立生
Structure      13C NMR   碳谱模拟图
2楼2015-06-15 14:56:40
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