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[求助]
本人新手,得到的实验数据一头雾水.请高人帮忙分析下数据,并画一下孔径分布图. 已有1人参与
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Quantachrome Instruments Quantachrome Autosorb Automated Gas Sorption System Report Autosorb 1 for Windows 1.55 File name: C:\QCdata\PhysData\LZF-150407-1.raw Sample ID: 2015-4-9 Description: blue Comments: Operator: QU Sample weight: 0.1238 g Analysis gas: Nitrogen X sect. area: 16.2 挪/molec Non-ideality: 6.58e-05 Adsbate (DRP): Nitrogen Bath Temp.: 77.30 Outgas Temp: 25.0 癈 Outgas Time: 30.0 hrs Analysis Time: 183.1 min P/Po tolerance: 3 Equil. time: 2 End of run: 04/09/2015 19:35 Station #: 1 PC sw. version: 1.55 TempComp: Off Isotherm P/Po Volume P/Po Volume P/Po Volume [cc/g] STP [cc/g] STP [cc/g] STP 6.0379e-02 0.5054 7.0992e-01 1.6794 6.3889e-01 1.7628 1.1147e-01 0.6156 7.5983e-01 1.7648 5.8860e-01 1.6798 1.6129e-01 0.7310 8.0942e-01 1.9389 5.3874e-01 1.5431 2.1121e-01 0.8147 8.5896e-01 2.2152 4.8838e-01 1.4019 2.6106e-01 0.9136 9.0871e-01 2.5155 4.3836e-01 1.3209 3.1098e-01 1.0011 9.5766e-01 3.1698 3.8844e-01 1.1974 3.6077e-01 1.1072 9.9940e-01 4.9737 3.3835e-01 1.1266 4.1088e-01 1.1514 9.4154e-01 3.3162 2.8841e-01 1.0076 4.6057e-01 1.2473 8.8948e-01 2.8014 2.3842e-01 0.8873 5.1063e-01 1.3030 8.3935e-01 2.4703 1.8838e-01 0.7764 5.6035e-01 1.4153 7.8916e-01 2.2106 1.3839e-01 0.6780 6.1029e-01 1.4886 7.3876e-01 2.0892 8.8382e-02 0.5658 6.6002e-01 1.5911 6.8889e-01 1.9359 4.0007e-02 0.4615 04/10/2015 Quantachrome Instruments Quantachrome Autosorb Automated Gas Sorption System Report Autosorb 1 for Windows 1.55 File name: C:\QCdata\PhysData\LZF-150407-1.raw Sample ID: 2015-4-9 Description: blue Comments: Operator: QU Sample weight: 0.1238 g Analysis gas: Nitrogen X sect. area: 16.2 挪/molec Non-ideality: 6.58e-05 Adsbate (DRP): Nitrogen Bath Temp.: 77.30 Outgas Temp: 25.0 癈 Outgas Time: 30.0 hrs Analysis Time: 183.1 min P/Po tolerance: 3 Equil. time: 2 End of run: 04/09/2015 19:35 Station #: 1 PC sw. version: 1.55 TempComp: Off AREA-VOLUME-PORE SIZE SUMMARY SURFACE AREA DATA Multipoint BET.............................................. 3.270E+00 m?g Single Point BET............................................ 3.002E+00 m?g BJH Method Cumulative Adsorption Surface Area............... 4.280E+00 m?g BJH Method Cumulative Desorption Surface Area............... 4.597E+00 m?g DH Method Cumulative Adsorption Surface Area................ 4.403E+00 m?g DH Method Cumulative Desorption Surface Area................ 4.707E+00 m?g PORE VOLUME DATA Total Pore Volume for pores with Radius less than 15958.6 ?at P/Po = 0.99940....................... 7.712E-03 cc/g BJH Method Cumulative Adsorption Pore Volume................ 8.182E-03 cc/g BJH Method Cumulative Desorption Pore Volume................ 8.291E-03 cc/g BJH Interpolated Cumulative Adsorption Pore Volume for pores in the range of 5000.0 to 0.0 ?Radius...................... 7.084E-03 cc/g BJH Interpolated Cumulative Desorption Pore Volume for pores in the range of 5000.0 to 0.0 ?Radius...................... 7.294E-03 cc/g DH Method Cumulative Adsorption Pore Volume................. 7.957E-03 cc/g DH Method Cumulative Desorption Pore Volume................. 8.066E-03 cc/g PORE SIZE DATA Average Pore Radius ....................................... 4.717E+01 ? BJH Method Adsorption Pore Radius (Mode).................. 8.741E+00 ? BJH Method Desorption Pore Radius (Mode).................. 1.196E+01 ? DH Method Adsorption Pore Radius (Mode).................. 8.741E+00 ? DH Method Desorption Pore Radius (Mode).................. 1.196E+01 ? DATA REDUCTION PARAMETERS Thermal Transpiration : OFF Last Po Acquired 512.00 mm Hg MaxiDose : ON Initial Fill : OFF DoseWizard : OFF BJH/DH Moving Average Size : 0 Thickness method : DeBoer Interaction Constant (K) 0.0000 nm^3 x kJ/mol ADSORBATE MODEL PARAMETERS Adsorbate Type = Nitrogen Adsorbate Temp. = 77.3500 K Molecular Weight = 28.0134 g/mol Cross-Sect. Area = 16.2000 挪/molecule Liquid Density = 0.8060 g/cc Critical Temp. = 126.2000 K Critical Pressure = 33.5000 atm Average Diameter = 0.3000 nm Polarizability = 1.4600 (cc/molec) x 1e-24 Magnetic Suscept. = 2.0000 (cc/molec) x 1e-29 Molecular Density = 6.7000 (molec/cm? x 1e14 Surface Tension = 8.8500 erg/cm? Contact Angle = 0.0000 degrees Supercritical Ads. Constant K = 1.0000 ADSORBENT MODEL PARAMETERS Adsorbent Type = Carbon Atom Diameter = 0.3400 nm Polarizability = 1.0200 (cc/molecule) x 1e-24 Magnetic Suscept. = 13.5000 (cc/molecule) x 1e-29 Surface Atom Density = 38.4500 (molec/cm? x 1e14 Adsorbent Density = 2.2460 g/cc DR exponent (n) = 2.0000 04/10/2015 Quantachrome Instruments Quantachrome Autosorb Automated Gas Sorption System Report Autosorb 1 for Windows 1.55 File name: C:\QCdata\PhysData\LZF-150407-1.raw Sample ID: 2015-4-9 Description: blue Comments: Operator: QU Sample weight: 0.1238 g Analysis gas: Nitrogen X sect. area: 16.2 挪/molec Non-ideality: 6.58e-05 Adsbate (DRP): Nitrogen Bath Temp.: 77.30 Outgas Temp: 25.0 癈 Outgas Time: 30.0 hrs Analysis Time: 183.1 min P/Po tolerance: 3 Equil. time: 2 End of run: 04/09/2015 19:35 Station #: 1 PC sw. version: 1.55 TempComp: Off BJH ADSORPTION PORE SIZE DISTRIBUTION Radius Pore Vol Pore Surf Area Dv(r) Ds(r) Dv(log r) Ds(log r) ? [cc/g] [m?g] [cc/?g] [m??g] [cc/g] [m?g] 7.44 1.523E-04 4.095E-01 1.106E-04 2.975E-01 1.889E-03 5.080E+00 8.74 4.363E-04 1.059E+00 2.306E-04 5.275E-01 4.633E-03 1.060E+01 9.98 6.010E-04 1.390E+00 1.332E-04 2.671E-01 3.056E-03 6.127E+00 11.24 8.527E-04 1.837E+00 1.951E-04 3.472E-01 5.043E-03 8.974E+00 12.58 1.063E-03 2.172E+00 1.515E-04 2.409E-01 4.384E-03 6.970E+00 14.04 1.354E-03 2.586E+00 1.904E-04 2.713E-01 6.149E-03 8.761E+00 15.66 1.404E-03 2.651E+00 2.918E-05 3.726E-02 1.051E-03 1.342E+00 17.50 1.641E-03 2.921E+00 1.210E-04 1.382E-01 4.869E-03 5.564E+00 19.63 1.733E-03 3.015E+00 3.995E-05 4.069E-02 1.804E-03 1.837E+00 22.15 2.006E-03 3.261E+00 9.984E-05 9.015E-02 5.086E-03 4.592E+00 25.19 2.148E-03 3.374E+00 4.249E-05 3.373E-02 2.461E-03 1.954E+00 28.99 2.369E-03 3.527E+00 5.219E-05 3.601E-02 3.477E-03 2.399E+00 33.88 2.539E-03 3.627E+00 3.046E-05 1.798E-02 2.371E-03 1.400E+00 40.52 2.687E-03 3.700E+00 1.928E-05 9.518E-03 1.794E-03 8.854E-01 50.08 3.040E-03 3.841E+00 3.094E-05 1.236E-02 3.553E-03 1.419E+00 65.27 3.606E-03 4.014E+00 2.982E-05 9.138E-03 4.450E-03 1.364E+00 94.14 4.184E-03 4.137E+00 1.491E-05 3.167E-03 3.185E-03 6.766E-01 175.45 5.374E-03 4.273E+00 9.610E-06 1.095E-03 3.715E-03 4.235E-01 8098.00 8.182E-03 4.280E+00 1.786E-07 4.412E-07 1.537E-03 3.795E-03 04/10/2015 Quantachrome Instruments Quantachrome Autosorb Automated Gas Sorption System Report Autosorb 1 for Windows 1.55 File name: C:\QCdata\PhysData\LZF-150407-1.raw Sample ID: 2015-4-9 Description: blue Comments: Operator: QU Sample weight: 0.1238 g Analysis gas: Nitrogen X sect. area: 16.2 挪/molec Non-ideality: 6.58e-05 Adsbate (DRP): Nitrogen Bath Temp.: 77.30 Outgas Temp: 25.0 癈 Outgas Time: 30.0 hrs Analysis Time: 183.1 min P/Po tolerance: 3 Equil. time: 2 End of run: 04/09/2015 19:35 Station #: 1 PC sw. version: 1.55 TempComp: Off BJH DESORPTION PORE SIZE DISTRIBUTION Radius Pore Vol Pore Surf Area Dv(r) Ds(r) Dv(log r) Ds(log r) ? [cc/g] [m?g] [cc/?g] [m??g] [cc/g] [m?g] 6.81 0.000E+00 0.000E+00 0.000E+00 0.000E+00 0.000E+00 0.000E+00 8.16 1.694E-04 4.152E-01 1.339E-04 3.280E-01 2.511E-03 6.152E+00 9.41 3.280E-04 7.522E-01 1.291E-04 2.744E-01 2.793E-03 5.936E+00 10.66 5.725E-04 1.211E+00 1.934E-04 3.631E-01 4.740E-03 8.898E+00 11.96 8.733E-04 1.714E+00 2.240E-04 3.746E-01 6.161E-03 1.030E+01 13.36 1.176E-03 2.168E+00 2.073E-04 3.103E-01 6.372E-03 9.538E+00 14.91 1.289E-03 2.319E+00 6.895E-05 9.249E-02 2.364E-03 3.172E+00 16.65 1.596E-03 2.687E+00 1.662E-04 1.997E-01 6.365E-03 7.646E+00 18.64 1.747E-03 2.849E+00 7.049E-05 7.563E-02 3.023E-03 3.243E+00 20.99 2.093E-03 3.179E+00 1.356E-04 1.292E-01 6.545E-03 6.237E+00 23.79 2.418E-03 3.452E+00 1.062E-04 8.926E-02 5.811E-03 4.884E+00 27.25 2.569E-03 3.563E+00 3.919E-05 2.876E-02 2.455E-03 1.802E+00 31.65 2.967E-03 3.815E+00 8.063E-05 5.096E-02 5.864E-03 3.706E+00 37.45 3.298E-03 3.992E+00 4.963E-05 2.650E-02 4.269E-03 2.280E+00 45.65 3.530E-03 4.093E+00 2.382E-05 1.044E-02 2.494E-03 1.093E+00 58.20 4.071E-03 4.279E+00 3.519E-05 1.209E-02 4.689E-03 1.611E+00 80.21 4.737E-03 4.445E+00 2.326E-05 5.801E-03 4.250E-03 1.060E+00 134.29 5.711E-03 4.590E+00 1.225E-05 1.824E-03 3.673E-03 5.471E-01 8066.33 8.291E-03 4.597E+00 1.634E-07 4.053E-07 1.315E-03 3.260E-03  无标题.jpg |
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liwentao2010: 金币-1, 屏蔽内容, 禁止发布个人信息，首次警告并扣1BB 2015-05-31 20:54:51
liwentao2010: 金币-1, 屏蔽内容, 禁止发布个人信息，首次警告并扣1BB 2015-05-31 20:54:51
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2楼2015-05-31 09:48:34
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3楼2015-05-31 19:24:03
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