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老实人sdu3375

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专业: 血液、泌尿与生殖系统药物

[求助] 急求谢谢大家！！！已有1人参与

13C NMR，化合物可能不纯，溶剂为甲醇。数据如下：
10.66,10.77,10.92,11.48,11.89,13.40,13.52,15.41,15.67,16.01,16.95,17.21,17.31,18.16,18.44,18.85,22.33,26.24,28.88,29.05,29.36,29.76,30.67,34.23,35.06,36.84,40.84,43.60,44.43,67.82,68.28,68.85,70.44,70.64,70.82,71.08,72.39,74.09,75.23,77.47,79.64,101.21,173.35,174.31,174.46。
谢谢啦！

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1楼 2015-05-11 19:49:49

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

卓越_先锋

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老实人sdu3375: 金币+25 2015-05-12 17:33:39

查询结果：共查到1327个化合物(查询结果仅供参考)
1 .    1α,3β,23-trihydroxy-olean-12-en-29-oate-23-O-α[3,4-diacetylrhamnopyranosyl] -29-O-α-rhamnopyranoside
C46H72O15    相似度:69.5%
Phytochemistry       2003                81-88
Antimicrobial activity of pentacyclic triterpenes isolated from African Combretaceae
David R. Katerere, Alexander I. Gray, Robert J. Nash, Roger D. Waigh
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
2 .    3-O-β-D-xylopyranosyl-(1→3)-α-L-rhamnopyranosyl-(1→2)-β-D-xylopyranosyl-12β,30-dihydroxy-olean-28,13β-olide
C46H74O17    相似度:69.5%
Carbohydrate Research       2011       346       2881-2885
New triterpenoid saponins from Patrinia scabiosaefolia
Liang Gao, Lin Zhang, Nan Li, Jiang-Yun Liu, Pei-lie Cai, Shi-lin Yang
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
3 .    Quamoclin V
C49H84O24    相似度:69.3%
Chemical & Pharmaceutical Bulletin       2012       60       1083-1087
Three New Resin Glycosides and a New Tetrahydropyran Derivative from the Seeds of Quamoclit pennata
Masateru Ono, Yoshinari Takaki, Masamitsu Takatsuji, Kousuke Akiyama, Masafumi Okawa, Junei Kinjo, Hiroyuki Miyashita, Hitoshi Yoshimitsu, Toshihiro Nohara
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
4 .    glycoside(1a)
相似度:68.8%
Chemical & Pharmaceutical Bulletin       2004       52(1)       142-145
Pregnane- and Furostane-Type Oligoglycosides from the Seeds of Allium tuberosum
Tsuyoshi IKEDA, Hidetsugu TSUMAGARI, Masafumi OKAWA, and Toshihiro NOHARA
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
5 .    23-hydroxyimberbic acid 3-O-α-L-rhamnopyranosyl-23-O-α-L-4-acetylrhamnopyranoside
C44H70O14    相似度:68.8%
Journal of Natural Products       1989       Vol 52       528
New Mono- and Bi-Desmosidic Triterpenoids Isolated from Combretum padoides Leaves
Colin B. Rogers
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
6 .    23-hydroxyimberbic acid 3-O-α-L-rhamnopyranosyl-23-O-α-L-rhamnoside
C42H68O13    相似度:68.8%
Journal of Natural Products       1989       Vol 52       528
New Mono- and Bi-Desmosidic Triterpenoids Isolated from Combretum padoides Leaves
Colin B. Rogers
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
7 .    lα,3β,23,29-tetrahydroxyolean-12-ene 3-O-α-L-rhamnopyranosyl-23-O-α-L-rhamnopyranoside
相似度:68.8%
Journal of Natural Products       1989       Vol 52       528
New Mono- and Bi-Desmosidic Triterpenoids Isolated from Combretum padoides Leaves
Colin B. Rogers
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
8 .    11,12-di-O-iso-butyryl-8,9-anhydro-erythromycin A 6,9-hemiketal
C45H77NO14    相似度:68.8%
Bioorganic & Medicinal Chemistry Letters       2007       17       6340-6344
Design and synthesis via click chemistry of 8,9-anhydroerythromycin A 6,9-hemiketal analogues with anti-MRSA and -VRE activity
Akihiro Sugawara, Toshiaki Sunazuka, Tomoyasu Hirose, Kenichiro Nagai, Yukie Yamaguchi, Hideaki Hanaki, K. Barry Sharpless, Satoshi ōmura
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
9 .    stellatoside E
C42H66O14    相似度:68.8%
Heterocycles       2012       85       1377-1392
New Triterpenoid Saponins from Stenocereus eruca
Kazutaka Kakuta, Takeshi Koike, Kaoru Kinoshita, Satoru Ito, Kiyotaka Koyama, and Kunio Takahashi
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
10 .    roxithromycin
相似度:68.8%
Magnetic Resonance in Chemistry       1990       28       846-855
Analysis of the 1H and 13C NMR spectra of the novel macrolide antibiotic roxithromycin. Structure and conformation in solution
Josyane Gharbi-Benarous, Marcel Delaforge, Isabelle Artaud and Jean-Pierre Girault
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
11 .    hauptsaponine S2
相似度:68.8%
Pharmazie       1987       42       143-143
Steroidsaponine aus Dioscorea hispida L.
Ng. X. Cuong, D. Zeigan, Gabriele Voigt, und K. Hiller
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
12 .    Macaoside H
C45H74O17    相似度:68.8%
Journal of Natural Products       2014       77       1770-1783
Anti-Inflammatory Spirostanol and Furostanol Saponins from Solanum macaonense
Chia-Lin Lee, Tsong-Long Hwang, Juan-Cheng Yang, Hao-Ting Cheng, Wan-Jung He, Chiao-Ting Yen, Chao-Lin Kuo, Chao-Jung Chen, Wen-Yi Chang, and Yang-Chang Wu
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
13 .    Compound 6
C48H80O14    相似度:68.7%
Bioorganic & Medicinal Chemistry Letters       2009       19       2310-2314
Synthesis, cytotoxicity, and haemolytic activity of chacotrioside lupane-type neosaponins and their germanicane-type rearrangement products
Charles Gauthier, Jean Legault, Marianne Piochon, Serge Lavoie, Samuel Tremblay, André Pichette
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
14 .    Compound 7
C48H80O15    相似度:68.7%
Bioorganic & Medicinal Chemistry Letters       2009       19       2310-2314
Synthesis, cytotoxicity, and haemolytic activity of chacotrioside lupane-type neosaponins and their germanicane-type rearrangement products
Charles Gauthier, Jean Legault, Marianne Piochon, Serge Lavoie, Samuel Tremblay, André Pichette
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
15 .    stellatoside C
C48H76O18    相似度:68.7%
Heterocycles       2012       85       1377-1392
New Triterpenoid Saponins from Stenocereus eruca
Kazutaka Kakuta, Takeshi Koike, Kaoru Kinoshita, Satoru Ito, Kiyotaka Koyama, and Kunio Takahashi
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
16 .    kudinoside A
C47H74O18    相似度:68.0%
Phytochemistry       1996       43       443-445
Triterpenoid glycosides from Ilex kudincha
Ming-An Ouyang, Han-Qing Wang, Zi-Li Chen, Chong-Ren Yang
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
17 .    Kudinoside F
C47H74O18    相似度:68.0%
Phytochemistry       1996       41       871-877
Triterpenes and triterpenoid glycosides from the leaves of Ilex kudincha
Ming-An Ouyang, Chong-Ren Yang, Zi-Li Chen, Han-Qing Wang
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
18 .    (20S)-3β,20,21-trihydroxydammar-24-ene 3-O-[α-L-rhamnopyranosyl(1→2)][β-D-xylopyranosyl(1→3)]-β-D-glucopyranoside
相似度:68.0%
Chinese Chemical Letters       2010       21       699-701
A new dammarane-type triterpene saponin from Gynostemma pentaphyllum
Lin Shi; Jia Qing Cao; Wei Li; Hong Zhao; Yu Qing Zhao
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
19 .    dudinoside F
C47H74O18    相似度:68.0%

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