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13C NMR (DMSO) δ184.26,169.32,162.40,161.58,158.10,152.94,140.82,108.16,107.21,104.11,104.06,101.54,101.33,101.16,100.18,77.39,77.12,76.86,75.95,73.99,73.92,70.54,70.06,69.15,61.50,55.97,20.67. |
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辣笔v小新
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【答案】应助回帖
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感谢参与，应助指数 +1
安然然: 金币+20, ★★★★★最佳答案 2015-05-07 15:20:49
感谢参与，应助指数 +1
安然然: 金币+20, ★★★★★最佳答案 2015-05-07 15:20:49
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20.67,55.97,61.50,69.15,70.06,70.54,73.92,73.99,75.95,76.86,77.12,77.39,100.18,101.16,101.33,101.54,104.06,104.11,107.21,108.16,140.82,152.94,158.10,161.58,162.40,169.32,184.26 查询结果：共查到42个化合物(查询结果仅供参考) 1 . rubrofusarin 6β-gentiobioside C27H32O15 相似度:100% Planta Medica 1990 56 120-121 Two Phenol Compounds from Berchemia racemosa Takao Inoue, Shin-ichi Nagashima, Setsuko Ohata,Masato Shinoda, and Nobuko Sakura Structure 13C NMR 碳谱模拟图 2 . rubrofusarin-6-β-gentiobioside 相似度:100% Planta Medica 1989 55 276-280 New Antihepatotoxic Naphtho-pyrone Glycosides from the Seeds of Cassia tora Sui-Ming Wong, Mary Moy Wong, Otto Seligmann, and Hildebert Wagner Structure 13C NMR 碳谱模拟图 3 . rubrofusarin 6-O-β-gentiobioside 相似度:100% Chemical & Pharmaceutical Bulletin 1999 47 1121-1127 Phenolic Constituents of Cassia Seeds and Antibacterial Effect of Some Naphthalenes and Anthraquinones on Methicillin-Resistant Staphylococcus aureus Tsutomu HATANO,Hiroshi UEBAYASHI,Hideyuki ITO,Sumiko SHIOTA,Tomofusa TSUCHIYA and Takashi YOSHIDA Structure 13C NMR 碳谱模拟图 4 . rubrofusarin 6-O-β-gentiobioside C27H32O15 相似度:96.2% Chemical & Pharmaceutical Bulletin 1988 36 3980-3984 Studies on the Constituents of Seeds of Cassia obtusifolia L. : The Structures of Two Naphthopyrone Glycosides SUSUMU KITANAKA and MICHIO TAKAIDO Structure 13C NMR 碳谱模拟图 5 . Rubrofusarin-6-O-β-D-gentiobioside 相似度:96.2% Archives of Pharmacal Research 2006 29 587-590 Naphthopyrone glucosides from the seeds ofCassia tora with inhibitory activity on advanced glycation end products (AGEs) formation Ga Young Lee, Dae Sik Jang, Yun Mi Lee, Jong Min Kim and Jin Sook Kim Structure 13C NMR 碳谱模拟图 6 . 8-hydroxy-3-methyl-6-methoxyxanthone-1-O-β-D-glucopyranosyl-(1→6)-β-D-glucopyranose C27H32O15 相似度:96.2% Natural Product Communications 2008 3 795-798 Two New Xanthone Glycosides from Ventilago leiocarpaBenth. Li-Li Wang, Jian-Ping Zuo, Lei Ma, Xia-Chang Wang and Li-Hong Hu Structure 13C NMR 碳谱模拟图 7 . rubrofusarin gentiobioside 相似度:96.2% Chinese Joumal of Experimental Traditional Medical Fomulae 2009 15 35-37 决明子中苷类化学成分研究 唐力英, 王祝举, 赫炎, 付梅红, 方婧, 吴宏伟, 黄璐琦 Structure 13C NMR 碳谱模拟图 8 . nor-rubrofusarin gentiobioside C26H30O15 相似度:85.1% Chemical & Pharmaceutical Bulletin 1999 47 1121-1127 Phenolic Constituents of Cassia Seeds and Antibacterial Effect of Some Naphthalenes and Anthraquinones on Methicillin-Resistant Staphylococcus aureus Tsutomu HATANO,Hiroshi UEBAYASHI,Hideyuki ITO,Sumiko SHIOTA,Tomofusa TSUCHIYA and Takashi YOSHIDA Structure 13C NMR 碳谱模拟图 9 . cassiaside C C27H32O15 相似度:81.4% Chemical & Pharmaceutical Bulletin 1988 36 3980-3984 Studies on the Constituents of Seeds of Cassia obtusifolia L. : The Structures of Two Naphthopyrone Glycosides SUSUMU KITANAKA and MICHIO TAKAIDO Structure 13C NMR 碳谱模拟图 10 . rubrofusarin 6-O-α-L-rhamnosyl- (1→6)-O-β-D-glucopyranoside C27H32O14 相似度:81.4% Journal of Asian Natural Products Research 2007 9 499-503 Two new benzochromone glycosides from the stem of Berchemia racemosa JIAN-WEI SHEN, JIAN-SHUANG JIANG, XIAO-FENG ZHANG,CHONG-FEI ZHENGand PEI-CHENG ZHANG Structure 13C NMR 碳谱模拟图 11 . toralactone-9-O-β-D-gentiobioside 相似度:81.4% Natural Product Research and Development 2010 22 60-62 α-Glucosidase Inhibitory Activity of Compounds from Eriocaulon buergerianum ZHU Hai-yan; YE Guan Structure 13C NMR 碳谱模拟图 12 . cassiaside B C26H30O14 相似度:77.7% Chemical & Pharmaceutical Bulletin 1988 36 3980-3984 Studies on the Constituents of Seeds of Cassia obtusifolia L. : The Structures of Two Naphthopyrone Glycosides SUSUMU KITANAKA and MICHIO TAKAIDO Structure 13C NMR 碳谱模拟图 13 . compound 2a 相似度:77.7% Journal of Asian Natural Products Research 2007 9 499-503 Two new benzochromone glycosides from the stem of Berchemia racemosa JIAN-WEI SHEN, JIAN-SHUANG JIANG, XIAO-FENG ZHANG,CHONG-FEI ZHENGand PEI-CHENG ZHANG Structure 13C NMR 碳谱模拟图 14 . demethylflavasperone gentiobioside C27H32O15 相似度:77.7% Chemical & Pharmaceutical Bulletin 1999 47 1121-1127 Phenolic Constituents of Cassia Seeds and Antibacterial Effect of Some Naphthalenes and Anthraquinones on Methicillin-Resistant Staphylococcus aureus Tsutomu HATANO,Hiroshi UEBAYASHI,Hideyuki ITO,Sumiko SHIOTA,Tomofusa TSUCHIYA and Takashi YOSHIDA Structure 13C NMR 碳谱模拟图 15 . Toralactone-9-O-β-D-gentiobioside 相似度:77.7% Archives of Pharmacal Research 2006 29 587-590 Naphthopyrone glucosides from the seeds ofCassia tora with inhibitory activity on advanced glycation end products (AGEs) formation Ga Young Lee, Dae Sik Jang, Yun Mi Lee, Jong Min Kim and Jin Sook Kim Structure 13C NMR 碳谱模拟图 16 . toralactone 9-O-yl-β-D-glucopyranosyl-(1→6)-β-D-glucopyranoside C27H32O15 相似度:77.7% The Journal of Organic Chemistry 2003 68 6309-6313 Total Synthesis of the Antiallergic Naphtho-r-pyrone Tetraglucoside, Cassiaside C2, Isolated from Cassia Seeds Zhaojun Zhang and Biao Yu Structure 13C NMR 碳谱模拟图 17 . casside B 相似度:77.7% Chinese Joumal of Experimental Traditional Medical Fomulae 2009 15 35-37 决明子中苷类化学成分研究 唐力英, 王祝举, 赫炎, 付梅红, 方婧, 吴宏伟, 黄璐琦 Structure 13C NMR 碳谱模拟图 18 . cassiaside C 相似度:77.7% Chemical & Pharmaceutical Bulletin 1998 46 1650−1652 Antiallergic Agent from Natural Sources. Structures and Inhibitory Effect of Histamine Release of Naphthopyrone Glycosides from Seeds of Cassia obtusifolia L. Susumu KITANAKA, Toshimitu NAKAYAMA, Takeshi SHIBANO, Emika OHKOSHI, michio TAKIDO Structure 13C NMR 碳谱模拟图 19 . toralactone-9-β-gentiobioside. 9-[(β-D-glucopyranosyl)-(1→6)-O-D-glucopyranosyl)oxy]-10-hydroxy-7-methoxy-3-methyl-1H-naphtho[2,3-c]pyran-1-one C27H32O15 相似度:74.0% Planta Medica 1989 55 276-280 New Antihepatotoxic Naphtho-pyrone Glycosides from the Seeds of Cassia tora Sui-Ming Wong, Mary Moy Wong, Otto Seligmann, and Hildebert Wagner Structure 13C NMR 碳谱模拟图 20 . isorubrofusarin gentiobioside 相似度:74.0% Archives of Pharmacal Research 1997 20 513-515 A rubrofusarin gentiobioside isomer from roasted Cassia tora Hee Jung Lee, Jee Hyung Jung, Sam Sick Kang and Jae Sue Choi Structure 13C NMR 碳谱模拟图 21 . 8-hydroxy-3-methyl-6-methoxyxanthone-1-O-α-L-rhamnopyranosyl-(1→6)-β-D-glucopyranose C27H32O14 相似度:74.0% Natural Product Communications 2008 3 795-798 Two New Xanthone Glycosides from Ventilago leiocarpaBenth. Li-Li Wang, Jian-Ping Zuo, Lei Ma, Xia-Chang Wang and Li-Hong Hu Structure 13C NMR 碳谱模拟图 22 . rubrofusarin-6-O-β-(4-O-methylglucopyranoside) C22H24O10 相似度:70.3% The Journal of Antibiotics 2007 60 577-581 Comparison of the Bioactive Secondary Metabolites from the Scale Insect Pathogens, Anamorph Paecilomyces cinnamomeus, and Teleomorph Torrubiella luteorostrata FREE Masahiko Isaka, Somporn Palasarn, Kanokarn Kocharin and Nigel L Hywel-Jones Structure 13C NMR 碳谱模拟图 23 . (S)-torosachrysone 8-O-β-D-gentiobioside 相似度:66.6% Natural Product Research 1993 2 151-157 (R)-Torosachrysone and the 8-O-β-D-gentiobiosides of (R)- and (S)-torosachrysone from Fungi of the Genus Cortinarius.1 Susan N. Eagle; Melvyn Gill; Simon Saubern; Jin Yu Structure 13C NMR 碳谱模拟图 24 . torachrysone gentiobioside C26H34O14 相似度:66.6% Chemical & Pharmaceutical Bulletin 1999 47 1121-1127 Phenolic Constituents of Cassia Seeds and Antibacterial Effect of Some Naphthalenes and Anthraquinones on Methicillin-Resistant Staphylococcus aureus Tsutomu HATANO,Hiroshi UEBAYASHI,Hideyuki ITO,Sumiko SHIOTA,Tomofusa TSUCHIYA and Takashi YOSHIDA Structure 13C NMR 碳谱模拟图 25 . genistin 7-O-gentiobioside 相似度:66.6% Food Chemistry 2011 124 703-710 Novel isoflavone diglycoside in groundnut (Apios americana Medik) Kazuhiro Nara, Ken-ichi Nihei, Yasuo Ogasawara, Hidenori Koga, Yoji Kato Structure 13C NMR 碳谱模拟图 26 . Genistein-7-O-gentibioside C27H30O15 相似度:66.6% Journal of Agricultural and Food Chemistry 2013 61 2183-2187 Novel Isoflavone Glucosides in Groundnut (Apios americana Medik) and Their Antiandrogenic Activities Marina Ichige, Erina Fukuda, Saki Miida, Jun-ichiro Hattan, Norihiko Misawa, Shun Saito, Takahiro Fujimaki, Masaya Imoto, and Kazutoshi Shindo Structure 13C NMR 碳谱模拟图 27 . (S)-torosachrysone 8-O-β-D-gentiobioside 相似度:64.2% Australian Journal of Chemistry 2000 53 213-220 Pigments of Fungi. LXVI. The Gentiobiosides of (R)- and (S)-Torosachrysone from Australian Toadstools and Methods for Assaying the Enantiomeric Purity of Natural Torosachrysone Melvyn Gill, Simon Saubern and Jin Yu Structure 13C NMR 碳谱模拟图 28 . Triptexanthoside D C26H30O16 相似度:62.9% Chemistry of Natural Compounds 2008 44 514-515 FLAVONOIDS AND XANTHONES FROM Tripterospermum chinense Jing-Jing Fang and Guan Ye Structure 13C NMR 碳谱模拟图 29 . isoetin-7-O-β-D-glucopyranosyl-2'-O-α-D-glucopyranoside C27H30O17 相似度:62.9% Chinese Chemical Letters 2007 18 1367-1370 Four new constituents from Taraxacum mongolicum Shu Yun Shi, Qi Zhou Hua Peng, Chang Xin Zhou, Ming Hui Hu, Qiao Feng Tao , Xiao Jiang Hao , Joachim Stockigt, Yu Zhao Structure 13C NMR 碳谱模拟图 30 . isoetin-7-O-β-D-glucopyranosyl-2'-O-α-D-glucopyranoside C27H30O17 相似度:62.9% Chinese Chemical Letters 2007 18 1367-1370 Four new constituents from Taraxacum mongolicum Shu Yun Shi, Qi Zhou, Hua Peng, Chang Xin Zhou, Ming Hui Hu, Qiao Feng Tao, Xiao Jiang Hao, Joachim Stockigt, Yu Zhao Structure 13C NMR 碳谱模拟图 31 . isoetin-7-O-β-D-glucopyranosyl-2'-O-α-D-glucopyranoside C27H30O17 相似度:62.9% China Journal of Chinese Materia Medica 2008 33 1147-1157 Studies on chemical constituents from herbs of Taraxacum mongolicum SHI Shuyun, ZHOU Changxin, XU Yan, TAO Qiaofeng, BAI Hua, LU Fusheng, LIN Wenyan, CHEN Haiyong, ZHENG Wei, WANG Liwei, WU Yihang, ZENG Su, HUANG Kexin, ZHAO Yu, LI Xiaokun, QU Jia Structure 13C NMR 碳谱模拟图 32 . triptexanthoside D C26H30O16 相似度:62.9% Chemical & Pharmaceutical Bulletin 1999 47 962-965 Triptexanthosides A-E : Xanthone Glycosides from Aerial Parts of Tripterospermum japonicum Hideaki OTSUKA Structure 13C NMR 碳谱模拟图 33 . saikoisoflavonoside A 相似度:62.9% Acta Pharmaceutica Sinica 2009 Vol 44 63-68 Isoflavone glycosides from the bark of Maackia amurensis LI Xiong; LI Jian-fang; WANG Dong; WANG Wei-ning; CUI Zheng Structure 13C NMR 碳谱模拟图 34 . biochanin A 7-O-β-D-gentiobioside 相似度:62.9% Acta Pharmaceutica Sinica 2009 Vol 44 63-68 Isoflavone glycosides from the bark of Maackia amurensis LI Xiong; LI Jian-fang; WANG Dong; WANG Wei-ning; CUI Zheng Structure 13C NMR 碳谱模拟图 35 . 1-O-[β‑D-Glucopyranosyl-(1→6)-β‑D-Glucopyranosyl]-3,8-dihy-droxy-4,5-dimethoxyxanthone C27H32O17 相似度:62.9% Planta Medica 2014 80 502-508 Xanthone Glycosides from Swertia bimaculata with α-Glucosidase Inhibitory Activity Yue, Yao-Dong; Zhang, Yu-Tang; Liu, Zhao-Xia; Min, Qiu-Xia; Wan, Luo-Sheng; Wang, Yong-Long; Xiao, Zuo-Qi; Chen, Jia-Chun: Structure 13C NMR 碳谱模拟图 36 . formononetin 7-O-β-gentiobioside 相似度:62.9% Natural Medicines 1998 52 527-528 A New Isoflavone Glycoside from Heartwood of Maackia fauriei HWANG MYUNG-HUI,KWON YONG-SOO,KIM CHANG-MIN Structure 13C NMR 碳谱模拟图 37 . isoetin-7-O-β-D-glucopyranosyl-29-O-α-D-glucopyranoside C27H30O17 相似度:62.9% Journal of Separation Science 2008 31 683-688 Preparative isolation and purification of three flavonoid glycosides from Taraxacum mongolicum by high-speed counter-current chromatography Shuyun Shi, Yuping Zhang, Yu Zhao and Kelong Huang Structure 13C NMR 碳谱模拟图 38 . apigenin 7-O-(2G-rhamnosyl)-gentiobioside 相似度:62.0% Journal of Natural Products 1996 59 314-315 Flavone Glycosides from Lonicera gracilipes var. glandulosa Masao Kikuchi and Noriko Matsuda Structure 13C NMR 碳谱模拟图 39 . torosachrysone 8-β-D-gentiobioside C28H36O15 相似度:60.7% Chemical & Pharmaceutical Bulletin 1984 32 3436-3440 Torosachrysone and Physcion Gentiobiosides from the Seeds of Cassia torosa SUSUMU KITANAKA and MICHIO TAKIDO Structure 13C NMR 碳谱模拟图 40 . compound 1 相似度:60.7% Archives of Pharmacal Research 1991 14 105-108 Insecticidal isoflavon glycoside from Maackia amurensis Hasik Youn, Sangkyun Lee, Jin-Ho Cho and Hunseung Oh Structure 13C NMR 碳谱模拟图 41 . 2'-Hydoxy,5-methoxy Genistein-4',7-O-diglucoside C28H32O16 相似度:60.7% Journal of Agricultural and Food Chemistry 2013 61 2183-2187 Novel Isoflavone Glucosides in Groundnut (Apios americana Medik) and Their Antiandrogenic Activities Marina Ichige, Erina Fukuda, Saki Miida, Jun-ichiro Hattan, Norihiko Misawa, Shun Saito, Takahiro Fujimaki, Masaya Imoto, and Kazutoshi Shindo Structure 13C NMR 碳谱模拟图 42 . 1,4,8-trimethoxyxanthone-6-O-β-D-glucoronyl-(1→6)-O-β-D-glucoside C28H34O16 相似度:60.7% Chinese Journal of Natural Medicines 2014 12 693-696 Two new xanthones from Lomatogonium carinthiacum Ba-gen-na, Yu-Lan CHEN, Baderihu, Yu-Feng TONG, Ye-ri-gui, Qing-Hu WANG Structure 13C NMR 碳谱模拟图 |
2楼2015-05-07 15:13:58
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3楼2015-05-07 15:42:41