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fengfajin新虫 (小有名气)
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[求助]
求助微谱一个，谢谢帮忙 已有1人参与
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13 NMR(CDCl3, 100MHz) 碳谱数据如下： 53.53,54.60,54.63,56.14,56.42,60.73,72.16,72.72,72.75,74.24,86.00,87.22,87.25,102.96,103.02,108.64,114.34,118.93,131.50,131.52,137.79,145.08,146.80,153.37,153.66 |
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辣笔v小新
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【答案】应助回帖
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感谢参与，应助指数 +1
fengfajin: 金币+10, ★有帮助, ok 2015-05-07 10:18:55
感谢参与，应助指数 +1
fengfajin: 金币+10, ★有帮助, ok 2015-05-07 10:18:55
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???????????鵽48????????(???????????ο?) 1 . (??)-buddlenol C ?????:80.7% Natural Product Research and Development 2003 15 277-283 STUDIES ON THE PHENYLPROPANOIDS FROM CARAGANA ROSEA CUI Yi-ling; MU Qing; HU Chang-qi Structure 13C NMR ??????? 2 . Rayalinol 22H26O8 ?????:80% Tetrahedron 2010 66 1716-1720 A new lignan and a new sesquiterpene from Eurotia ceratoides (L.) Bina Shaheen Siddiqui, Kalamkas Zhanarbekovna Butabayeva, Gauhar Shahmanovna Burasheva, Sobiya Perwaiz, Syed Kashif Ali, Huma Aslam Bhatti Structure 13C NMR ??????? 3 . erythro-buddlenol C ?????:80% China Journal of Chinese Materia Medica 2013 38 2826-2831 Chemical constituents from stems of Aquilaria sinensis LI Wei, MEI Wen-li, WANG Hao, ZUO Wen-jian, YANG De-lan, DAI Hao-fu, Structure 13C NMR ??????? 4 . phyllostadimer A C42H50O16 ?????:76% Phytochemistry 2003 991-996 Two lignan dimers from bamboo stems (Phyllostachys edulis) Ai Suga, Yoshihisa Takaishi, Satoru Goto,Tatsuo Munakata, Izumi Yamauchi, Kentaro Kogure Structure 13C NMR ??????? 5 . Buddlenol C C22H26O8 ?????:75% Phytochemistry 1985 24 819-826 Lignans and neolignans from Buddleja davidii Peter J. Houghton Structure 13C NMR ??????? 6 . (-)-(7R,7'R,7''R,8S,8'S,8''S)-4',4''-Dihydroxy-3,3',3'',5,5'-pentamethoxy-7,9':7',9-diepoxy-4,8''-oxy-8,8'-sesquineolignan-7'',9''-diol C32H38O12 ?????:73.3% Journal of Natural Products 2011 74 1188-1200 Lignans and Neolignans from Sinocalamus affinis and Their Absolute Configurations Liang Xiong, Chenggeng Zhu, Yanru Li, Ye Tian, Sheng Lin, Shaopeng Yuan, Jinfeng Hu, Qi Hou, Naihong Chen, Yongchun Yang, and Jiangong Shi Structure 13C NMR ??????? 7 . (+)-de-O-methyhnagnolin C22H26O7 ?????:72% Phytochemistry 1993 34 1501-1507 Biotransformation of lignans: a specific microbial oxidation of (+)-eudesmin and (+)-magnolin by Aspergillus niger Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 8 . (+)-de-O-methylmagnolin ?????:72% Phytochemistry 1992 31 3666-3668 Phenolic lignans from flower buds of Magnolia fargesii Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 9 . hedyotisol A ?????:71.4% Chemical & Pharmaceutical Bulletin 2007 55(8) 1175-1180 Rhyncosides A??F, Phenolic Constituents from the Chinese Mangrove Plant Bruguiera sexangula var. rhynchopetala Shuyun BAO,Yi DING,Zhiwei DENG,Peter PROKSCH,d an Wenhan LIN Structure 13C NMR ??????? 10 . ficusesquilingnan A C31H36O11 ?????:70.3% Natural Product Research and Development 2014 26 1610-1613,1617 Chemical Constituents from the Twigs and Leaves of Endospermum chinense ZOU Tao, HE Hong-ping, ZHAO Qing, HAO Xiao-jiang Structure 13C NMR ??????? 11 . ficusesquilignan A C31H36O11 ?????:70.3% Journal of Yunnan College of Traditional Chinese Medicine 2011 34 21-23,27 HPLC Determination of Bulleyaconitine A in Aconitum georgei GONG Yun-Qi, ZHANG Wei, ZHU Ze Structure 13C NMR ??????? 12 . (-)-(7R,7'R,7''R,8S,8'S,8''S)-4',4''-Dihydroxy-3,3',3'',5-tetramethoxy-7,9':7',9-diepoxy-4,8''-oxy-8,8'-sesquineolignan-7'',9''-diol C31H36O11 ?????:70% Journal of Natural Products 2011 74 1188-1200 Lignans and Neolignans from Sinocalamus affinis and Their Absolute Configurations Liang Xiong, Chenggeng Zhu, Yanru Li, Ye Tian, Sheng Lin, Shaopeng Yuan, Jinfeng Hu, Qi Hou, Naihong Chen, Yongchun Yang, and Jiangong Shi Structure 13C NMR ??????? 13 . De-4'-O-methylmagnolin ?????:68% Phytochemistry 1993 32 1421-1424 Biotransformation of (+)-magnolin and (+)-yangabin in rat Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 14 . de-O-methylmagnollin ?????:68% Journal of the Chinese Chemical Society 1998 45 773-778 The Constituents from the Leaves of Magnolia coco ???a??(Hsi-Jung Yu);?????(Chien-Chih Chen);?x???M(Bor-Jinn Shieh) Structure 13C NMR ??????? 15 . (??)-ficusesquilignan A ?????:67.8% Natural Product Research and Development 2003 15 277-283 STUDIES ON THE PHENYLPROPANOIDS FROM CARAGANA ROSEA CUI Yi-ling; MU Qing; HU Chang-qi Structure 13C NMR ??????? 16 . (-)-(7R,7'R,7''S,8S,8'S,8''S)-4',4''-Dihydroxy-3,3',3'',5-tetramethoxy-7,9':7',9-diepoxy-4,8''-oxy-8,8'-sesquineolignan-7'',9''-diol C31H36O11 ?????:66.6% Journal of Natural Products 2011 74 1188-1200 Lignans and Neolignans from Sinocalamus affinis and Their Absolute Configurations Liang Xiong, Chenggeng Zhu, Yanru Li, Ye Tian, Sheng Lin, Shaopeng Yuan, Jinfeng Hu, Qi Hou, Naihong Chen, Yongchun Yang, and Jiangong Shi Structure 13C NMR ??????? 17 . ficusesquilingnan B C31H36O11 ?????:66.6% Natural Product Research and Development 2014 26 1610-1613,1617 Chemical Constituents from the Twigs and Leaves of Endospermum chinense ZOU Tao, HE Hong-ping, ZHAO Qing, HAO Xiao-jiang Structure 13C NMR ??????? 18 . ficusesquilignan B C31H36O11 ?????:66.6% Journal of Yunnan College of Traditional Chinese Medicine 2011 34 21-23,27 HPLC Determination of Bulleyaconitine A in Aconitum georgei GONG Yun-Qi, ZHANG Wei, ZHU Ze Structure 13C NMR ??????? 19 . thero-ficusesquilignan A ?????:66.6% China Journal of Chinese Materia Medica 2013 38 2826-2831 Chemical constituents from stems of Aquilaria sinensis LI Wei, MEI Wen-li, WANG Hao, ZUO Wen-jian, YANG De-lan, DAI Hao-fu, Structure 13C NMR ??????? 20 . hedyotisol B C42H50O16 ?????:65.5% Natural Product Research and Development 2014 26 1780-1784 Chemical Constituents from the Fruits of Capparis masaikai LIAO Jin-hua, HU Xu-jia*, YUAN Chun-mao, HE Hong-ping, DI Ying-tong Structure 13C NMR ??????? 21 . (??)-buddlenol D ?????:65.3% Natural Product Research and Development 2003 15 277-283 STUDIES ON THE PHENYLPROPANOIDS FROM CARAGANA ROSEA CUI Yi-ling; MU Qing; HU Chang-qi Structure 13C NMR ??????? 22 . (+)-(7'S,8'R,7''S,8''R)-Guaiacylglycerol ??-O-4'-Dihydrodisinapyl Ether C31H36O11 ?????:65.3% Chemistry & Biodiversity 2015 12 380−387 A Comparative Study on Hulled Adlay and Unhulled Adlay through Evaluation of Their LPS-Induced Anti-Inflammatory Effects, and Isolation of Pure Compounds Goeun Choi, Ah-Reum Han, Joo Hee Lee, Ji-Youn Park, Unwoo Kang, Jongki Hong, Yeong Shik Kim and Eun-Kyoung Seo Structure 13C NMR ??????? 23 . phyllostadimer B C42H50O16 ?????:64% Phytochemistry 2003 991-996 Two lignan dimers from bamboo stems (Phyllostachys edulis) Ai Suga, Yoshihisa Takaishi, Satoru Goto,Tatsuo Munakata, Izumi Yamauchi, Kentaro Kogure Structure 13C NMR ??????? 24 . (+)-magnolin ?????:64% Phytochemistry 1994 35 611-613 An insect growth inhibitory lignan from flower buds of Magnolia fargesii Mitsuo Miyazawa, Yukio Ishikawa, Hiroyuki Kasahara, Jun-ichi Yamanaka, Hiromu Kameoka Structure 13C NMR ??????? 25 . fragransin D1 C22H28O6 ?????:64% Phytochemistry 1988 27 563-568 New neolignans and lignans from the aril of Myristica fragrans Sumitra Hada,Masao Hattori,Yasuhiro Tezuka,Tohru Kikuchi,Tsuneo Namba Structure 13C NMR ??????? 26 . (+)-Medioresinol ?????:64% Journal of Chinese Pharmaceutical Sciences 2013 22 431-434 Chemical constituents from the leaves of Premna microphylla Turcz Zhengxi Hu, Yongbo Xue, Guangmin Yao, Zengwei Luo, Yanyan Wang*, Yonghui Zhang Structure 13C NMR ??????? 27 . threobuddlenol C ?????:64% China Journal of Chinese Materia Medica 2013 38 2826-2831 Chemical constituents from stems of Aquilaria sinensis LI Wei, MEI Wen-li, WANG Hao, ZUO Wen-jian, YANG De-lan, DAI Hao-fu, Structure 13C NMR ??????? 28 . 5'-medioresinol C21H24O7 ?????:64% Chinese Traditional and Herbal Drugs 2013 44 2358-2363 Chemical constituents from barks of Cinnamomum cassia growing in China ZHAO Kai, YIANG Yong, XUE Pei-feng, TU Peng-fei Structure 13C NMR ??????? 29 . (-)-(7R,7'R,7''S,8S,8'S,8''S)-4',4''-Dihydroxy-3,3',3'',5,5'-pentamethoxy-7,9':7',9-diepoxy-4,8''-oxy-8,8'-sesquineolignan-7'',9''-diol C32H38O12 ?????:63.3% Journal of Natural Products 2011 74 1188-1200 Lignans and Neolignans from Sinocalamus affinis and Their Absolute Configurations Liang Xiong, Chenggeng Zhu, Yanru Li, Ye Tian, Sheng Lin, Shaopeng Yuan, Jinfeng Hu, Qi Hou, Naihong Chen, Yongchun Yang, and Jiangong Shi Structure 13C NMR ??????? 30 . (??)-buddlenol D ?????:63.3% China Journal of Chinese Materia Medica 2013 38 2826-2831 Chemical constituents from stems of Aquilaria sinensis LI Wei, MEI Wen-li, WANG Hao, ZUO Wen-jian, YANG De-lan, DAI Hao-fu, Structure 13C NMR ??????? 31 . magnolin ?????:60% Journal of Chinese Pharmaceutical Sciences 2005 14 137-139 A Benzofuranoid Neolignan from Magnolia biondii Pamp LU Yan-hua; GAO Yang; WANG Zheng-tao; LIU Jian-qun; and WEI Dong-zhi Structure 13C NMR ??????? 32 . medioresinol ?????:60% Journal of Asian Natural Products Research 2001 3 95-102 Two New Germacranolides from Magnolia Grandiflora SHAO-HUA WU, XIAO-DONG LUO, YUN-BAO MA,XIAO-JIANG HAO, JUN ZHOU and DA-GANG WU Structure 13C NMR ??????? 33 . magnolin ?????:60% China Journal of Chinese Materia Medica 1995 20 102-104 Biolgically Active Lignins from Magnolia bilndii Pamp Ma Yuliang and Han Guiqiu Structure 13C NMR ??????? 34 . (+)-Magnolin ?????:60% Phytochemistry 1995 39 1027-1030 Biotransformation of lignans: Metabolism of (+)-eudesmin and (+)-magnolin in Spodoptera litura Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 35 . (+)-De-O-methylepimagnolin A C22H26O7 ?????:60% Phytochemistry 1994 35 1191-1193 Microbial oxidation of (+)-epimagnolin a by Aspergillus niger Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 36 . (+)-magnolin ?????:60% Phytochemistry 1993 32 1421-1424 Biotransformation of (+)-magnolin and (+)-yangabin in rat Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 37 . De-4'-O-methylyangabin ?????:60% Phytochemistry 1993 32 1421-1424 Biotransformation of (+)-magnolin and (+)-yangabin in rat Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 38 . (+)-magnolin ?????:60% Phytochemistry 1993 34 1501-1507 Biotransformation of lignans: a specific microbial oxidation of (+)-eudesmin and (+)-magnolin by Aspergillus niger Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 39 . de-4'-O-methyl-5'-hydroxymagnolin C22H26O8 ?????:60% Phytochemistry 1993 34 1501-1507 Biotransformation of lignans: a specific microbial oxidation of (+)-eudesmin and (+)-magnolin by Aspergillus niger Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 40 . (+)-magnolin ?????:60% Phytochemistry 1992 31 3666-3668 Phenolic lignans from flower buds of Magnolia fargesii Mitsuo Miyazawa, Hiroyuki Kasahara, Hiromu Kameoka Structure 13C NMR ??????? 41 . (+)-medioresinol C21H24O7 ?????:60% Korean Journal of Pharmacognosy 2000 31(3) 357-363 Phytochemical Constituents of Actinidia arguta Whang, Joon-Ih; Zee, Ok-Pyo; Moon, Hyung-In Structure 13C NMR ??????? 42 . (+)-medioresinol ?????:60% China Journal of Chinese Materia Medica 2010 35 1261-1271 Chemical constituents of stems and branches of Adina polycephala ZHANG Yanling; GAN Maoluo; LI Shuai; WANG Sujuan; ZHU Chenggen; YANG Yongchun; HU Jinfeng; CHEN Naihong; SHI Jiangong Structure 13C NMR ??????? 43 . (+)-fraxiresinol ?????:60% Chinese Traditional and Herbal Drugs 2008 39 1132-1135 Studies on chemical constituents of Ilex pernyi XIE Guang-bo; ZHAO Ming-bo; WANG Xiao-jing; TU Peng-fei Structure 13C NMR ??????? 44 . (-)-syringaresinol-4-O-??-D-glucopyranoside ?????:60% Pharmacy and Pharmacology Communications 1997 3 525-527 Lignans from Eleutherococcus senticosus (Siberian Ginseng) TATYANA N. MAKARIEVA, ANDREY S. DMITRENOK, VALENTIN A. STONIK, ASMITA V. PATEL and LESLEY M. CANFIELD Structure 13C NMR ??????? 45 . medioresinol ?????:60% Chinese Journal of Modern Applied Pharmacy 2013 30 115-118 Study on the Lignan Constituents in Seeds of Nandina Domestica Thunb. SHU Ji-cheng, LIU Jian-qun, PENG Cai-ying, WANG Ya-li Structure 13C NMR ??????? 46 . Pseuderesinol C21H24O8 ?????:60% Chemical & Pharmaceutical Bulletin 2012 60 1125-1133 Lignans and Triterpenes from the Root of Pseuderanthemum carruthersii var. atropurpureum Thi Nga Vo, Phi Linh Nguyen, Lam Truong Tuong, Lawrence Michael Pratt, Phung Nguyen Vo, Kim Phi Phung Nguyen, Ngoc Suong Nguyen Structure 13C NMR ??????? 47 . Medioresinol ?????:60% Guihaia 2013 33 191-194 Study on phenylpropanoids from hypocotyls of the mangrove plant Bruguiera gymnorrhiza YI Xiang-Xi, GAO Cheng-Hai*, HE Bi-Juan, CHEN Bo Structure 13C NMR ??????? 48 . (+)-Medioresinol ?????:60% Phytochemistry Letters 2015 11 80−84 Chemical constituents from the stems of Alyxia schlechteri Thurdpong Sribuhom, Uraiwan Sriphana, Yordhathai Thongsri, Chavi Yenjai Structure 13C NMR ??????? |
2楼2015-05-06 20:21:39
